Ex Parte Wang et alDownload PDFPatent Trial and Appeal BoardJul 26, 201814163553 (P.T.A.B. Jul. 26, 2018) Copy Citation UNITED STA TES p A TENT AND TRADEMARK OFFICE APPLICATION NO. FILING DATE FIRST NAMED INVENTOR 14/163,553 01/24/2014 Xiao Wang 44639 7590 07/30/2018 CANTOR COLBURN LLP-BAKER HUGHES, A GE COMPANY, LLC 20 Church Street 22nd Floor Hartford, CT 06103 UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www .uspto.gov ATTORNEY DOCKET NO. CONFIRMATION NO. TYI4-57013-US (BA01187US) 9558 EXAMINER VALDEZ, DEVE E ART UNIT PAPER NUMBER 1765 NOTIFICATION DATE DELIVERY MODE 07/30/2018 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address(es): usptopatentmail@cantorcolbum.com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte XIAO WANG and ANIL K. SADAN A Appeal2017-009572 Application 14/163,553 Technology Center 1700 Before JEFFREY B. ROBERTSON, A VEL YN M. ROSS, and JENNIFER R. GUPTA, Administrative Patent Judges. GUPTA, Administrative Patent Judge. DECISION ON APPEAL 1 Appellants2 appeal under 35 U.S.C. § 134(a) from the Examiner's final decision rejecting claims 1---6, 10-12, and 18-20. 3 We have jurisdiction under 35 U.S.C. § 6(b ). We affirm. 1 In this Decision, we refer to the Specification filed January 24, 2014, the Final Office Action dated July 1, 2016 ("Final Act."), the Appeal Brief filed February 22, 2017 ("Br."), and the Examiner's Answer dated April 11, 2017 ("Ans."). 2 Appellants identify the real party in interest as Baker Hughes Incorporated. Br. 2. 3 Although the Final Office Action dated July 1, 2016, lists claims 8 and 9 as pending (Final Act. 1 ), claims 8 and 9 were canceled in an Amendment After Final filed October 17, 2016. Claims 13, 14, 16, and 17 are withdrawn from consideration by the Examiner. Final Act. 1. Appeal2017-009572 Application 14/163,553 The subject matter of the appealed claims relates to nanocomposite microgels comprising a polymer and a water-swellable mineral clay. Spec. ,r 1. Claim 1, reproduced below from the Claims Appendix with emphasis on key disputed limitations, is illustrative of the claims on appeal. 1. Nanocomposite microgel particles, comprising a three-dimensional network comprising: a water-swellable nanoclay; and an organic network polymer; wherein the nanocomposite microgel particles comprise primary nanocomposite microgel particles having a mean diameter of 1 to 10 micrometers as measured by scanning electron microscopy, wherein the organic network polymer is the polymerization product of a monomer composition comprising, based on the total weight of the monomers: 20 to less than 100 wt.% of a water-soluble, polar, nonionic ethylenically monounsaturated monomer, the water- soluble, polar, nonionic ethylenically monounsaturated monomer comprising an acrylamide, methacrylamide, N-(C1- Cs alkyl)(meth)acrylamide, N,N-di(C1-Cs alkyl)acrylamide, or a combination comprising at least one of the foregoing monomers; and greater than O to 80 wt.% of a water-soluble, polar, anionic ethylenically monounsaturated monomer, the water- soluble, polar, anionic ethylenically monounsaturated monomer comprising 2-acrylamido-2-methylpropane sulfonic acid or a salt thereof. Br. 13 (Claims App.) (emphasis added). 2 Appeal2017-009572 Application 14/163,553 REJECTIONS 4 The Examiner maintains the following rejections on appeal: Rejection 1: Claims 1---6, 10-12, and 18-205 over Lorah et al. (US 2002/0055580 Al, published May 9, 2002) ("Lorah") (Ans. 2); and Rejection 2: Claims 1---6, 10-12, and 18-20 are rejected for non- statutory obviousness type double patenting over claims 1, 4, 5 and 7-14 of U.S. Patent No. 9,334,337 (Application No. 14/209,057). (Ans. 9, 17). DISCUSSION We review the appealed rejections for error based upon the issues identified by Appellants and in light of the arguments and evidence produced thereon. Cf Ex parte Frye, 94 USPQ2d 1072, 107 5 (BP AI 2010) (precedential) (cited with approval in In re Jung, 637 F.3d 1356, 1365 (Fed. Cir. 2011) ("it has long been the Board's practice to require an applicant to identify the alleged error in the examiner's rejections")). After considering each of Appellants' contentions, we are not persuaded that Appellants 4 Claim 9 was canceled in an Amendment filed October 17, 2017. Thus, the rejection of claim 9 under 35 U.S.C. § 103 over Lorah in view of additional prior art is moot. In addition, the Examiner withdrew the rejection of claim 18 under 35 U.S.C. § 112(b) as indefinite. Ans. 2. 