Xie, Yuxuan et al.Download PDFPatent Trials and Appeals BoardMar 31, 202013030170 - (D) (P.T.A.B. Mar. 31, 2020) Copy Citation UNITED STATES PATENT AND TRADEMARK OFFICE UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www.uspto.gov APPLICATION NO. FILING DATE FIRST NAMED INVENTOR ATTORNEY DOCKET NO. CONFIRMATION NO. 13/030,170 02/18/2011 Yuxuan Xie 213532.00232 2131 21324 7590 03/31/2020 HAHN LOESER & PARKS, LLP 200 Public Square, Suite 2800 Cleveland, OH 44114 EXAMINER WALCK, BRIAN D ART UNIT PAPER NUMBER 1736 NOTIFICATION DATE DELIVERY MODE 03/31/2020 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address(es): patents@hahnlaw.com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE ____________ BEFORE THE PATENT TRIAL AND APPEAL BOARD ____________ Ex parte YUXUAN XIE, CHEN ZHU, JULIE M. CAIRNEY, SIMON P. RINGER, CHRISTOPHER R. KILLMORE, FRANK BARBARO, and JAMES WILLIAMS __________ Appeal 2019-004035 Application 13/030,170 Technology Center 1700 ____________ Before MICHAEL P. COLAIANNI, GEORGE C. BEST, and DEBRA L. DENNETT, Administrative Patent Judges. COLAIANNI, Administrative Patent Judge. DECISION ON APPEAL Appellant appeals under 35 U.S.C. § 134(a) the final rejection of claims 15–19 and 21–30.1 Claims 1–14, the other claims pending in this application, stand withdrawn from consideration by the Examiner. Claim 20 is canceled. We have jurisdiction over the appeal. 35 U.S.C. § 6(b). We AFFIRM. 1 We use the word “Appellant” to refer to “applicant” as defined in 37 C.F.R. § 1.42. Appellant identifies Nucor Corp. as the real party in interest (Appeal Br. 3). Appeal 2019-004035 Application 13/030,170 2 STATEMENT OF THE CASE Appellant’s invention is directed to a method for making a high strength thin cast strip by a twin roll caster (Spec. ¶ 1; Fig. 2). The Specification describes that twin roll casting has enabled the development of a Nb-microalloyed steel thin cast strip (id. at ¶ 7). According to the Specification, the Nb-microalloyed steel’s properties can be improved by nitriding (id.). Claim 15 is illustrative (emphasis added): 15. A method of preparing nitrided thin cast steel strip comprising the steps of: assembling internally a cooled roll caster having laterally positioned casting rolls forming a nip between them, and forming a casting pool of molten steel supported on the casting rolls above the nip and confined adjacent the ends of the casting rolls by side dams, counter rotating the casting rolls to solidify metal shells on the casting rolls as the casting rolls move through the casting pool, and forming from the metal shells downwardly through the nip between the casting rolls a steel strip, and cooling the steel strip at a rate of at least 10 °C per second, coiling the cast strip and nitriding the steel strip to provide a composition comprising by weight, less than 0.25% carbon, between 0.20 and 2.0% manganese, between 0.05 and 0.50% silicon, less than 0.01 % aluminum, between 0.01 % and 0.20% niobium, and between 0.01 and 0.075% nitrogen, and having a majority of the microstructure comprised of bainite and acicular ferrite, having more than 70% niobium in solid solution prior to nitriding, and having yield strength between about 600 MPa and 723.4 MPa, tensile strength between about 650 MPa and 802.4 MPa, and having a total elongation of between about 10% and 16.5%. Appeal Br. 31 (Claims App.). Appeal 2019-004035 Application 13/030,170 3 The Examiner maintains the following rejection: 1. Claims 15–19 and 21–30 are rejected under 35 U.S.C. § 103(a) as unpatentable over Williams et al. (US 2008/0219879 A1; published Sept. 11, 2008, “Williams”), in view of C.H. Knerr et al., Gas Nitriding, ASM Handbook: Vol. 4, Heat Treating, ASM International (1991) 387–409 (“Knerr”) (Final Act. 3–7). Appellant offers separate arguments in support of independent claim 15 and dependent claims 16–19 (Appeal Br. 8–24). Appellant argues claims 21 and 22 as a group; claims 23–26 as a group; and claims 27–30 as a group (id. at 24–26). Each of these claims and claims groups will be discussed separately. FINDINGS OF FACT & ANALYSIS After review of the respective positions provided by Appellant and the Examiner, we affirm the Examiner’s prior art rejection under 35 U.S.C. § 103(a) for the reasons presented by the Examiner and add the following for emphasis. A. Rejection of claims 15–19 and 21–30 as unpatentable over the combination of Williams and Knerr. 