Ex Parte ReeseDownload PDFPatent Trial and Appeal BoardOct 24, 201713528909 (P.T.A.B. Oct. 24, 2017) Copy Citation United States Patent and Trademark Office UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O.Box 1450 Alexandria, Virginia 22313-1450 www.uspto.gov APPLICATION NO. FILING DATE FIRST NAMED INVENTOR ATTORNEY DOCKET NO. CONFIRMATION NO. 13/528,909 06/21/2012 Jack R. Reese BMS122006/MD08-22 4509 157 7590 Covestro LLC 1 Covestro Circle PITTSBURGH, PA 15205 10/26/2017 EXAMINER MURESAN, ANA Z ART UNIT PAPER NUMBER 1671 NOTIFICATION DATE DELIVERY MODE 10/26/2017 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address(es): veronica.thompson@covestro.com US-IPR@covestro.com laura.finnell @ covestro. com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte JACK R. REESE1 Appeal 2016-000385 Application 13/528,909 Technology Center 1600 Before FRANCISCO C. PRATS, JEFFREY N. FREDMAN, and RYAN H. FLAX, Administrative Patent Judges. FLAX, Administrative Patent Judge. DECISION ON APPEAL This is a decision on appeal under 35 U.S.C. § 134(a) involving claims directed to a continuous process for the production of a polyoxyalkylene polyether polyol having a hydroxyl content of from about 3.4 to about 12.1% by weight. Claims 1—28 are on appeal as rejected under 35 U.S.C. § 103(a) and as provisionally rejected for obviousness-type double patenting. We have jurisdiction under 35 U.S.C. § 6(b). We reverse the obviousness rejections and decline to reach the merits of the provisional double patenting rejection. 1 Appellant identifies the Real Party in Interest as “Bayer MaterialScience LLC.” App. Br. 1. Appeal 2016-000385 Application 13/528,909 STATEMENT OF THE CASE The Specification states, “[t]he preparation of polyoxyalkylene polyols by double metal cyanide (DMC) catalysts is known” and “[w]hile double metal cyanide catalysts provide numerous advantages in preparing polyoxyalkylene polyols, there are, unfortunately, some disadvantages to this type of catalysis. . . . These disadvantages include the tendency of the catalyst to deactivate.” Spec. 1:11—29. The Specification further states: The present invention allows the preparation of low molecular weight polyoxyalkylene polyether polyols by a continuous process in which a low molecular weight starter is alkoxylated in the presence of a double metal cyanide catalyst. It has been found that carefully maintaining the oxyalkylation reaction at a sufficiently high temperature prevents catalyst deactivation, even in the presence of high levels of low molecular weight starters. Id. at 3:21-27. Claims 1, 18, 19, 21, 23, and 28 are independent claims. Claim 1 is representative and is reproduced below: 1. A continuous process for the production of a polyoxyalkylene polyether polyol having a hydroxyl content of from about 3.4 to about 12.1% by weight, which comprises: establishing oxyalkylation conditions in a continuous oxyalkylation reactor in the presence of a double metal cyanide catalyst; continuously introducing alkylene oxide and a low molecular weight starter into said continuous oxyalkylation reactor, wherein said starter has a number average molecular weight of from 50 to 250; continuously recovering a partially oxyalkylated polyether polyol from the continuous oxyalkylation reactor; 2 Appeal 2016-000385 Application 13/528,909 wherein (i) said oxyalkylation in the continuous oxyalkylation reactor occurs at a sufficiently high temperature to prevent deactivation of the DMC catalyst; (ii) the concentration of unreacted alkylene oxide in the contents of the continuous reactor is maintained at a level of from 1 to 3% by weight; and (iii) the hydroxyl content of the reactor contents is maintained at 3.4 to 12.1% by weight; and allowing further reaction of the partially oxyalkylated polyether polyol which is recovered from the continuous oxyalkylation reactor to occur until the unreacted alkylene oxide content of the mixture is reduced to 0.001% or less by weight App. Br. 14 (Claims App’x). The following rejections are on appeal: Claims 1—28 stand rejected under 35 U.S.C. § 103(a) over Pazos.2 Final Action 6—8. Claims 1—28 stand rejected under 35 U.S.C. § 103(a) over Sasaki.3 Id. at 8—10. Claims 1—28 stand provisionally rejected under the doctrine of non- statutory obviousness-type double patenting over claims 1—28 of ’394 application.4 Id. at 12—13. DISCUSSION I. Obviousness “[A] claim must be read in view of the specification of which it is a part.” Renishaw PLC v. Marposs Societa'per Azioni, 158 F.3d 1243, 1248 2 U.S. Patent 5,777,177 (issued July 7, 1998) (“Pazos”). 