Ex Parte LarssonDownload PDFPatent Trial and Appeal BoardJun 27, 201813132974 (P.T.A.B. Jun. 27, 2018) Copy Citation UNITED STA TES p A TENT AND TRADEMARK OFFICE APPLICATION NO. FILING DATE 13/132,974 06/27/2011 21839 7590 06/29/2018 BUCHANAN, INGERSOLL & ROONEY PC POST OFFICE BOX 1404 ALEXANDRIA, VA 22313-1404 FIRST NAMED INVENTOR Mats Larsson UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www .uspto.gov ATTORNEY DOCKET NO. CONFIRMATION NO. 0078834-000010 9429 EXAMINER WU,JENNYR ART UNIT PAPER NUMBER 1733 NOTIFICATION DATE DELIVERY MODE 06/29/2018 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address(es): ADIPDOC 1@BIPC.com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte MATS LARSSON Appeal2017-000373 Application 13/132,974 Technology Center 1700 Before TERRY J. OWENS, JENNIFER R. GUPTA, and JANEE. INGLESE Administrative Patent Judges. OWENS, Administrative Patent Judge. DECISION ON APPEAL STATEMENT OF THE CASE The Appellant appeals under 35 U.S.C. § 134(a) from the Examiner's rejection of claims 7-15 and 18-22. We have jurisdiction under 35 U.S.C. § 6(b). The Invention The Appellant claims a diffusion alloyed powder and an iron-based powder composition containing the diffusion alloyed powder. Claim 7 is illustrative: 7. A diffusion alloyed powder, comprising a total content of copper and nickel of at most 20% by weight, wherein the copper content of the diffusion alloyed powder is above 4.0 wt% and the weight ratio between copper and nickel is between 9/1 and 3/1, said powder consisting of an iron or Appeal2017-000373 Application 13/132,974 iron-based core powder having particles of an average size less than 15 µm of a unitary alloying powder containing copper and nickel, bonded to the surface of core particles of the iron or iron-based core powder. [lJ Takata Semel Singh The References us 5,356,453 us 6,068,813 US 2006/0222554 Al The Rejections Oct. 18, 1994 May 30, 2000 Oct. 5, 2006 The claims stand rejected under 35 U.S.C. § 103 as follows: claims 7, 8, 10-15 and 18-21 over Semel in view of Takata and claim 9 and 22 over Semel in view of Takata and Singh. OPINION We affirm the rejections. The Appellant argues the claims in three groups: 1) claims 7, 8, 10-15 and 19-21, 2) claims 9 and 18, and 3) claim 22 (App. Br. 4--11). We therefore limit our discussion to claim 22 and one claim in each of the other groups, i.e., claims 7 and 9. Claims 8, 10-15 and 19-21 stand or fall with claim 7, and claim 18 stands or falls with claim 9. See 37 C.F.R. § 4I.37(c)(l)(iv) (2012). 1 The Appellant's Specification states: "The term 'unitary powder' in this context designates a powder, the separate particles of which contain both Cu and Ni. Thus, it is not a mixture of powder particles containing Cu and other powder particles containing Ni, but e.g. alloy powder particles comprising both Cu and Ni or complex powder particles where different types of particles are bonded to each other to form complex particles each of which comprises both Cu and Ni" (Spec. 5:30-34). 2 Appeal2017-000373 Application 13/132,974 Claim 7 Semel makes an iron-based metallurgical powder by prealloying iron and molybdenum to form a prealloy powder, mixing the prealloy powder with a copper-containing powder and a nickel-containing powder, and annealing the mixture (col. 3, 1. 60- col. 4, 1. 4). The metallurgical powder's copper-containing powder content preferably is at least 0.5 wt%, more preferably about 0.5 to about 4.0 wt%, and most preferably about 1.0 to about 2.0 wt%, its nickel-containing powder content preferably is at least 0.5 wt%, more preferably about 0.5 to about 8.0 wt%, and most preferably about 1.0 to about 6.0 wt%, and the combined copper-containing powder and nickel-containing powder content is at least about 83 wt% of the metallurgical powder (col. 3, 11. 41-51; col. 9, 11. 