1. Claim 15 With respect to claim 15, the Examiner’s findings and conclusions regarding Williams and Knerr are located on pages 3–5 of the Final Office Action. The Examiner finds that Williams’ method of preparing a thin cast steel strip would have rendered obvious each step of the method recited in Appeal 2019-004035 Application 13/030,170 4 independent claim 15, except that Williams does not disclose two recited features (Final Act. 3–5). Regarding Williams’ first missing feature, the Examiner finds that Williams’ method does not disclose nitriding the steel strip to produce a composition with between 0.01 and 0.075% nitrogen (id. at 4). The Examiner finds that Knerr discloses “[p]rincipal reasons for nitriding” steel, including a list of several properties that are conferred to steel that has been nitrided (id. (citing Knerr 387)). The Examiner determined that it would have been obvious for one of ordinary skill in the art at the time of the invention to nitride Williams’ steel strip as suggested by Knerr (Final Act. 4). According to the Examiner, one of ordinary skill in the art would have been motivated to implement Knerr’s nitriding step in preparing Williams’ steel strip “to obtain high surface hardness, increase wear resistance and antigalling properties, improve fatigue life [and] corrosion resistance, and to obtain a surface that is resistant to the softening effect of heat at . . . the nitriding temperature” (id. (citing Knerr 387)). With respect to Williams’ second missing feature, the Examiner finds that Williams does not explicitly disclose each of the claimed ranges for the steel strips’ properties (id. at 5). The Examiner, however, finds that Williams’ thin cast steel strip has a yield strength of at least 650 MPa (overlapping the instantly claimed range of between about 600 MPa and 723.4 MPa) and tensile strength of at least 700 MPa (overlapping the instantly claimed range of between about 650 MPa and 802.4 MPa) and Appeal 2019-004035 Application 13/030,170 5 having a total elongation of at least 10% (overlapping the instantly claimed range of at least 10%). Id. at 4. The Examiner determines that it would have been obvious to one of ordinary skill in the art at the time the invention was made to select any portion of the disclosed ranges, including the ranges recited in claim 15, as “Williams discloses the same utility throughout the disclosed ranges” (id. at 5). Appellant argues that one of ordinary skill in the art would not have combined Knerr’s nitriding step with Williams’ method of preparing a thin cast steel strip less than 3 mm in thickness (Appeal Br. 10). Specifically, Appellant argues that Knerr does not teach or suggest nitriding steel less than 6 mm in thickness (id.). We are not persuaded by this argument because it is directed to limitations not recited in independent claim 15, which is silent regarding any required thickness. We, furthermore, agree with the Examiner that there is no teaching that nitriding is limited to case hardening a surface of a thicker steel (Ans. 6). Rather, Kerr explicitly states that “at suitable temperature[,] all steels are capable of forming iron nitrides in the presence of nascent nitrogen” (Knerr 387) (emphasis added). Appellant argues that Knerr recognizes the trade-off between increased hardness and increased brittleness and that “[t]hese potential drawbacks are only amplified in a thin steel strip of less than 3 mm as taught by Williams” (Appeal Br. 10). In particular, Appellant argues that Knerr teaches away from nitriding Williams’ coiled strip because Knerr’s nitrided steel requires additional stabilizing treatment or stress relieving steps, which require grinding and machining the strip (id. at 15–17). Appellant argues that Knerr recognizes nitriding’s effects on aluminum-containing steels, such Appeal 2019-004035 Application 13/030,170 6 as the tradeoff of low ductility (id. at 18; see also id. at 19 (arguing that the Examiner ignores “the drawbacks of Knerr’s[,] e.g.