3 PCT Pub. WO 2011/136367 A1 (published Nov. 3, 2011) (“Sasaki”) (English translation via EPO/Espacenet). 4 Co-pending U.S. Patent Application 13/826,394 (“’394 application”). 3 Appeal 2016-000385 Application 13/528,909 (Fed. Cir. 1998). “The specification acts as a dictionary when it expressly defines terms used in the claims or when it defines terms by implication.” Vitronics Corp. v. Conceptronic, Inc., 90 F.3d 1576, 1582 (Fed. Cir. 1996). Further, one “does not interpret claim terms in a vacuum, devoid of the context of the claim as a whole.” Kyocera Wireless Corp. v. Int’l Trade Com’n, 545 F.3d 1340, 1347 (Fed. Cir. 2003) (citingHockerson— Halberstadt, Inc. v. Converse Inc., 183 F.3d 1369, 1374 (Fed. Cir. 1999) (“[pjroper claim construction . . . demands interpretation of the entire claim in context, not a single element in isolation.”)). In determining patentability, “we must give effect to all claim limitations.” In re Angstadt, 537 F.2d 498, 501 (CCPA 1976). “In rejecting claims under 35 U.S.C. § 103, the examiner bears the initial burden of presenting a prima facie case of obviousness. Only if that burden is met, does the burden of coming forward with evidence or argument shift to the applicant.” In re Rijckaert, 9 F.3d 1531, 1532 (Fed. Cir. 1993). “Even when obviousness is based on a single prior art reference, there must be a showing of a suggestion or motivation to modify the teachings of that reference.” In re Kotzab, 217 F.3d 1365, 1370 (Fed. Cir. 2000). “[Rejections on obviousness grounds cannot be sustained by mere conclusory statements; instead, there must be some articulated reasoning with some rational underpinning to support the legal conclusion of obviousness.” KSR Int’l Co. v. Teleflex Inc., 550 U.S. 398, 418 (2007) (quoting In re Kahn, 441 F.3d 977, 988 (Fed. Cir. 2006)). When a prima facie case of obviousness has not been established, the rejection must be reversed. In re Fine, 837 F.2d 1071, 1075 (Fed. Cir. 1988). 4 Appeal 2016-000385 Application 13/528,909 “[W]here the general conditions of a claim are disclosed in the prior art, it is not inventive to discover the optimum or workable ranges by routine experimentation.” In reAller, 220 F.2d 454, 456 (CCPA 1955). However, “[t]his rule is limited to cases in which the optimized variable is a ‘result- effective variable.’” In re Applied Materials, Inc., 692 F.3d 1289, 1295 (Fed. Cir. 2012) (quoting In re Antonie, 559 F.2d 618, 620 (CCPA 1977)); see also In re Boesch, 617 F.2d 272, 276 (Fed. Cir. 1980) (“[Discovery of an optimum value of a result effective variable ... is ordinarily within the skill of the art.”). Obviousness and Pazos We find the Examiner has not established a prima facie case that claim 1 would have been obvious over Pazos. In making this rejection, the Examiner, in relevant part, states: In example 1 (col. 9 and continuing on col. 10) of [Pazos], it is disclosed that the process for producing polyol is conducted at 130 °C (instant claims recite temperature of at least 135 °C) and that the reactor pressure drops as results for DMC catalyst activation. . . . The difference between instantly claimed process for producing polyoxyalkylene polyether polyol and the process of [Pazos], is that the process of prior art is conducted at a slightly lower temperatures 130 °C compared to >135 °C of instantly claimed process and does not disclose the specific build ratio of the reactor as recited by instant claims 3, 4 or the pipe reactor, instead it recites that reactors of the appropriate