9-31). "The copper containing powder has a relatively small weight average particle size that is about 60 microns or less, preferably about 20 microns or less, and more preferably about 15 microns or less. A preferred copper containing powder has a weight average particle size in the range of between about 5 and about 15 microns, preferably between about 9 and about 13 microns" (col. 8, 11. 58---64). "The weight average particle size of the nickel containing powder is preferably about 20 microns or less, and more preferably about 15 microns or less (col. 9, 11. 36-38). Semel believes "prealloying the iron and molybdenum achieves more complete mixing at an atomic level, which results in the final sintered metal part receiving the full benefits of the molybdenum" (col. 6, 11. 54--57), and "by prealloying the iron and molybdenum, the diffusion rates of other alloying powders such as nickel and copper, and the extent to which the alloying powders eventually alloy is increased in comparison to a process where a mixture of iron, molybdenum, 3 Appeal2017-000373 Application 13/132,974 and other alloying powders are diffusion bonded and partially alloyed" ( col. 6, 11. 58---63). Takata discloses "a mixed powder for powder metallurgy based on Fe powder and an alloy powder and capable of providing a sintered product having a high density and high strength and with less scattering in dimensional accuracy upon sintering" ( col. 1, 11. 7-11 ). The alloy powder comprises Ni, Mo, Mn and one or more of Cr, Si, Al, Ti, P, V, Nb, Sn, W, Co, Cu and B (col. 5, 11. 53-56). "[T]he addition amount of such elements should be about 5 to 100 parts based on the 100 parts by weights in total of the basic ingredients such as Ni, Mo and Mn" ( col. 5, 11. 64---66). "However, the addition amount of Cu has to be restricted to less than 10% of the alloy powder since the dimension upon sintering is liable to expand if the addition amount thereof is excessive" ( col. 6, 11. 12-16). The "Ni has an effect of improving the toughness, while Mo improves the hardening property and prevents softening upon hardening and tempering" ( col. 5, 11. 26-28). "Addition of Mn lowers the melting point of the alloy powder, improves the diffusibility of the alloy powder and contributes to the formation of a homogeneous martensite structure developed into a network configuration in a sintered product" ( col. 5, 11. 40-44). The alloying powder can be made by mixing the components and sintering them ( col. 4, 1. 68 - col. 5, 1. 1 ). "[A] sintering powder having a uniform alloying ingredient ratio from a micro point of view can be obtained by using an alloyed powder. Accordingly, the properties of the powder are made constant and the properties of the resulting sintering product also become uniform" (col. 5, 11. 5-10). The Appellant asserts that "Takata discloses that a unitary powder must include nickel, molybdenum (Mo), and Manganese (Mn)" (App. Br. 8), 4 Appeal2017-000373 Application 13/132,974 "Takata teaches specific weight ratios and inclusion of Mo and Mn are needed in a unitary alloying powder (Reply Br. 4--5), and "Takata discloses that a unitary alloyed powder must have a copper content well below the nickel content of the alloyed powder" (App. Br. 9). Takata discloses that "the alloy ingredients such as Ni, Mo and Mn have to be in alloyed form not in the form of individual metal powders" (col. 4, 11. 52-54), but does not disclose that a unitary powder must include Ni, Mo and Mn or must contain more Ni than Cu. Takata's disclosure that prealloying provides a sintering product having uniform characteristics appears to apply to prealloyed powders generally ( col. 4, 1. 62 - col. 5, 1. 10). The disclosed effects of Ni, Mo and Mn do not include enabling formation of a prealloyed powder (col. 5, 11. 26-28, 40-44), and the limitation on the Cu content is to reduce swelling, not to enable prealloyed powder formation (col.6,11.11-16). 