SAUDI BASIC INDUSTRIES CORPORATIONDownload PDFPatent Trials and Appeals BoardOct 22, 202015689452 - (D) (P.T.A.B. Oct. 22, 2020) Copy Citation UNITED STATES PATENT AND TRADEMARK OFFICE UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www.uspto.gov APPLICATION NO. FILING DATE FIRST NAMED INVENTOR ATTORNEY DOCKET NO. CONFIRMATION NO. 15/689,452 08/29/2017 Ashim Kumar Ghosh 12CHEM0044-US-CNT 7293 102091 7590 10/22/2020 Cantor Colburn LLP - SABIC Americas 20 Church Street Hartford, CT 06103 EXAMINER CHONG, JASON Y ART UNIT PAPER NUMBER 1772 NOTIFICATION DATE DELIVERY MODE 10/22/2020 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address(es): usptopatentmail@cantorcolburn.com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte ASHIM KUMAR GHOSH, MOHAMED ELBACCOUCH, MOHAMMAD SHAFIEI, and MURALI GOPALAKRISHNAN Appeal 2019-005578 Application 15/689,452 Technology Center 1700 Before BRIAN D. RANGE, DEBRA L. DENNETT, and LILAN REN, Administrative Patent Judges. DENNETT, Administrative Patent Judge. DECISION ON APPEAL1 Pursuant to 35 U.S.C. § 134(a), Appellant2 appeals from the Examiner’s decision to reject claims 1–11. See Final Act. 1. We have jurisdiction under 35 U.S.C. § 6(b). 1 In our Decision, we refer to the Specification (“Spec.”) of Application No. 15/689,452 filed August 29, 2017 (“the ’452 App.”); the Final Office Action dated September 10, 2018 (“Final Act.”); the Appeal Brief filed February 11, 2019 (“Appeal Br.”); the Examiner’s Answer dated May 16, 2019 (“Ans.”); and the Reply Brief filed July 16, 2019 (“Reply Br.”). 2 We use the word “Appellant” to refer to “applicant” as defined in 37 C.F.R. § 1.42. Appellant identifies the real party in interest as SAUDI BASIC INDUSTRIES CORPORATION. Appeal Br. 2. Appeal 2019-005578 Application 15/689,452 2 We AFFIRM IN PART. STATEMENT OF THE CASE The ’452 Application relates to toluene methylation with transalkylation of heavy aromatics for preparing xylene products. Spec. ¶ 1. Para-xylene (p-xylene) is said to be particularly valuable as a precursor to forming polyester fibers and resins. Id. ¶ 3. According to the ’452 Application, toluene methylation used in laboratory studies to produce mixed xylene (o-, m-, and p-xylene) has technical hurdles and results in less valuable C9+ aromatics byproducts, making the previously known process of toluene methylation commercially unattractive. Id. ¶ 5. Claim 1 is representative of the ’452 Application’s claims and is reproduced below from the Claims Appendix of the Appeal Brief. 1. A method of producing a purified mixed xylene comprising: introducing toluene and methanol to an alkylation reactor; reacting the toluene and the methanol in the alkylation reactor to form a hydrocarbon stream comprising a first mixed xylene, wherein the alkylation reactor comprises an alkylation catalyst; separating the hydrocarbon stream into a toluene stream and a separated C8+ stream; introducing the toluene stream to a transalkylation reactor with a transalkylation catalyst to produce a transalkylated stream comprising a second mixed xylene; adding the transalkylated stream to the hydrocarbon stream; and separating a C8 product stream comprising the purified mixed xylene from the separated C8+ stream. Appeal 2019-005578 Application 15/689,452 3 REFERENCES The Examiner relies on the following prior art: Name Reference Date Ghosh et al. (“Ghosh”) US 8,062,987 B2 Nov. 22, 2011 Haizmann et al. (“Haizmann”) US 2012/0271071 A1 Oct. 25, 2012 Ding et al. (“Ding”) US 2013/0267746 A1 Oct. 10, 2013 REJECTIONS The Examiner rejects claims under 35 U.S.C. § 1033 as follows: (1) claims 1 and 10 as unpatentable over Ding; (2) claims 2–7 and 11 as unpatentable over Ding in view of Ghosh; and (3) claims 8 and 9 as unpatentable over Ding in view of Haizmann. Final Act. 7–14. OPINION We review the appealed rejections for error based upon the issues identified by Appellant and in light of the arguments and evidence produced thereon. Ex parte Frye, 94 USPQ2d 1072, 1075 (BPAI 2010) (precedential), (cited with approval in In re Jung, 637 F.3d 1356, 1365 (Fed. Cir. 2011)) (“[I]t has long been the Board’s practice to require an applicant to identify the alleged error in the [E]xaminer’s rejections.”). After considering the evidence presented in this Appeal and each of Appellant’s arguments, Appellant persuades us of reversible error in the Examiner’s rejection of claims 4–7, but fails to persuade us of reversible error in the rejections of claims 1–3, and 8–11. 