5 Claim 6 is omitted from the statement of rejection. Because claim 6 is discussed in the body of the rejection (Final Act. 5), and Appellants recognize that claim 6 should have been included in the rejection (Br. 3), we consider the omission harmless error, and modify the statement of rejection to include claim 6 for clarity. The Examiner also includes claim 8 in the statement of rejection, however, as discussed above, claim 8 was canceled by Appellants in an Amendment filed October 17, 2016. Thus, for clarity we omit claim 8 from the statement of rejection. 3 Appeal2017-009572 Application 14/163,553 identify reversible error. Thus, we sustain the Examiner's rejections for the reasons expressed in the Final Office Action, the Answer, and below. Rejection 1 Appellants present separate arguments for the patentability of claims 1, 12, 19, and 20. We discuss each of these claims in tum below. Claim 1 The Examiner finds that Lorah teaches claim 1 's nanocomposite microgel particles. Final Act. 3--4. Specifically, the Examiner finds that Lorah teaches nanocomposite dispersions comprising an aqueous dispersion of at least one clay, and a monomer mixture that includes from 25 weight percent to 100 weight percent of an ethylenically unsaturated monomer, preferably C1-C1s alkyl (meth)acrylate monomers, and at least 10 weight percent of an acid containing monomer, for example 2-acrylamido-2- methylpropone sulphonic acid. Final Act. 3 (citing Lorah Abstract, ,r,r 35- 38). The Examiner finds that Lorah teaches the diameter of the nanocomposite is 1 micron. Final Act. 3 ( citing Lorah ,r 97). Appellants contend that Lorah's paragraph 97 discloses the average particle size of the core obtained by a single stage process or a process involving several stages. Br. 4. According to Appellants, the average particle size of a core is not equivalent to the diameter of a nanocomposite as the Examiner finds. Id. Accordingly, Appellants argue that Lorah does not teach or suggest nanocomposite microgel particles with a mean diameter of 1 to 10 micrometers as recited in claim 1. Id. In the Answer the Examiner responds to Appellants' argument and finds that Lorah's paragraph 75 teaches core shell nanocomposites having a 4 Appeal2017-009572 Application 14/163,553 particle diameter of greater than 1000 nanometers, which is 1 micron. Ans. 10. Appellants did not file a Reply Brief, and thus do not identify error in the Examiner's finding. Thus, we are not persuaded by Appellants' argument of reversible error in the Examiner's rejection. Appellants argue that there is no teaching in Lorah that would have led one skilled in the art to the specific combination of a water-soluble, polar, nonionic ethylenically monounsaturated monomer, and a water soluble, polar, anionic ethylenically monosaturated monomer as defined in instant claim 1, let alone in the amounts recited in claim 1. Br. 4. Appellants' argument is not persuasive of reversible error. Lorah's disclosures would have indicated to one of ordinary skill in the art to use a monomer mixture comprising from 25 weight percent to 100 weight percent of C1-C1s alkyl (meth)acrylate monomers, a preferable ethylenically unsaturated monomer for its low cost and commercial availability, in combination with at least 10% by weight of acid containing monomer, for example 2-acrylamido-2-methylpropone sulphonic acid. See Merck & Co., Inc. v. Biocraft Labs., Inc., 874 F.2d 804, 807 (Fed. Cir. 1989) (The fact that a reference "discloses a multitude of effective combinations does not render any particular formulation less obvious."). Thus, we discern no reversible error in the Examiner's conclusion that claim 1 's polymer, which is the polymerization product of