2 The Appellant asserts that Semel reduces the Distaloy® AB powder manufacturing cost by using three separate powders (iron based, copper based and nickel based) and combining them to allow for an easier annealing process (App. Br. 6-7), and "the focus of Semel is introducing copper and 2 This interpretation of Takata's disclosure is supported by Singh's disclosures, in the context of copper powder/nickel powder mixtures and prealloyed powders, that "[a]dmixed powders have a major disadvantage over prealloyed powders because they are prone to: a) segregation ( due to the non-uniform composition of components) during transportation and processing; and b) dusting during handling" (i15), "[i]n fully prealloyed powders segregation is not an issue because every particle has the same composition. Dusting is less of a concern due to the absence of very fine particles" (i1 6), and "[p ]arts makers often add nickel to copper-containing steel, because the nickel causes densification, which counteracts the swelling caused by the copper" (i13). 5 Appeal2017-000373 Application 13/132,974 nickel as two separate powders. See, e.g., Semel, column 2 at line 32 to column 3 at line 24" (Reply Br. 3). Semel' s metallurgical powder improvement is due to use of an iron/molybdenum prealloy powder instead of separate iron and molybdenum powders, not to use of separate iron-based, copper-based and nickel-based powders (col. 2, 1. 67-col. 3, 1. 19; col. 3, 1. 60-col. 4, 1. 4; col. 6, 11. 47- 63). Claim 9 Claim 9 depends from claim 1 and requires that "the content of copper is between 5 - 15 wt% and the content of nickel is between 0.5 - 5 wt%." Singh discloses a metallurgical powder made by mixing a diffusion bonded nickel/copper precursor mixture with an iron-based metallurgy master powder to form a powder blend, and consolidating and sintering the powder blend (claim 28). The nickel/copper precursor mixture contains about 1-99 wt% Ni and about 99-1 wt% Cu (claim 31). The Appellant asserts that "there is no teaching in Singh that the copper content of a diffusion alloyed powder should be above 4.0 wt-%" (App. Br. 11). Semel's disclosure that the metallurgical powder's copper content is at least about 0.5 wt%, more preferably about 0.5 to about 4.0 wt% (col. 3, 11. 45--48), would have led one of ordinary skill in the art, through no more than ordinary creativity, to use copper contents somewhat above 4.0 wt%, such as 5 wt% (which appears to include values which round up to 5 wt%, such as 4.6 wt%), which is within the Appellant's 5-15 wt% range. See KSR Int'! Co. v. Teleflex Inc., 550 U.S. 398,418 (2007) (in making an 6 Appeal2017-000373 Application 13/132,974 obviousness determination one "can take account of the inferences and creative steps that a person of ordinary skill in the art would employ"). Claim 22 Claim 22 depends from claim 1 and requires that "the total content of copper and nickel is between 18 - 20% by weight." The Appellant asserts that "Semel requires that the pre-alloy powder (i.e., the iron based powder that the copper containing powder and the nickel containing powder are added to) be at least 83 wt-%. See e.g., lines 49-50 of column 3, or lines 10-11 of column 4" (App. Br. 11 ). Semel' s disclosure that the prealloy powder content is at least about 83 wt% (col. 3, 11. 50-51) would have led one of ordinary skill in the art, through no more than ordinary creativity, to use prealloy powder contents permitted by the term "about," including contents somewhat less than 83 wt%, e.g., 82 wt%, such that the total content of copper and nickel is 18 wt%, which is within the Appellant's 18-20 wt% range. See KSR, 550 U.S. at 418. For the above reasons we are not persuaded of reversible error in the rejections. DECISION The rejections under 35 U.S.C. § 103 of claims 7, 8, 10-15 and 18-21 over Semel in view of Takata and claim 9 and 22 over Semel in view of Takata and Singh are affirmed. The Examiner's decision is affirmed. No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. § 1.136(a). AFFIRMED 7 Copy with citationCopy as parenthetical citation