WACKER CHEMIE AGDownload PDFPatent Trials and Appeals BoardJul 16, 20202019004817 (P.T.A.B. Jul. 16, 2020) Copy Citation UNITED STATES PATENT AND TRADEMARK OFFICE UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www.uspto.gov APPLICATION NO. FILING DATE FIRST NAMED INVENTOR ATTORNEY DOCKET NO. CONFIRMATION NO. 14/889,347 11/05/2015 Simon PEDRON WASN0229PUSA 6544 22045 7590 07/16/2020 Brooks Kushman 1000 Town Center 22nd Floor Southfield, MI 48075 EXAMINER LEUNG, JENNIFER A ART UNIT PAPER NUMBER 1774 NOTIFICATION DATE DELIVERY MODE 07/16/2020 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address(es): docketing@brookskushman.com kdilucia@brookskushman.com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE ____________ BEFORE THE PATENT TRIAL AND APPEAL BOARD ____________ Ex parte SIMON PEDRON and GERHARD FORSTPOINTNER ____________ Appeal 2019-004817 Application 14/889,347 Technology Center 1700 ____________ Before CHRISTOPHER C. KENNEDY, DEBRA L. DENNETT, and JANE E. INGLESE Administrative Patent Judges. DENNETT, Administrative Patent Judge. DECISION ON APPEAL1 STATEMENT OF THE CASE Pursuant to 35 U.S.C. § 134(a), Appellant2 appeals from the Examiner’s decision to reject claims 20–35 of Application 14/889,347, which constitute all the claims pending in this application. We have jurisdiction under 35 U.S.C. § 6(b). 1 In our Decision, we refer to the Specification (“Spec.”) of Application No. 14/889,347 filed Nov. 5, 2015; the Final Office Action dated July 6, 2018 (“Final Act.”); the Advisory Action dated Oct. 9, 2018 (“Adv. Act.); the Appeal Brief filed Feb. 4, 2019 (“Appeal Br.”); the Examiner’s Answer dated Apr. 2, 2019 (“Ans.”); and the Reply Brief filed May 30, 2019 (“Reply Br.”). 2 We use the word “Appellant” to refer to “applicant” as defined in 37 C.F.R. § 1.42. Appellant identifies the real party in interest as Wacker Chemie AG. Appeal Br. 1. Appeal 2019-004817 Application 14/889,347 2 For the reasons set forth below, we REVERSE. The subject matter of the invention relates to fluidized bed reactors and a method for producing granular polysilicon. Spec. 1, ll. 5–6. Polysilicon granules produced in a fluidized bed reactor have bulk material properties and can be used directly as a raw material. Spec. 1, ll. 14–16, 19. According to the Specification, pressure conditions varying with time and locality in fluidized beds cause fluctuations of the gas mass streams that are fed, leading to instabilities in the chemical process and in the temperature distribution. Spec. 3, ll. 21–28. The openings in a conventional gas distributor plate via which all gas mass streams can be fed do not have a sufficient pressure drop for distributing the respective mass streams in a uniform manner with respect to time and locality. Spec. 3, ll. 34–4, ll. 2. Applicant accomplishes a uniform distribution of gas mass streams fed to a fluidized bed over time and all inlet openings via Laval nozzles, preferably operated at a supercritical pressure ratio. Spec. 7, ll. 32–36. A Laval nozzle is a flow element having an initially convergent and subsequently divergent cross section, wherein the transition from one part to the other part proceeds gradually. Spec. 5, ll. 14–17. Claim 20, reproduced below from the Claims Appendix of the Appeal Brief, illustrates the claimed subject matter: 20. In a fluidized bed reactor for producing granular polysilicon, having an inner reactor tube for a fluidized bed of granular polysilicon, the inner reactor tube having a reactor base with openings for entry of fluidizing gas and reaction gas, a heater for heating the fluidized bed of polysilicon, a silicon particle feed, an opening above the fluidized bed for removing offgas, and an opening in the inner reactor tube for removing a granular silicon product, the improvement comprising: Appeal 2019-004817 Application 14/889,347 3 at least two reaction gas openings in the reactor base, each of the at least two reaction gas openings fed by a Laval nozzle positioned outside of the reactor tube and upstream of the at least two reaction gas openings, the Laval nozzle suitable for expanding supercritically at least one mass stream of reaction gas, the at least two reaction gas openings comprising a gas distributor, a valve, a hole in the reactor base, or a nozzle, wherein the intake pressure of the Laval nozzle is controlled by gas quantity regulation. REFERENCES The Examiner relies on the following references in rejecting the claims: Name Reference Date Schmit US 5,489,166 Feb. 6, 1996 Hertlein et al. (“Hertlein”) US 2008/0241046 A1 Oct. 2, 2008 REJECTIONS The Examiner maintains the rejection of claims 20–35 under 35 U.S.C. § 1033 as obvious over Hertlein in view of Schmit. Final Act. 3–11. DISCUSSION Having considered the respective positions advanced by the Examiner and Appellant in light of the record before us, we reverse the Examiner’s rejections based on arguments presented by Appellant. With respect to all of the claims, the Examiner finds that Hertlein discloses the fluidized bed reactor and related limitations recited in claim 20. 