Ex Parte Wusatowska-Sarnek et alDownload PDFPatent Trial and Appeal BoardAug 21, 201813563216 (P.T.A.B. Aug. 21, 2018) Copy Citation UNITED STA TES p A TENT AND TRADEMARK OFFICE APPLICATION NO. FILING DATE FIRST NAMED INVENTOR 13/563,216 07/31/2012 Agnieszka M. Wusatowska-Sarnek 54549 7590 08/23/2018 CARLSON, GASKEY & OLDS/PRATT & WHITNEY 400 West Maple Road Suite 350 Birmingham, MI 48009 UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www .uspto.gov ATTORNEY DOCKET NO. PA11338US; 67097-1751PUS1 CONFIRMATION NO. 7017 EXAMINER LIANG, ANTHONY M ART UNIT PAPER NUMBER 1734 NOTIFICATION DATE DELIVERY MODE 08/23/2018 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address(es): ptodocket@cgolaw.com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte AGNIESZKA M. WUSATOWSKA-SARNEK and RONALD S. MACE Appeal2017-009757 Application 13/563,216 Technology Center 1700 Before TERRY J. OWENS, ROMULO H. DELMENDO, and MICHAEL G. McMANUS, Administrative Patent Judges. OWENS, Administrative Patent Judge. DECISION ON APPEAL STATEMENT OF THE CASE The Appellants 1 appeal under 35 U.S.C. § 134(a) from the Examiner's rejection of claims 1-8, 16, 19, 20, and 22. We have jurisdiction under 35 U.S.C. § 6(b). The Invention The Appellants claim a powder metallurgy method and a superalloy article. Claims 1 and 19 are illustrative: 1. A powder metallurgy method comprising: (a) consolidating a metallic powder into a shape; 1 The real party in interest is United Technologies Corporation (App. Br. 2). Appeal2017-009757 Application 13/563,216 (b) thermo-mechanically forging the shape into an article having a polycrystalline micro structure; ( c) heat treating the article to cause coarsening of the polycrystalline microstructure; and ( d) controlling the grain size homogeneity and distribution in the article formed during coarsening in step ( c) by selecting the metallic powder in step (a) to include a metallic powder particle size distribution that is truncated on fine and coarse particle size sides, the selected metallic powder particle size distribution reducing abnormal grain growth such that grains of the polycrystalline microstructure coarsen and are all within an ASTM grain size number of 4-8. 19. An article comprising: a superalloy composition having a polycrystalline microstructure defining a uniform grain size such that the grains of the polycrystalline microstructure are all within an ASTM grain size number of 4-8. Larson Raymond The References us 3,976,482 us 5,584,947 Mesh to Micron Conversion Chart 1-2, http://www.showmegold.org/news/Mesh.htm (undated). The Rejections Aug. 24, 1976 Dec. 17, 1996 The claims stand rejected as follows: claims 19 and 20 under 35 U.S.C. § 102(b) or, in the alternative, under 35 U.S.C. § 103(a) over Raymond, and claims 1-8, 16, and 22 under 35 U.S.C. § 103(a) over Raymond in view of Larson as evidenced by Mesh to Micron Conversion Chart. 2 Appeal2017-009757 Application 13/563,216 OPINION We reverse the rejection under 35 U.S.C. § 102(b) over Raymond, affirm the rejection under 35 U.S.C. § 103(a) over Raymond, and reverse the rejection under 35 U.S.C. § 103(a) over Raymond in view of Larson as evidenced by Mesh to Micron Conversion Chart. Claims 19 and 20 Rejection under 35 US.C. § 102(b) over Raymond "Anticipation requires that every limitation of the claim in issue be disclosed, either expressly or under principles of inherency, in a single prior art reference." Corning Glass Works v. Sumitomo Elec. US.A., Inc., 868 F.2d 1251, 1255-56 (Fed. Cir. 1989). Raymond adds to a nickel-base superalloy an amount of carbon above its solubility level to form a carbide phase within the alloy sufficient to pin the grain boundaries to prevent localized abnormal excessive grain growth to diameters exceeding a desired range, which preferably is between about ASTM 7 and ASTM 8 for some gas turbine engine components, during supersolvus heat treatment ( above the alloy's y' solvus temperature) ( col. 1, 11. 29-30, 36-40; col. 2, 11. 44--51 ). The supersolvus heat treatment "is sufficient to uniformly coarsen the grains of the article to at least about ASTM 9" (col. 7, 11. 66-67) and "can be performed to achieve a uniform grain size within a range of about 2 or 3 ASTM units, such as about ASTM 7-8 without grains larger than ASTM 4" (col. 8, 11. 1--4). The Examiner finds (Ans. 2): Regarding claim 19, Raymond et al. teaches an article comprising a nickel superalloy composition having a uniform grain size (i.e. having a polycrystalline, or multi-grain, microstructure) within a range of about 2 or 3 ASTM units, 3 Appeal2017-009757 Application 13/563,216 such as about ASTM 7-8 without grains larger than ASTM 4, which satisfies the instantly limitation [sic] "defining a uniform grain size such that the grains of the polycrystalline microstructure are all within an ASTM grain size number of 4-8." (col. 1 ln. 6, col. 7 ln. 61-67, col. 8 ln. 1-4). The Examiner does not establish that Raymond's disclosure of an article having a uniform grain size of ASTM 4 to "about ASTM 7-8" ( col. 8, 11. 