[,] nitriding ductility/hardness tradeoffs; distortion and dimensional changes; stabilizing/stress relieving; etc.”)). Appellant’s arguments are not persuasive because Knerr explicitly discloses that “[f]or many parts, this lengthy [stress relieving] procedure may not be required” (Knerr 394). With respect to stabilizing treatments and low ductility as evidence that Knerr teaches away, we agree that a person of ordinary skill in the art would have understood and weighed this tradeoff in benefits. Winner Int’l Royalty Corp. v. Wang, 202 F.3d 1340, 1349 n.8 (Fed. Cir. 2000) (“The fact that the motivating benefit comes at the expense of another benefit, . . . should not nullify its use as a basis to modify the disclosure of one reference with the teachings of another. Instead, the benefits, both lost and gained, should be weighed against one another.”). Therefore, we do not find that Kerr’s disclosure teaches away; it does not indicate that “the line of development flowing from the reference’s disclosure is unlikely to be productive of the result sought by the applicant.” In re Gurley, 27 F.3d 551, 553 (Fed. Cir. 1994). As set forth above, the Examiner finds that Knerr discloses several beneficial properties that are conferred to steel post-nitriding (Final Act. 4). Appellant argues that the combination of Williams and Knerr would not have rendered the instantly claimed nitrogen content obvious (Appeal Br. 10, 20; see also Reply Br. 11–14). In particular, Appellant argues that because “Knerr does not recite how much nitrogen should be added to a steel such as disclosed in Williams,” there is no recognition that nitrogen content is recognized as a result-effective variable (Appeal Br. 20). Appeal 2019-004035 Application 13/030,170 7 As the Examiner finds, however, because Knerr recognizes that the case depth (and thus nitrogen content . . .) of the steel may be controlled by conditions of nitriding[,] such as duration of nitriding time[,] and that the case depth affects the resultant hardness profile of the steel[,] . . . [i]t would require little more than routine experimentation by one of ordinary skill in the art to determine the optimal or workable ranges of case depth (and thus nitrogen content) to achieve a desired hardness profile for a given application of [Williams’] steel . . . in view of Knerr. Final Act. 5 (citing Knerr 390–91; Fig. 5). Appellant, moreover, does not allege any criticality with respect to the claimed nitrogen content between 0.01 and 0.075% (see Ans. 7). Therefore, the preponderance of the evidence favors the Examiner’s finding and conclusion that, in the absence of unexpected results, it would have required routine experimentation to determine the optimum value of a result effective variable, such as the claimed nitrogen content between 0.01 and 0.075%. Appellant argues that Williams’ steel, modified in view of Knerr, would not have possessed the instantly claimed properties because nitriding the steel of Williams would have changed the properties of Williams’ steel (Appeal Br. 11). Appellant argues that there is no teaching in either Knerr or Williams to select and then nitride Williams’ specific steel composition (id. at 20). We are not persuaded by these arguments as Appellant has not presented evidence other than attorney argument. As set forth above, the Examiner has provided a well-reasoned analysis of how and why the ordinarily skilled artisan would have reasonably expected that Williams’ modified thin cast steel strip made by a similar process would possess the Appeal 2019-004035 Application 13/030,170 8 yield and tensile strength and total elongation properties recited in the claim. On this record, Appellant has not met the burden of showing that the Examiner’s proposed thin cast steel strip does not possess the claimed strengths and elongation properties. In re Best, 562 F.2d 1252, 1255 (CCPA 1977) (explaining that “[w]here . . . the claimed and prior art products are identical or substantially identical, or are produced by identical or substantially identical processes, the PTO can require an applicant to prove that the prior art products do not necessarily or inherently possess the characteristics of his claimed product.”). We, furthermore, agree with the Examiner that one of ordinary skill in the art at the time of the invention would have gleaned from Knerr that appropriate nitriding conditions may be selected to maintain desirable strengths and elongation properties in Williams’ steel (see Ans. 7, 9–10).2 Accordingly, Appellant’s arguments do not persuasively address the Examiner’s reasoning, which supports the findings and conclusions in the stated rejection. Therefore, Appellant’s arguments are insufficient to convince us of reversible error in the Examiner’s rejection. 