Ex Parte Skoug et alDownload PDFPatent Trial and Appeal BoardSep 27, 201713773935 (P.T.A.B. Sep. 27, 2017) Copy Citation United States Patent and Trademark Office UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O.Box 1450 Alexandria, Virginia 22313-1450 www.uspto.gov APPLICATION NO. FILING DATE FIRST NAMED INVENTOR ATTORNEY DOCKET NO. CONFIRMATION NO. 13/773,935 02/22/2013 ERIC J. SKOUG P020051-RD-SDJ 3024 60770 7590 09/27/2017 General Motors Corporation c/o REISING ETHINGTON P.C. P.O. BOX 4390 TROY, MI 48099-4390 EXAMINER LEE, REBECCA Y ART UNIT PAPER NUMBER 1734 MAIL DATE DELIVERY MODE 09/27/2017 PAPER Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte GM GLOBAL TECHNOLOGY OPERATIONS LLC1 Appeal 2016-008340 Application 13/773,93 52 Technology Center 1700 Before PETER F. KRATZ, DONNA M. PRAISS, and JEFFREY R. SNAY, Administrative Patent Judges. PRAISS, Administrative Patent Judge. DECISION ON APPEAL3 1 The inventors are Eric J. Skoug, Martin S. Meyer, Jan F. Herbst, and Frederick E. Pinkerton. 2 General Motors Company and its wholly owned subsidiary, GM Global Technology Operations LLC, are identified as the real parties in interest. App. Br. 2. 3 In this Opinion, we refer to the Specification filed Feb. 22, 2013 (“Spec.”), the Final Office Action dated Oct. 14, 2015 (“Final Act.”), the Appeal Brief filed Mar. 10, 2016 (“App. Br.”), the Declaration of Jan F. Herbst under 37 C.F.R. § 1.132 dated Oct. 18, 2013 (“Herbst Decl.”), the Examiner’s Answer dated July 22, 2016 (“Ans.”), and the Reply Brief filed Sept. 8, 2016 (“Reply Br.”). Appeal 2016-008340 Application 13/773,935 Appellant appeals under 35 U.S.C. § 134(a) from the Examiner’s decision to reject claims 1, 2, 4—6, 8, and 9 as obvious under 35 U.S.C. § 103(a) over Yamamoto.4 App. Br. 5. We have jurisdiction under 35 U.S.C. § 6(b). We AFFIRM. The invention relates to rare earth-iron-boron permanent magnets, more particularly, cerium-iron-boron permanent magnets and cerium-iron- cobalt-boron magnets. Spec. 12. According to Appellant, renewed interest in optimizing the permanent magnet properties of cerium-iron-boron compositions has been stimulated by developments in the supply and price of rare earth elements. App. Br. 4. While Nd2Fei4B is said to be the best permanent magnet, neodymium is expensive and the future cost and availability of Nd, Pr, Dy, and Tb are also of concern. Id. Claim 1 is illustrative (disputed limitations italicized): 1. A method of making a permanent magnet composition comprising: preparing a melt consisting essentially of the elements cerium, iron, and boron, the melt being under a non-oxidizing atmosphere; forming rapidly solidified, amorphous or nano-crystalline particles of the cerium-iron-boron composition from the melt, such particles having properties of a soft magnetic material; annealing the soft magnetic particles at a predetermined temperature above about 450°C for a predetermined time to form a crystalline material having permanent magnet properties characterized by values of intrinsic coercivity, Hci in kOe, and 4 Hiroshi Yamamoto, Mitsuru Nagakura & Masahiko Saito, Magnetic Properties of Melt-spun Ce-(Fe, Co)-(B, Si) System Alloys, 51 J. Japan Instit. Metals 83—90 (1987). The Examiner and Appellant refer to this reference as Hiroshi and Yamamoto interchangeably in the record. 2 Appeal 2016-008340 Application 13/773,935 remanence, Br in kG, where the numerical sum of Hci and Br is 10 or greater, the crystalline material further being characterized as comprising at least seventy percent by mass of the compound Ce2Fei4B and the balance comprised of secondary phases, each secondary phase containing one or more of cerium, iron, and boron, the permanent magnet properties and the proportions of the compound Ce2Fei4B and the secondary phases in the annealed material resulting from the proportions of the elements cerium, iron, and boron in the prepared melt and the annealing time and temperature, the proportions of the compound Ce2Fei4B and the secondary phases being determined from analyses of X- ray diffraction patterns of powder samples of the annealed permanent magnet material. App. Br. 12 (Claims Appendix). OPINION The Examiner finds that claims 1, 2, 4—6, 8, and 9 would have been obvious to one of ordinary skill in the art at the time of the invention over Yamamoto for the reasons stated on pages 2—5 of the Final Office Action. Appellant does not separately argue the claims rejected, therefore, we select claim 1 as representative. See 37 C.F.R. § 41.37(c)(l)(iv). Appellant argues that the Examiner erred in rejecting the claims over Yamamoto because Yamamoto does not disclose a magnet composition where at least 70% is Ce2Fei4B and the