dimensions are utilized for the process that overcome build ratio limitations. Note the phrase “sufficiently high” recited by instant claim 1 pertaining to the temperature of the process is a relative term which does not provide a standard for ascertaining the requisite temperature required by the process. Disclosed on col. 10 lines 5 Appeal 2016-000385 Application 13/528,909 4-7 of [Pazos] is that the reaction mixture is heated at 130 °C to activate the catalyst. Final Action 6—7. Thus, the Examiner concedes Pazos does not expressly disclose the claimed “wherein (i) said oxyalkylation in the continuous oxyalkylation reactor occurs at a sufficiently high temperature to prevent deactivation of the DMC catalyst,” but determines that it is merely an optimizable feature based on “the disclosure in the prior art, and the art recognized problem or [sic] optimizing temperature.” Id. at 7—8. Appellant argues the “Pazos reference uses a constant temperature of 130°C throughout the process,” which Appellant argues is not a “sufficiently high temperature to prevent deactivation of the DMC catalyst” per the examples described in the Specification and as claimed. App. Br. 8. Appellant identifies that the Specification describes that a temperature of 130°C was used in Examples 1 and 3 and the DMC catalyst deactivated and the process stopped, but contrasts this data with Examples 2 and 4, where a temperature of 140°C was used and the process “continued with no problems.” Id. Therefore, Appellant contends, “a process temperature of 140°C is a sufficiently high temperature,” as claimed, and Pazos does not teach or suggest such a temperature. Id. Finally, Appellant argues Pazos does not disclose information to provide a basis for the skilled artisan to reasonably expect that the temperature of the reactor might be increased to achieve a desired result, i.e., provide the “sufficiently high temperature” of the claims, and that providing such a temperature is not merely optimizing the temperature of Pazos because the Specification identifies that Pazos’s temperature fails in view of the claim element. Id. at 9. 6 Appeal 2016-000385 Application 13/528,909 We are persuaded by Appellant’s arguments on Pazos. Pazos teaches using a temperature of only 130°C to activate a catalyst and does not recognize a need to keep that catalyst active or temperature’s role therein; it does not suggest temperature is an optimizable variable. Appellant’s Specification’s examples describe that 130°C may be hot enough to initially activate a catalyst, but is not hot enough to keep the catalyst activated. The Specification describes temperatures of 135°C, and specifically 140°C, are sufficient. Even relying upon a KSR rationale, the Examiner must provide some basis for optimizing a variable such as temperature, and no such evidence has been provided. See MPEP § 2144.05(II)(B). For the above reasons, we reverse this rejection. Obviousness and Sasaki In making a determination that the claims are obvious over Sasaki, the Examiner stated: it would have been obvious to one of ordinary skill in the art at the time of invention was made, to utilize the process of producing the polyoxyalkylene polyol by oxyalkylation in the presence of a DMC catalyst and glycerol (glycerin) as starter, as disclosed in [Sasaki] and optimize the process by employing the appropriate built ratio and ratio, adjusting the temperature and the pressure of the process to enhance the efficiency of the process, because it involves preparation of the same product, polyoxyalkylene polyol, by using the same starting materials, catalyst and similar reaction parameters and would reasonable expect the process of prior art to be successful for the instantly claimed process of preparing said product. Absent a clear and convincing showing of unexpected results, the instant invention is found to be prima facie obvious over the prior art. Final Action 10. The Examiner also identified certain limitations of some claims and indicated where Sasaki teaches or suggests such limitations. Id. 7 