3 Because this application was filed after the March 16, 2013, effective date of the America Invents Act, we refer to the AIA version of the statute. Appeal 2019-005578 Application 15/689,452 4 Rejection of claims 1 and 10 as obvious over Ding Regarding claim 1, the Examiner finds that Ding teaches the limitations of claim 1 except for explicitly disclosing the step of adding the transalkylated stream to the hydrocarbon stream. Final Act. 8. The Examiner finds that Ding teaches subjecting a methylation production stream (i.e., the claimed hydrocarbon stream) and a transalkylated product stream to the same separation step in which toluene is separated from the remaining C8+ aromatics and sent to the transalkylation step. Id. (citing Ding ¶ 25). The Examiner finds that Ding discloses separation and recovery of benzene and toluene from the methylation effluent and the transalkylation effluent, and that the recovered benzene and toluene can be sent to the transalkylation step and the methylation step. Ans. 10 (citing Ding ¶¶ 24– 25). The Examiner finds that the claimed invention differs from Ding only in that it requires combining the methylation effluent with the transalkylation effluent prior to the toluene separation column. Id. at 13. The Examiner reasons that one of ordinary skill in the art would reasonably expect the same result of the separation step, whether the methylation product stream and transalkylation stream enter the separation section separately or in a combined stream, thus claim 1 is not patentably distinguishable from Ding’s disclosure. Final Act. 8–9. Appellant argues Ding merely discloses the benzene and toluene from the reactor effluent are subjected to a methylation step, which produces a mixture of xylenes, and, in a transalkylation step, C9+ aromatics from the reactor effluent or those derived from the methylation step is subjected to transalkylation to yield a mixture of xylenes. Appeal 2019-005578 Application 15/689,452 5 Appeal Br. 4. Appellant contends that, based on Ding’s disclosure that “effluents from the methylation step and transalkylation step share the same separation step,” the skilled artisan “might at best consider directing the effluents from the methylation step and transalkylation step [to] share the same separation step in order to separate out their products.” Id. Appellant provides an annotated version of Ding’s FIG. 4 with an asterisk added to show “where it is believed that an artisan presented with Ding might at best consider a shared separation step in order to separate their xylene from the TM (methylation) and TA (transalkylation) steps from the benzene.” Id. at 5. Appellant’s annotated figure is reproduced below with the asterisk added by Appellant circled in red: Ding FIG. 4 shows a process for maximizing para-xylene production by the integration of the methylation and transalkylation steps in accordance with an embodiment of Ding’s invention. Ding. ¶ 11. TA represents transalkylation, TM represent transmethylation, T represents toluene, B represent benzene, X represents mixed xylene, PX represents para-xylene, and C9A+ represents C9+ aromatics. Ding ¶¶ 15, 22. Appeal 2019-005578 Application 15/689,452 6 Appellant argues that subjecting effluents from a methylation step and a transalkylation step to the same separation step does not meet the requirements of claim 1. Appeal Br. 5. More specifically, Appellant urges that claim 1 requires a portion of the hydrocarbon stream is directed to the transalkylation reactor