3 Because this application was filed after the March 16, 2013, effective date of the America Invents Act, we refer to the AIA version of the statute. Appeal 2019-004817 Application 14/889,347 4 Final Act. 3–5, 8–11. The Examiner finds that Hertlein does not disclose that each of the at least two reaction gas openings is fed by a Laval nozzle positioned outside the reactor tube and upstream of the reaction gas openings. Id. at 4. The Examiner finds that Schmit teaches a Laval nozzle situated upstream of openings. Id. at 5. The Examiner determines It would have been obvious to one of ordinary skill in the art before the effective filing date of the claimed invention to provide a Laval nozzle upstream of each of the [at] least two reaction gas openings in the reactor of Hertlein et al., on the basis of suitability for the intended use thereof, because the at least two reaction gas openings could then be supplied with reaction gas by a supersonic flow through the Laval nozzle, which would make it possible to fix the gas flow rate at a defined value, as taught by Schmit. Id.; see also Ans. 11. Hertlein discloses a fluidized bed reactor for producing granular polysilicon in which a gas or gas mixture containing silicon is fed through the fluidized bed, depositing elementary silicon on all hot surfaces to grow silicon particles. Hertlein ¶¶ 1, 4. Hertlein teaches a problem in such devices is deposition of silicon on the hot reactor surfaces such as the reactor walls, resulting in thermo-mechanical loading of the reactor and reactor outages. Id. ¶ 4. Hertlein teaches use of a fluidizing gas, a reaction gas comprising a high proportion of a gaseous silicon compound, as well as a “wall-shielding” gas comprising 99.5 to 95 mol.% hydrogen and 0.5 to 5 mol.% gaseous silicon compound. Id. ¶¶ 20, 24. Hertlein’s wall-shielding gas is present on the surface of the reactor, provided in the region of the reactor surfaces. Id. Schmit, which relates to removing granular or pulverulent solid residues from a gas purification installation, describes creating overpressure Appeal 2019-004817 Application 14/889,347 5 in a closed vessel with two Laval nozzles, one between the gas supply source and fluidization surface and the other in the gas removal pipeline. Schmit col. 1, ll. 7–11; col. 4, ll. 33–37. Schmit teaches the fluidization device is supplied with gas preferably by a supersonic flow through a Laval nozzle. Id. col. 7, ll.7–10. During examination, the Examiner bears the initial burden of establishing a prima facie case of obviousness. In re Oetiker, 977 F.2d 1443, 1445 (Fed. Cir. 1992). “[R]ejections on obviousness grounds cannot be sustained by mere conclusory statements; instead, there must be some articulated reasoning with some rational underpinning to support the legal conclusion of obviousness.” KSR Int’l v. Teleflex Inc., 550 U.S. 398, 418 (2007) (quoting In re Kahn, 441 F.3d 977, 988 (Fed. Cir. 2006)); see also, Ball Aerosol and Specialty Container, Inc. v. Ltd. Brands, Inc., 555 F.3d 984, 993 (Fed. Cir. 2009) (“[T]he analysis that ‘should be made explicit’ refers not to the teachings in the prior art of a motivation to combine, but to the court’s analysis.”). “Obviousness requires more than a mere showing that the prior art includes separate references covering each separate limitation in a claim under examination.” Unigene Labs., Inc. v. Apotex, Inc., 655 F.3d 1352, 1360 (Fed. Cir. 2011). “Rather, obviousness requires the additional showing that a person of ordinary skill at the time of the invention would have selected and combined those prior art elements in the normal course of research and development to yield the claimed invention.” Id. While the individual elements of the claims may appear in the individual references, we discern no motivation to combine the references in the manner suggested by the Examiner. Appeal 2019-004817 Application 14/889,347 6 Specifically, the Examiner has not convincingly explained why one skilled in the art would modify Hertlein’s device, which minimizes wall deposition of silicon by flow of a wall-shielding gas that blankets the walls, by employing Schmit’s Laval nozzle to inject reaction gas at supersonic flow. See Appeal Br. 5. As Appellant explains, Hertlein desires inhomogeneous distribution of gas in the reactor, so that gas along the walls of the reactor is 99.5 to 95 mol.% hydrogen, and 0.5 to 5 mol.% gaseous silicon compound. Reply Br. 8–9; see also Hertlein ¶ 12. The gas in the reaction space, in contrast, must have a much higher silicon content in order to deposit silicon onto silicon seeds. Hertlein ¶ 20. The Examiner fails to explain why one of ordinary skill in the art would provide reaction gas to Hertlein at supersonic flow via Laval nozzles, given that the “predictable result” would be homogenization of gases in the reactor, defeating Hertlein’s intended purpose. See DePuy Spine, Inc. v. Medtronic Sofamor Danek, Inc., 567 F.3d 1314, 1326 (Fed. Cir. 2009) (“[T]he ‘predictable result’ discussed in KSR refers not only to the expectation that prior art elements are capable of being physically combined, but also that the combination would have worked for its intended purpose.”). We are persuaded that the Examiner has not provided sufficient reasons to support the position that Hertlein and Schmit may be combined in a manner that would render the claimed subject matter obvious. We do not sustain the rejection of claims 20–35 as obvious over Hertlein in view of Schmit. DECISION SUMMARY In summary: Appeal 2019-004817 Application 14/889,347 7 Claims Rejected 35 U.S.C. § Reference(s)/Basis Affirmed Reversed 20–35 103 Hertlein, Schmit 20–35 REVERSED Copy with citationCopy as parenthetical citation