a water-soluble, polar, nonionic ethylenically monounsaturated monomer, and a water-soluble, polar, anionic ethylenically monounsaturated monomer, would have been prima facie obvious to one of ordinary skill in the art based on Lorah. Finally, Appellants argue that the evidence presented in the Declaration under 37 C.F.R. § 1.132 of Xiao Wang executed May 10, 2016 5 Appeal2017-009572 Application 14/163,553 ("the Wang Declaration"), and the Declaration under 37 C.F.R. § 1.132 of Anil Sadana executed September 13, 2016 ("the Sadana Declaration"), demonstrate that the claimed subject matter would not have been obvious because the particular combination of claimed elements results in unexpectedly beneficial properties. Br. 5-8. The burden rests with Appellants to establish that the alleged unexpected results presented as being associated with the claimed invention are, in fact, unexpected. In re Klosak, 455 F.2d 1077, 1080 (CCPA 1972). It is not enough for the Appellants to show that the results in the compared examples differ. The difference must be shown to be an unexpected difference. We have considered the Wang and Sadana Declarations. Although the Wang and Sadana Declarations state that the excellent compatibility of the inventive micro gel particles with brines containing divalent calcium ions is "surprising" (Wang Deel. ,r 13; Sadana Deel. ,r 14), on this record Appellants have not established with objective evidence that the difference in the compatibility of the inventive and the comparative examples with the divalent brines would not have been expected by one skilled in the art at the time of the invention. See, e.g., Wang Deel. ,r 9 ("some Comparative Sample B particles precipitated in the 10 wt.% CaCb brine."). The burden also rests with Appellants to establish that the supplied evidentiary showing is commensurate in scope with the claimed subject matter. In re Grasselli, 713 F.2d 731, 743 (Fed. Cir. 1983) (concluding that unexpected results "limited to sodium only" were not commensurate in scope with claims to a catalyst having "an alkali metal"). As the Examiner explains, the evidence presented in the Wang and Sadana Declarations is not 6 Appeal2017-009572 Application 14/163,553 reasonably commensurate in scope with the appealed claims. Ans. 13-14. Claim 1 's nonionic ethylenically monounsaturated monomer is not limited to acrylamide. Appellants have not established that the results obtained using the single embodiment is representative of the results which would be obtained for the other polymer networks covered by the claims. In view of the foregoing, we sustain the rejection of claim 1 over Lorah. Because Appellants do not present separate arguments for the patentability of claims 2---6, 10, 11, and 20, which directly or indirectly depend from claim 1, we also sustain the rejection of those claims over Lorah. Claim 12 Claim 12 is reproduced below from the Claims Appendix of the Appeal Brief. 12. The nanocomposite microgel particles of claim 1, further comprising crosslinks forming a bond between the water-swellable nanoclay and the organic network polymer. Br. 15 (Claims App.) Appellants argue that the Examiner fails to establish that Lorah's combination of nanoclay and polymer network would intrinsically crosslink when they are combined together. Br. 9-10. Appellants' argument is not persuasive of reversible error. As the Examiner finds, Lorah teaches nanocomposites that include clay and a polymer network comprised of at least one ethylenically unsaturated monomer and an acid containing monomer. Final Act. 6 ( citing Lorah, Abstract). Lorah teaches that suitable ethylenically unsaturated monomers include nitrogen containing vinyl unsaturated monomers ( e.g., acrylonitrile, 7 Appeal2017-009572 Application 14/163,553 methacrylonitrile, and C1 -C18 alkyl (meth)acrylamides, and the like), and a suitable acid containing monomer includes 2-acrylamido-2-methylpropane sulfonic acid, which read on the monomers recited in claim 12. Lorah ,r,r 36, 3 8. Lorah further teaches that suitable clays include synthetic minerals or