balance comprised of secondary phases. App. Br. 7. Appellant contends that Yamamoto “has no idea of the proportionality of Ce2Fei4B or any other element or phase” because Yamamoto states “it is difficult to calculate theoretical values because it is impossible to calculate the proportions of the two phases.” Id. (quoting Yamamoto 85) (emphasis omitted). According to Appellant, the Examiner erred in finding that it would have been obvious to discover an optimum 3 Appeal 2016-008340 Application 13/773,935 value of a result effective variable in view of Yamamoto’s teaching that it is impossible to calculate the proportions of the composition phases. Id. Similarly, Appellant contends that Yamamoto does not “provide any teaching of how to manage crystal phases and proportions to obtain the combination of intrinsic coercivity and remanence values obtained” in view of Yamamoto’s teaching that “it is difficult to calculate theoretical values because it is impossible to calculate the proportions of the two phases from the results of X-ray diffraction.” Id. at 8 (quoting Yamamoto 85) (emphasis omitted). Appellant argues that the Examiner erred in finding that the claimed sum of values of intrinsic coercivity and remanence would have been expected in the Yamamoto process because the effect of the time and temperature of Appellant’s annealing processes require analysis and control of the crystal structure to be produced, which Yamamoto did not and could not accomplish. Id. at 9. Regarding the Herbst Declaration, Appellant contends that the Examiner erred in “reject[ing] Dr. Herbst’s analysis” that Yamamoto’s statement on page 90 that “the creation of fine structure yielding maximum coercivity by the annealing of amorphous samples was found to be extremely difficult” reflects Yamamoto’s “failure to successfully discover or devise the methods for obtaining optimum Ce-Fe-B and Ce-(Fe, Co)-B permanent magnets that we have disclosed and claimed in our present application.” Id. at 10 (quoting Yamamoto 90; Herbst Decl. 114). According to Appellant, “[a]ny fair reading of the Hiroshi paper, as summarized and evaluated in the Herbst declaration, reveals that Hiroshi made some Ce2oFe7oBio alloy ribbons at different quench wheel speeds, and annealed some of them, but was wholly unable to analyze the proportions of 4 Appeal 2016-008340 Application 13/773,935 any crystal phases or effectively modify the amount of any phase, including the Ce2Fei4B ‘variable.’” Id. at 9. The Examiner responds that “[e]ven if... it is difficult to obtain desirable results, or to improve the current result, difficult to achieve is not impossible to achieve; and less than desirable result, or unimproved result, does not necessarily [mean] being an unsatisfactory result.” Ans. 5—6. The Examiner also responds that Yamamoto teaches that determination by X-ray diffraction has been conducted (Yamamoto Section II, Experimental Methods). Id. at 5. Regarding the recited numerical sum of HCi and Br, the Examiner responds that such properties would be expected in Yamamoto in view of Yamamoto’s disclosure of “the same or substantially the same method using the same or substantially the same composition as instantly claimed” and the lack of factual evidence to show otherwise. Id. at 6. Regarding optimizing the quantities of compound Ce2Fei4B in order to achieve desired magnetic properties, the Examiner finds that Yamamoto teaches the quantity of the compound “greatly affects the magnetic properties (Pages 84-85)” and therefore the quantity as well as the remaining phase are result effective variables. Ans. 6—7. The Examiner concludes that Appellant has not rebutted the evidence of obviousness with the Herbst Declaration because “discovering an optimum value of a result effective variable requires only routine skill in the art.” Id. at 7. In the Reply Brief, Appellant argues that “[t]he Examiner has again improperly refused to consider Dr. Herbst’s declaration.” Reply Br. 4. Appellant contends that the Declaration explains why the claimed methods “requires much more than just sorting out optimum values for ‘variables’ presented in the Hiroshi Yamamoto paper.” Id. Appellant further argues 5 Appeal 2016-008340 Application 13/773,935 that the Herbst Declaration is factually supported objective evidence in its detailed analysis in paragraphs 7—11. Id. at 4—5. According to Appellant, Yamamoto’s statements about being difficult to calculate the proportions of the two phases because it was impossible to calculate the proportions from the results of the X-ray diffraction means “[t]hey couldn’t do it, they didn’t do it, and they certainly didn’t encourage anyone else to try to do it” since Appellant’s