3--4), which includes grain sizes smaller than ASTM 8, is a disclosure of an article whose grains "all are within an ASTM grain size number of 4-8" as required by the Appellants' claim 19 and its dependent claim 20. Accordingly, we reverse the rejection under 35 U.S.C. § 102(b). Rejection under 35 USC§ 103(a) over Raymond Raymond's disclosure of an article having a uniform grain size of ASTM 4 to about ASTM 7-8 (col. 8, 11. 3--4) would have led one of ordinary skill in the art, through no more than ordinary creativity, to use any lower grain size limit within that range, including ASTM 8, such that all grains are within ASTM 4--8 as required by the Appellants' claim 19 and its dependent claim 20. See KSR Int'! Co. v. Teleflex Inc., 550 U.S. 398,418 (2007) (in making an obviousness determination one "can take account of the inferences and creative steps that a person of ordinary skill in the art would employ"). The Appellants assert that "[t]he phrase 'without grains larger than ASTM 4' implies that not all of the grains are size 7-8" (Reply Br. 4) and "[ c ]oupled with Raymond's silence on whether there are grains smaller than size 8, one cannot say whether Raymond's grains meet the claim language" (id.). 4 Appeal2017-009757 Application 13/563,216 The Appellants' claims do not require that all grains are ASTM 7-8. Raymond's grains can be ASTM 4 to about ASTM 7-8 (col. 8, 11. 3--4) which, as pointed out above, would have suggested the Appellants' range of ASTM 4--8. We therefore are not persuaded of reversible error in the rejection of claims 19 and 20 under 35 U.S.C. § 103(a). Claims 1---8, 16 and 22 Larson discloses that subjecting IN-792 powder to one or more rolling mill passes followed by hot isostatic pressing produces a duplex microstructure with fine grains substantially surrounding large grains, but subjecting screened IN-792 powder to one or more passes through a rolling mill produces consolidated particles having a relatively uniform ASTM 16-10 grain size and a true aspect ratio 2 of about 2 or more ( col. 4, 11. 20-24). An aspect ratio of 2.0 was obtained using a -200 + 325 mesh size and one pass through the rolling mill ( col. 4, 11. 25-35). The Examiner concludes (Ans. 4-5): It would have been obvious to one of ordinary skill in the art at the time of the invention to use a consolidation process wherein nickel-based superalloy powder is screened using mesh size -200 + 325, rolled, and subjected to hot isostatic pressing consolidating in the method of Raymond et al., as taught by Larson, in order to form a uniformly fine grain size of AS TM 16-10 while avoiding the forming of a duplex microstructure wherein large grains are surrounded by fine grams. 2 "True aspect ratio is represented as the average diameter of the rolled particles divided by average particle thickness" (col. 3, 11. 63---65). 5 Appeal2017-009757 Application 13/563,216 The Examiner does not address the differences between Raymond's method for obtaining a desired grain size range by using carbide particles to pin grain boundaries and Larson's method for obtaining a desired grain size range and aspect ratio by screening powder and then passing it through a rolling mill, and establish that regardless of those differences, the references would have provided one of ordinary skill in the art with an apparent reason to combine their disclosures as proposed by the Examiner. See KSR, 550 U.S. at 418. Thus, the Examiner's rejection of claims 1-8, 16 and 22 appears to be based upon impermissible hindsight in view of the Appellants' disclosure. See In re Warner, 379 F.2d 1011, 1017 (CCPA 1967) ("A rejection based on section 103 clearly must rest on a factual basis, and these facts must be interpreted without hindsight reconstruction of the invention from the prior art"). Accordingly, we reverse the rejection. DECISION The rejection of claims 19 and 20 under 35 U.S.C. § 102(b) over Raymond is reversed. The rejection of claims 19 and 20 under 35 U.S.C. § 103(a) over Raymond is affirmed. The rejection of claims 1-8, 16 and 22 under 35 U.S.C. § 103(a) over Raymond in view of Larson as evidenced by Mesh to Micron Conversion Chart is reversed. The Examiner's decision is affirmed-in-part. No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. § 1.136(a). 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