and a portion of the transalkylated stream is also redirected/recycled back into the transalkylation reactor. Id. According to Appellant, the application explains that the transalkylated stream can be combined with the hydrocarbon stream and can be added to the toluene separation column to introduce more xylene into the column. Id. Appellant acknowledges that claim 1 does not require combination of the hydrocarbon stream and the transalkylated stream prior to being added to a separation unit. Reply Br. 4. Appellant contends that the inventive feature of adding the transalkylated stream comprising the second mixed xylene to the hydrocarbon stream and then adding the toluene separated from the transalkylated stream back into the transalkylation reactor is not disclosed or suggested by Ding. Id. at 4–5. Appellant argues that there is no motivation in Ding to add these steps, thus no reasonable expectation of success without consideration of the ’452 Application—which is barred by hindsight. Appeal Br. 6. Appellant’s position is not persuasive of reversible error. Ding teaches that at least a portion of the methylated aromatic hydrocarbon-enriched fraction created in the methylation step is subjected to a transalkylation step to form paraxylene. Ding ¶ 15. Ding also teaches that, in certain embodiments, a portion of benzene and toluene from the methylation step is transferred to the transalkylation step. Id. ¶ 24. For this to occur, as the Examiner explains, the methylated aromatic hydrocarbon- Appeal 2019-005578 Application 15/689,452 7 enriched fraction of Ding must be separated into a benzene and toluene stream and a C8+ fraction. Ans. 10. Ding teaches that the effluents from the methylation step and transalkylation step share the same separation section. Id. ¶ 25. Thus, both a hydrocarbon stream (the methylated aromatic hydrocarbon-enriched fraction created in the methylation step) and a transalkylated stream are fed to the same separation column. Claim 1 does not require the hydrocarbon stream and the transalkylated stream to be combined prior to being added to a separation unit. See Reply Br. 4. Ding teaches that benzene and toluene are recovered and recycled from the transalkylation step. See Ding FIG. 1 (indicating the C8+ streams of methylation and transalkylation are combined and C6, C7 are separated); FIGs. 4, 5 (indicating that all benzene and toluene are recycled). The benzene and toluene, either mixed or separated, are transferred to the methylation step and the transalkylation step. Id. ¶ 25. Contrary to Appellant’s position (see Reply Br. 4–5), Ding thus discloses adding the transalkylated stream to the hydrocarbon stream and then adding the toluene separated from the transalkylated stream back into the transalkylation reactor. For the above reasons, Ding at least renders claim 1 obvious. Appellant presents argument referring to claim 10, but the arguments address claim 9 instead. See Ans. 14–15; Reply Br. 5. Thus, Appellant offers no separate argument for patentability of claim 10. We sustain the rejection of claim 10 for the reasons we provide above for claim 1. Rejection of claims 2–7 and 11 as obvious over Ding in view of Ghosh Claims 2–7 and 11 depend directly or indirectly from claim 1. Appeal Br. 11–12 (Claims App.). Appeal 2019-005578 Application 15/689,452 8 Claims 2, 3, and 11 Claim 2 requires that the alkylation catalyst comprises a phosphorus containing, medium pore, pentasil zeolite having a silica/alumina ratio of greater than or equal to 200. Id. at 11. Claims 3 and 11 depend from claim 2. Id. Claims 3 and 11 require that phosphorus is present in an amount of 0.01 (claim 3) or 0.07 (claim 11) to 0.15 g per gram of zeolite. Id. at 11, 12. With regard to claims 2, 3, and 11, the Examiner finds that Ding discloses methylation (alkylation) in the presence of a zeolite catalyst such as ZSM-5. Final Act. 9 (citing Ding ¶ 16). The Examiner relies on Ghosh as teaching a phosphorus-modified ZSM-5 zeolite catalyst that is