Appeal 2016-000385 Application 13/528,909 8—10. However, we conclude that the Examiner has failed to sufficiently explain or show where Sasaki teaches or suggests each and every limitation of the invention of independent claims 1, 18, 19, 21, 23, and 28. Appellant argues Sasaki “requires three distinct polymerization steps,” which “are completely separate processes,” where DMC catalyst is used in just one of those steps. App. Br. 10. Appellant contrasts this with the invention, which, they argue is “a continuous process which uses a DMC (double metal cyanide) catalyst throughout the entire process.” Id. at 11. Appellant argues the claims require continuous addition of a low molecular weight starter (average mol.wt. of 50—250), but Sasaki does not continuously add starter, and its disclosed starters, e.g., triol starter, have an average mol.wt. outside the claimed range(s), i.e., 1500 or 1200. Id. Appellant also argues Sasaki’s example(s) use a temperature of 130°C, which is not a “sufficiently high temperature to prevent deactivation of the DMC catalyst.” Id. Finally, Appellant argues: a logical basis does not exist for one of ordinary skill in the art to reasonably predict or expect from reading the Sasaki et al reference that it is possible to control or increase the activity of a continuous reactor system by maintaining a sufficiently high temperature during oxyalkyation [sic] to obtain a polyoxyalkylene polyether polyol having a total hydroxyl content of from about 3.4 to about 12.1% by weight. App. Br. 12-13. While we are not persuaded by most of the above-identified arguments by Appellant, we are persuaded by the last. The Examiner has not identified where the “(iii) the hydroxyl content of the reactor contents is maintained at 3.4 to 12.1% [or 3.4 to 9.1%] by weight.” We also note that 8 Appeal 2016-000385 Application 13/528,909 much of the Examiner’s rationale for this rejection is unclear, including a determination of where Sasaki discloses, specifically, continuously recovering “partially oxyalkylated polyether polyol,” “(ii) the concentration of unreacted alkylene oxide in the contents of the continuous reactor is maintained at a level of from 1 to 3% by weight,” “allowing further reaction of the partially oxyalkylated polyether polyol which is recovered from the continuous oxyalkylation reactor to occur until the unreacted alkylene oxide content of the mixture is reduced to 0.001% or less by weight,” or similarly worded limitations, of the various independent claims. As our reviewing court has held, each claim element must be considered in rejecting any claim and the initial burden is upon the Examiner to set forth a prima facie case for obviousness. See Angstadt, 437 F.2d at 501; Rijckaert, 9 F.3d at 1532. Based on these findings we conclude that the Examiner has not established a prima facie case that the independent claims would have been obvious over Sasaki. Disclosing the claimed starting materials and some of the claimed processing parameters is not enough to establish obviousness of the claimed method(s), as a whole, over the prior art. Therefore, we reverse this rejection. II. Double Patenting The Examiner makes the provisional double patenting rejection over claims 1—28 of U.S. Patent Application No. 13/826,394, which the Examiner finds are patentably indistinct from Appellant’s claim 1. Appellant does not contest the substance of the provisional obviousness-type double patenting rejection, and states “Appellant has previously stated on the record that a terminal disclaimer will be filed once an indication of allowable subject 9 Appeal 2016-000385 Application 13/528,909 matter is received.” App. Br. 13. Under this Board’s precedential decision in Ex parte Moncla, 95 USPQ2d 1884 (BPAI 2010), we decline to address the merits of this rejection. SUMMARY The obviousness rejection over Pazos is reversed. The obviousness rejection over Sasaki is reversed. We decline to address the provisional double patenting rejection. REVERSED 10 Copy with citationCopy as parenthetical citation