claimed methods are not the result of optimizing the teachings of Yamamoto. Id. at 5. We are not persuaded by Appellant’s arguments for the reasons stated by the Examiner in the Final Office Action and Answer. We add the following primarily for emphasis. The problem with Appellant’s argument is that Yamamoto explicitly teaches “[o]n the basis of these results, it is thought that Ce2Fei4B is formed in melt-spun Ce-Fe-B ternary alloy ribbons and that the quantity of this compound greatly affects its magnetic properties.” Yamamoto 84. Thus, the Examiner’s finding that Yamamoto recognizes that the amount of Ce2Fei4B is a result effective variable that greatly affects the magnetic properties of the compound (Final Act. 3) is supported by the preponderance of the evidence cited in this appeal. The discovery of an optimum value of a variable in a known process is normally obvious. In re Aller, 220 F.2d 454, 456 (CCPA 1955) (experimentation to find optimum conditions was “no more than the application of the expected skill of the chemical engineer.”). To the extent that Appellant argues criticality in achieving the claimed properties, Appellant’s argument is not adequately supported by evidence in the cited record on appeal. As the Examiner finds, the claim is not limited to any specific composition, such as Ce2oFe7oBio, the alloy of 6 Appeal 2016-008340 Application 13/773,935 Yamamoto’s example that Appellant criticizes. Ans. 8; Yamamoto 85—88. Moreover, it is not necessary that Yamamoto disclose the claimed composition as a working example as Appellant’s arguments suggest. In re Mills, 470 F.2d 649, 651 (CCPA 1972) (citation omitted) (“a reference is not limited to the disclosure of specific working examples.”). In addition, Appellant does not adequately explain why the compositions taught by Yamamoto would not be expected to share the same properties as the claimed composition (App. Br. 9; Reply Br. 2). As Appellant notes, the “magnetic properties are demonstrated to depend on proportions of the formed crystal structures” (Reply Br. 2), and Appellant does not dispute that Yamamoto discloses that quantity “greatly affects its magnetic properties” (Yamamoto 84). In the absence of evidence to the contrary, the Examiner’s finding that the claimed properties would be expected in Yamamoto’s composition (Final Act. 3) is supported by the record on appeal. The Examiner has provided the record with a preponderance of evidence including commonalities shared by the method of Yamamoto and the claims (id. at 2—3), which justifies requiring Appellant to show that Yamamoto’s product would not be expected to have the claimed numerical sum of Hci and Br. See In re Best, 562 F.2d 1252, 1255 (CCPA 1977) (“[T]he PTO can require an applicant to prove that the prior art products do not necessarily or inherently possess the characteristics of his claimed product. . . . Whether the rejection is based on ‘inherency’ under 35 U.S.C. § 102, on ‘prima facie obviousness’ under 35 U.S.C. § 103, jointly or alternatively, the burden of proof is the same, and its fairness is evidenced by the PTO’s inability to manufacture products or to obtain and compare prior art products.” (footnote omitted)). The Herbst Declaration is 7 Appeal 2016-008340 Application 13/773,935 insufficient to rebut the Examiner’s findings because it is not necessary that Yamamoto use the same methods of optimization that Appellant used in view of Yamamoto’s express disclosure of optimizing quantity to achieve the desired result (Ans. 7). Appellant’s argument that Yamamoto did not calculate proportions of the two phases from the results of X-ray diffraction because the reference states that it was difficult to do so (App. Br. 8—9; Reply Br. 5) is not persuasive. As discussed above, Appellant provides no evidence to support its argument other than that Yamamoto discloses difficulties in calculations performed in connection with an example. Appellant does not dispute the Examiner’s finding that difficult to achieve does not mean impossible to achieve. Ans. 5—6. Moreover, neither Appellant nor the Herbst Declaration addresses whether the difficulties described by Yamamoto are simply due to the state of the laboratory equipment available at the time for analyzing Yamamoto’s samples. In sum, we affirm the Examiner’s rejection of claims 1, 2, 4—6, 8, and 9 as obvious over Yamamoto. CONCLUSION We affirm the Examiner’s rejection of claims 1, 2, 4—6, 8, and 9 as obvious under 35 U.S.C. § 103(a). DECISION The Examiner’s decision is affirmed. 8 Appeal 2016-008340 Application 13/773,935 No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. § 1.136(a)(1). AFFIRMED 9 Copy with citationCopy as parenthetical citation