pretreated with water to be used in alkylation of toluene with methanol, and that ZSM- 5 has the claimed properties. Id. at 9. The Examiner finds that Ghosh discloses increasing para-xylene selectivity by modifying ZSM-5 zeolite with phosphorus. Id. at 9–10. The Examiner finds that Ghosh teaches the phosphorous-treated ZSM- 5 catalyst may contain 0.0001 to 0.15 g phosphorous per gram of zeolite (claim 3) and about 0.007 to about 0.12 g phosphorus per gram of zeolite (clam 11), which ranges overlap the claimed ranges. Final Act. 10, 12. The Examiner concludes that it would have been obvious to one of ordinary skill in the art at the time of the filing to modify Ding by treating the ZSM-5 zeolite catalyst with phosphorus because such treatment will increase the para-selectivity properties of the zeolite and improve para- xylene selectivity. Id. at 10. The Examiner further concludes that the modification would involve substitution of a known prior art methylation catalyst for another known prior art methylation catalyst to improve a known Appeal 2019-005578 Application 15/689,452 9 process for the methylation of toluene with methanol to obtain predictable results. Id. In the Answer, the Examiner explains that Ding discloses a broad range of zeolite frameworks that may be used as a catalyst in the methylation step but does not provide specific details on the catalyst composition or the preparation steps of such a catalyst. Ans. 15. According to the Examiner, one skilled in the art, reading the disclosure of Ding, would look to other prior art for information on workable zeolite catalysts and their preparation in accordance with the guidance of Ding, and Ghosh exemplifies such a known methylation catalyst having ZSM-5 framework zeolite. Id. The Examiner also finds that Ding’s figures do not identify which catalyst and process conditions (e.g. temperature, pressure, feed rate) were employed and, therefore, do not provide meaningful information on the effect of the catalysts suggested by Ding. Id. at 15–16. Appellant argues that there is no motivation for one of ordinary skill in the art to replace Ding’s catalyst with Ghosh’s because Ding achieves a high amount of xylene in its product streams. Appeal Br. 8; Reply Br. 6. Appellant contends that Ding discloses several specific examples of catalysts, thus there is no need for one of ordinary skill to rely on Ghosh to glean catalyst details. Reply Br. 6. Appellant urges that catalysis is notoriously unpredictable as a further reason not to modify Ding with Ghosh. Id. at 6–7. Ding discloses a group of possible catalysts for alkylation, including ZSM-5. Ding ¶¶ 16, 18. One of ordinary skill in the art in possession of Ding would reasonably look to other art (such as Ghosh) for more information on specific catalysts—a reason that would have prompted a Appeal 2019-005578 Application 15/689,452 10 person of ordinary skill in the relevant field to combine the elements in the way the claimed new invention does. See KSR Int’l Co. v. Teleflex Inc., 550 U.S. 398, 418 (2007). “When there is a design need or market pressure to solve a problem and there are a finite number of identified, predictable solutions, a person of ordinary skill has good reason to pursue the known options within his or her technical grasp.” Id. at 421. Here, a design need existed to choose a specific catalyst for use in Ding’s method. The choice of Ghosh’s ZSM-5 catalyst is the product of ordinary skill and common sense. See id. Appellant’s contention that catalysis is notoriously unpredictable does not alter our opinion. See Reply Br. 6–7. “Our precedent, however, does not require that the motivation be the best option, only that it be a suitable option from which the prior art did not teach away.” Par Pharm., Inc. v. TWI Pharm., Inc., 773 F.3d 1186, 1197–98 (Fed. Cir. 2014). “[A] reasonable expectation of success, not absolute predictability” supports a conclusion of obviousness. In re Longi, 759 F.2d 887, 897 (Fed. Cir. 1985). Ding