2 Appellant cites the Board’s decision in Appeal No. 2017-006822, pages 5– 6, to support the argument that the Examiner has not established a prima facie case of obviousness as Williams’ compositional ranges for nitrogen do not overlap the claimed range (Appeal Br. 13). However, Appellant’s reliance on Appeal No. 2017-006822 is unavailing as the sole reference relied upon by the Examiner in that case did not teach or suggest each and every limitation in the appealed claim. As set forth above and in the Answer, the Examiner relies on Knerr’s disclosure for teaching or suggesting the instantly claimed nitrogen content between 0.01 and 0.075% in Williams’ modified thin steel strip (see, e.g., Final Act. 4–5). Appeal 2019-004035 Application 13/030,170 9 Thus, based on a preponderance of evidence in this record, we sustain this rejection as to claim 15. 2. Claim 16–19 With regard to claims 16–19, the Examiner’s findings and conclusions regarding Williams and Knerr are located on page 6 of the Final Office Action. Representative claim 16 is set forth below: 16. The method of preparing nitrided thin cast steel strip as claimed in claim 15 where the steel strip as coiled has fine oxide particles of silicon and iron distributed through the steel microstructure having an average particle size less than 50 nanometers. Appeal Br. 32 (Claims App.). The Examiner finds that “Williams discloses the steel strip as coiled may have fine oxide particles of silicon and iron distributed through the steel microstructure having an average particle size less than 50 nanometers” (Final Act. 6 (citing Williams claim 116)). Appellant argues that “Knerr requires stabilizing treatment . . . and . . . stress relieving” of the steel prior to the nitriding step, but “[t]his simply cannot occur in the coiled steel of Williams” (Appeal Br. 22 (citing Knerr 394)). For the reasons set forth above and in the Answer, Appellant has not identified reversible error in the Examiner’s findings that Knerr’s stabilizing treatment and stress relieving steps are not mandatory (see Ans. 10). Rather, these steps are tradeoffs to be weighed by one of ordinary skill in the art in light of the benefits conferred by nitriding (see Winner Int’l Royalty Corp., 202 F.3d at 1349 n.8). Appeal 2019-004035 Application 13/030,170 10 Claims 17–19 depend on claim 16. Although Appellant offers separate arguments in support of dependent claims 17–19 (Appeal Br. 21– 24), we find that each of these arguments are substantially similar to Appellant’s unpersuasive arguments in support of claim 16. Thus, based on a preponderance of evidence in this record, we sustain this rejection as to claims 16–19. 3. Claims 21 and 22 With regard to claims 21 and 22, the Examiner’s findings and conclusions regarding Williams and Knerr are located on page 6 of the Final Office Action. Claims 21 and 22 are set forth below: 21. The method of preparing [a] nitrided thin cast steel strip as claimed in claim 15 where the total elongation is between 12.5 ± 0.5% and 14.2 ± 2.3%. 22. The method of preparing a nitrided thin cast steel strip as claimed in claim 16 where the total elongation is between 12.5 ± 0.5% and 14.2 ± 2.3%. Appeal Br. 33 (Claims App.). The Examiner finds that “Williams discloses the strip has a total elongation of at least 6% or 10% . . . overlapping the instantly claimed ranges” (Final Act. 6 (citing Williams Abstract)). Appellant argues that Knerr teaches away from nitriding aluminum- containing steel when good ductility or elongation is required (Appeal Br. 24). Appellant argues that the Examiner has not met the “burden of establishing [that] a nitrided version of the steel strip of Williams possesses Appeal 2019-004035 Application 