synthetic phyllosilicates, such as LAPONITE®. Id. ,r 46. According to Appellants' Specification, the nanoclay acts as a multifunctional cross-linker of the monomer compositions. Spec. ,r 12. Appellants' Specification discloses Laponite as an example of a nanoclay used in its nanocomposite. Id. ,r 13. Thus, on this record, we determine that the Examiner has provided an adequate factual basis upon which to shift the burden to the Appellants to come forward with evidence to show Lorah's nanocomposite does not include crosslinks forming a bond between the water-swellable nanoclay and the organic network polymer, as recited in claim 12. See In re Spada, 911 F.2d 705, 708 (Fed. Cir. 1990) ("[W]hen the PTO shows sound basis for believing that the products of the applicant and the prior art are the same, the applicant has the burden of showing that they are not."). Appellants, however, do not provide such a showing. Thus, we sustain the rejection of claim 12. Claims 19 and 2 0 Claims 19 and 20 are reproduced below from the Claims Appendix of the Appeal Brief. 19. The nanocomposite microgel particles of claim 5, wherein the water-swellable nanoclay is a synthetic layered hectorite magnesium lithium silicate, the water-soluble, polar, nonionic ethylenically monounsaturated monomer is acrylamide, and the water-soluble, polar, anionic ethylenically 8 Appeal2017-009572 Application 14/163,553 monounsaturated monomer is 2-acrylamido-2-methylpropane sulfonic acid or a salt thereof. 20. The nanocomposite micro gel particles of claim 10, wherein the water-swellable nanoclay is a synthetic layered hectorite magnesium lithium silicate, the water-soluble, polar, nonionic ethylenically monounsaturated monomer is acrylamide, and the water-soluble, polar, anionic ethylenically monounsaturated monomer is 2-acrylamido-2-methylpropane sulfonic acid or a salt thereof. Br. 16-17 (Claims App.). Appellants argue that the Wang and Sadana Declarations demonstrate the surprising results obtained with claim 18 and claim 19 's nanocomposites. Br. 10. Appellants also argue that Lorah does not disclose a nanocomposite that includes acrylamide as the nonionic ethylenically unsaturated monomer. Id. Appellants' arguments are not persuasive of reversible error. Lorah teaches that its ethylenically unsaturated monomers include nitrogen- containing vinyl unsaturated monomers, for example, C1-C18 alkyl (meth)acrylamides) and the like. Lorah ,r 36. Based on this disclosure, we determine that Lorah teaches or reasonably suggests acrylamide as a suitable nitrogen-containing vinyl unsaturated monomer for use in Lorah's monomer mixture. Moreover, as discussed above with respect to claim 1, although the Wang and Sadana Declaration state that the results are "surprising" (Wang Deel. ,r 13; Sadana Deel. ,r 14), it does not establish with objective evidence that the difference between the results obtained with the claimed invention and those obtained with the comparative examples would not have been expected by one skilled in the art at the time of the invention. 9 Appeal2017-009572 Application 14/163,553 In view of the foregoing, we sustain the rejection of claims 19 and 20 over Lorah. Rejection 2 As the Examiner points out, Appellants does not present any arguments regarding the double patenting rejection in their Appeal Brief. Ans. 17. Thus, we summarily affirm the rejection. See Manual of Patent Examining Procedure (MPEP) § 1205.02 (9th ed., Mar. 2014) ("If a ground of rejection stated by the examiner is not addressed in the appellant's brief, appellant has waived any challenge to that ground of rejection and the Board may summarily sustain it, unless the examiner subsequently withdrew the rejection in the examiner's answer."). DECISION For the above reasons, the rejections of claims 1---6, 10-12, and 18-20 under 35 U.S.C. § 103 over Lorah, and the rejection of claims 1---6, 10-12, and 18-20 on the ground of non-statutory double patenting are affirmed. No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. § 1.136(a). AFFIRMED 10 Copy with citationCopy as parenthetical citation