discloses use of, inter alia, a ZSM-5 zeolite catalyst, and Ghosh discloses details of a ZSM-5 zeolite catalyst. Ding ¶ 16; Ghosh generally. The Examiner’s finding that a skilled artisan would have a reasonable expectation of success in substituting Ghosh’s ZSM-5 catalyst in Ding’s method is therefore supported by the record before us. Evidence of a motivation to combine prior art references “may flow from the prior art references themselves, the knowledge of one of ordinary skill in the art, or, in some cases, from the nature of the problem to be solved.” Brown & Williamson Tobacco Corp. v. Philip Morris Inc., 229 F.3d 1120, 1125 (Fed. Cir. 2000). Although catalysis may have some Appeal 2019-005578 Application 15/689,452 11 unpredictability, “a given course of action often has simultaneous advantages and disadvantages, and this does not necessarily obviate motivation to combine.” Medichem, S.A. v. Rolabo, S.L., 437 Fed. 1157, 1165 (Fed. Cir. 2006) (citation omitted). One of ordinary skill in the art would have known that selecting a specific catalyst involved some unpredictability, but would reasonably turn to Ghosh, given its disclosure of providing para-selective properties to the ZSM-5 zeolite catalyst by treating it with phosphorus-containing compounds. See Ghosh 3:15–18. The fact that the motivating benefit (improved para-selective properties) comes at the expense of choosing a different catalyst from those disclosed generally in Ding should not nullify its use as a basis to modify the disclosure of Ding with the teachings of Ghosh. Winner Int’l Royalty Corp. v. Wang, 202 F.3d 1340, 1349 at n. 8 (Fed. Cir. 2000). “Instead, the benefits, both lost and gained, should be weighed against one another.” Id. The Examiner articulated reasoning has the requisite rational underpinning to support the legal conclusion of obviousness of claims 2, 3, and 11. See In re Kahn, 441 F.3d 977, 9888 (Fed. Cir. 2006). Claims 4–7 Claim 4 requires conversion of greater than or equal to 0.05 g of C9+ aromatics per gram of toluene in the alkylation reactor. Id. at 11. Claim 5 requires the purified mixed xylene comprises greater than or equal to 85 wt% p-xylene based on the total amount of mixed xylene. Id. Claims 6 and 7 require the selectivity of the alkylation catalyst for para-xylene to be greater than or equal to 80 mol% (claim 6) or less than or equal to 75 mol% (claim 7). Id. Appeal 2019-005578 Application 15/689,452 12 With regard to claims 4–7, the Examiner finds that Ding does not explicitly disclose the claimed limitations regarding the production of C9+ in the alkylation reactor (claim 4), the ratio of p-xylene based on the total xylenes produced (claim 5), or catalyst selectivities for p-xylene (claims 6 and 7). Id. However, the Examiner finds that Ghosh teaches that a ZSM-5 zeolite catalyst that is modified with phosphorus allows for increased para- xylene selectivity, and therefore it would have been obvious to one skilled in the art to modify Ding by using a phosphorus-modified ZSM-5 catalyst, as discussed above. Id. Specifically, the Examiner finds that Ding in view of Ghosh discloses a similar process of alkylation of toluene with methanol as the method recited in claim 1 under similar conditions including catalyst (compare Ghosh 3:16–4:27 with Spec. ¶¶ 34–37), temperature (compare Ding ¶ 16 with Spec. ¶ 19), and pressure (compare Ding ¶ 16 with Spec. Table 4). Id. The Examiner finds that one of ordinary skill in the art would have reasonably expected the process of Ding in view of Ghosh to function the same as the process of alkylation recited in claims 4 and 5 and produce the required results, absent evidence to the contrary. Id. The Examiner finds that Ghosh is silent on the selectivity for para- xylene, but discloses a similar catalyst to that claimed. Id. at 11–12. The Examiner finds that Ghosh’s catalyst is reasonably expected to have a selectivity range similar to that claimed in claims 6 and 7. Id. at 12. Appellant argues that neither