13/030,170 11 the presently claimed elongation properties” recited in claims 21 and 22 (id.). For the reasons set forth above and in the Answer, Appellant has not identified reversible error in the Examiner’s findings that low ductility or poor elongation are tradeoffs to be weighed by one of ordinary skill in the art in light of the benefits conferred by nitriding (see Winner Int’l Royalty Corp., 202 F.3d at 1349 n.8; see Ans. 11). We, furthermore, agree with the Examiner that one of ordinary skill in the art at the time of the invention would have gleaned from Knerr that appropriate nitriding conditions may be selected to maintain desirable strengths and elongation properties in Williams’ steel (see Ans. 7, 9–10; see also Best, 562 F.2d at 1255). Thus, based on a preponderance of evidence in this record, we sustain this rejection as to claims 21 and 22. 4. Claims 23–26 With regard to claims 23–26, the Examiner’s findings and conclusions regarding Williams and Knerr are located on page 6 of the Final Office Action. Representative claim 23 is set forth below: 23. The method of preparing a nitrided thin cast steel strip as claimed in claim 15 where the steel product is a thin cast steel strip of less than 3 millimeters in thickness. Appeal Br. 33 (Claims App.). Appellant argues that Knerr’s Figure 9 illustrates that undesirable growth of the wall section of a hollow cylinder increases at an exponential rate below 5 mm (Reply Br. 9 (citing Knerr 395; Fig. 9)). According to Appellant, one of ordinary skill in the art would not have looked to Knerr’s wall section of a hollow cylinder and found any motivation to nitride Appeal 2019-004035 Application 13/030,170 12 Williams’ thin cast steel strip of 3 mm or less (Reply Br. 10; see also Appeal Br. 25–26). Appellant’s arguments are not persuasive because the exponential growth that Appellant refers to ranges from about 100 µm to about 240 µm (Knerr Fig. 9). This change in diameter amounts to an approximate additional 0.1–0.24 mm in thickness. We are not persuaded that such a relatively minor increase to Williams’ 3 mm strip teaches away from the Examiner’s proposed combination (see Gurley, 27 F.3d at 553). As the Examiner finds, “Williams discloses the strip may have a thickness of 1.1 mm . . . lying within the instantly claimed ranges” (Final Act. 6 (citing Williams Table 1)). Thus, based on a preponderance of evidence in this record, we sustain this rejection as to claims 23–26. 5. Claims 27–30 With regard to claims 27–30, the Examiner’s findings and conclusions regarding Williams and Knerr are located on pages 6–7 of the Final Office Action. Representative claim 30 is set forth below: 30. The method of preparing a nitrided thin cast steel strip as claimed in claim 15 where the steel product is nitrided for 1 hour. Appeal Br. 34 (Claims App.). Appeal 2019-004035 Application 13/030,170 13 The Examiner supports the rejection of these claims by finding that “Knerr recognizes that nitriding is a result effective variable which influences the case depth of the steel” (Final Act. 6). Appellant argues that “Knerr does not teach nitriding for any time less than 8 hours” and, thus, the Examiner’s “basis for optimization . . . is misapplied” (Appeal Br. 26 (citing Knerr Table 2)). Appellant’s arguments are not persuasive. For the reasons set forth above and in the Answer, the Examiner reasonably concluded that “[i]t would require little more than routine experimentation by one of ordinary skill in the art to determine the optimal or workable ranges of nitriding time to achieve a desired case depth for [Williams’] steel . . . in view of Knerr.” (Final Act. 6–7 (citing Knerr 390 (explicitly disclosing that “[c]ase depth and case hardness . . . vary . . . with the duration . . . of nitriding.”); Figs. 5, 7, 17, 31)). Thus, based on a preponderance of evidence in this record, we sustain this rejection as to claims 27–30. CONCLUSION In summary: Claims Rejected 35 U.S.C. § Reference(s)/Basis Affirmed Reversed 15–19, 21– 30 103(a) Williams, Knerr 15–19, 21–30 Appeal 2019-004035 Application 13/030,170 14 No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. § 1.136(a)(1)(iv). AFFIRMED Copy with citationCopy as parenthetical citation