Ding nor Ghosh specifically disclose the additional limitations in claims 4–7. Appeal Br. 8; Reply Br. 7. Appellant contends that neither reference suggests the high para-xylene selectivities of claims 6–8. Id. Instead, Appellant argues, the references merely disclose an Appeal 2019-005578 Application 15/689,452 13 amount of xylene produced (Ding) and the percentage toluene conversion (Ghosh). Id. Where a product is produced by a claimed process and prior art products are produced by identical or substantially identical processes, the PTO can require an applicant to prove that the prior art products do not necessarily or inherently possess the characteristics of his claimed product. In re Best, 562 F.2d 1252, 1256 (CCPA 1977). This is the doctrine that the Examiner invokes in determining that one of ordinary skill in the art would reasonably expect the process disclosed by Ding in view of Ghosh to function the same as the alkylation process in claims 4 and 5 and produce the claimed results. Here, however, the Examiner finds that the processes are “similar,” not identical or substantially identical. See Final Act. 11. In addition, the use of inherency, a doctrine originally rooted in anticipation, must be carefully circumscribed in the context of obviousness. See, e.g., In re Rijckaert, 9 F.3d 1531, 1533–34 (Fed. Cir. 1993) (“The mere fact that a certain thing may result from a given set of circumstances is not sufficient [to establish inherency].” (internal quotation omitted)). “[T]he inherency of an advantage and its obviousness are entirely different questions. . . . Obviousness cannot be predicated on what is unknown.” In re Shetty, 566 F.2d 81, 86 (CCPA 1977) (quoting In re Spormann, 363 F.2d 444, 448 (1966)). Our reviewing court and its predecessor established that the concept of inherency must be limited when applied to obviousness, and is present only when the limitation at issue is necessarily present or the “natural result” of the combination of prior art elements. PAR Pharm., Inc. v. TWi Pharms., Appeal 2019-005578 Application 15/689,452 14 Inc., 773 F.3d 1187, 1195–96 (Fed. Cir. 2014) (emphasis added). On the record before us, we cannot say that the limitations of claims 4–7 are necessarily present or the natural result of the combination of Ding and Gosh. Therefore, we do not sustain the rejection of claims 4–7. Rejection of claims 8 and 9 as obvious over Ding in view of Haizmann Claim 8 depends from claim 1 and further requires separating the C8+ stream in a xylene column into the C8 product stream and a separated C9+ stream. See Appeal Br. 11 (Claims App.). Claim 9 depends from claim 8 and further requires separating the separated C9+ stream in a C9 separation column into a C9 stream and a C10+ stream; and introducing the C9 stream to the transalkylation reactor. Id. at 12. Regarding claim 8, the Examiner finds that Ding discloses separating a C8+ stream into a C8 product stream and a C9+ stream. Id. at 13. The Examiner finds that Ding does not explicitly disclose that the separation section comprises a xylene column. Final Act. 12. The Examiner relies on Haizmann for teaching use of a xylene column to separate a fraction of reformate to produce a stream comprising C8 aromatic hydrocarbons and a different stream comprising C9, C10 and heavier aromatic hydrocarbons. Id. (citing Haizmann ¶¶ 9, 18, 32). The Examiner views this disclosure as teaching “separating a C8+ stream in a xylene column into the C8 product stream and a separated C9+ stream.” Id. The Examiner concludes that it would have been obvious to one of ordinary skill in the art to modify Ding by separating the C8+ stream produced from the methylation and transalkylation steps into a C8 product stream and a C9+ stream by using a xylene column, as the method involves Appeal 2019-005578 Application 15/689,452 15 application of a known technique to operate a known process to yield predictable results. Id. at 13. Appellant argues only that Haizmann fails to cure the deficiency of Ding identified in the discussion of claim 1. Appeal Br. 9. Because we find no error in the Examiner’s rejection of claim 1 over Ding, we sustain the rejection of claim 8 over Ding in view of Haizmann. Regarding claim 9, the Examiner finds that Ding discloses sending a C9+ stream to the transalkylation step to produce C8 aromatics, the reference does not explicitly disclose separating the C9+ stream into a C9 stream and a C10+ stream and introducing the C9 stream to the transalkylation reactor. Final Act. 13. The Examiner relies on Haizmann for teaching separating the C9+ stream to produce a trimethylbenzene-enriched fraction (a C9 stream) and a C10 aromatic hydrocarbon-enriched fraction by using a distillation column, which the Examiner identifies as a C9 separation column. Id. (citing Haizmann ¶¶ 32, 38, Fig. 1). The Examiner finds that Haizmann discloses sending the separated trimethylbenzene-enriched fraction to the transalkylation step to produce C8 aromatics. Id. (citing Haizmann ¶ 33). The Examiner cites Haizmann as teaching that transalkylation processes are significantly more selective for transalkylating methyl group substituents of an aromatic ring, compared to higher alkyl group substituents (e.g. ethyl, propyl, and butyl), because higher alkyl groups are much more susceptible, under transalkylation conditions, to being non-selectively dealkylated or removed from the aromatic ring, thereby forming benzene and light alkene hydrocarbons. Id. at 13–14 (citing Haizmann ¶¶ 9–11). The Examiner finds that Haizmann teaches that the use of a methylated aromatic hydrocarbon- Appeal 2019-005578 Application 15/689,452 16 enriched fraction in the transalkylation is advantageous because it increases production of para-xylene. Id. at 14 (citing Haizmann ¶ 27). The Examiner determines it would have been obvious to separate in a C9 separation column a trimethylbenzene-enriched fraction (i.e. a C9 stream) from the C9+ stream obtained from the xylene column, and send the separated trimethylbenzene-enriched fraction to the transalkylation step, as taught by Haizmann, because (i) Ding, in view of Haizmann, teaches obtaining a C9+ stream which is then used as a feed to a transalkylation to produce C8 aromatics, (ii) Haizmann further teaches separating trimethylbenzene from a C9+ stream and sending it to transalkylation increases transalkylation performance and paraxylene selectivity, and (iii) this involves application of a known technique of preparing a transalkylation feed to improve a known transalkylation process to yield predictable results. Id. Appellant argues that because Ding is completely silent to separating a C9+ stream into a C9 stream and a C10+ stream, one skilled in the art would have no motivation or suggestion to do so based on Ding’s disclosure. Appeal Br. 7; Reply Br. 5. Appellant cites to Ding’s disclosure that the invention is directed to a process “for producing xylenes by using benzene, toluene and C9 plus aromatics” and claim 1 of Ding recites “a transalkylation step that converts the C9 plus aromatics from the methylation step to C8 aromatics. Reply Br. 5. The Examiner relies on Haizmann, not Ding, for separating a C9+ stream into a C9 stream and a C10+ stream. Final Act. 13. Therefore, Appellant fails to address the Examiner’s rejection of claim 9 over Ding combined with Haizmann persuasively. Appeal 2019-005578 Application 15/689,452 17 We sustain the rejection of claim 9 as obvious over Ding in view of Haizmann. CONCLUSION The Examiner’s decision to reject claims 1–3 and 8–11 is AFFIRMED and claims 4–7 is REVERSED. DECISION SUMMARY In summary: Claim(s) Rejected 35 U.S.C. § Reference(s)/Basis Affirmed Reversed 1, 10 103 Ding 1, 10 2–7, 11 103 Ding, Ghosh 2, 3, 11 4–7 8, 9 103 Ding, Haizmann 8, 9 Overall Outcome 1–3, 8–11 4–7 TIME PERIOD FOR RESPONSE No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. § 1.136(a). See 37 C.F.R. § 1.136(a)(1)(iv). AFFIRMED IN PART Copy with citationCopy as parenthetical citation