Ex Parte Kodas et alDownload PDFPatent Trials and Appeals BoardApr 25, 201914285804 - (D) (P.T.A.B. Apr. 25, 2019) Copy Citation UNITED STA TES p A TENT AND TRADEMARK OFFICE APPLICATION NO. FILING DATE 14/285,804 05/23/2014 60601 7590 04/29/2019 Muncy, Geissler, Olds & Lowe, P.C. 4000 Legato Road Suite 310 Fairfax, VA 22033 FIRST NAMED INVENTOR Toivo T. Kodas UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www .uspto.gov ATTORNEY DOCKET NO. CONFIRMATION NO. 4303/0l 45PUS 1 4847 EXAMINER GREENE, NAN A ART UNIT PAPER NUMBER 1619 NOTIFICATION DATE DELIVERY MODE 04/29/2019 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address(es): MAILROOM@MG-IP.COM PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte TOIVO T. KODAS, MARK J. HAMPDEN-SMITH, SCOTT T. HAUBRICH, HENG YU, NED J. HARDMAN, RALPH E. KORNBREKKE, AARON STUMP, KLAUS KUNZE, DAVID DERICOTTE, and KAREL V ANHEUSDEN Appeal 2018-008156 Application 14/285,804 Technology Center 1600 Before JEFFREY N. FRED MAN, DEBORAH KATZ, and JOHN G. NEW, Administrative Patent Judges. FREDMAN, Administrative Patent Judge. DECISION ON APPEAL This is an appeal 1,2 under 35 U.S.C. § 134(a) involving claims to a process for making multi-component particles of inorganic nanoparticles distributed in an organic matrix. The Examiner rejected the claims as 1 Appellants identify the Real Party in Interest as SICP A HOLDING SA (App. Br. 2). 2 We have considered and herein refer to the Specification of May 23, 2014 ("Spec."); Final Office Action of Dec. 22, 2017 ("Final Act."); Appeal Brief of Apr. 27, 2018 ("App. Br."); Examiner's Answer of June 13, 2018 ("Ans."); and Reply Brief of Aug. 9, 2018 ("Reply Br."). Appeal 2018-008156 Application 14/285,804 obvious and under the grounds of obviousness-type double patenting. We have jurisdiction under 35 U.S.C. § 6(b). We reverse. Statement of the Case Background "N anoparticles, and processes for making nanoparticles, have been the subject of recent interest and research because of the advantages provided by nanoparticles over larger sized particulate materials" (Spec. ,-J 3). N anoparticles have a tendency "to agglomerate because of their high surface area and surface energy" (Spec. ,-J 4). "[T]he tendency of nanoparticles to agglomerate makes the forming, processing, handling, transporting and use of nanoparticles difficult" (id.). "Thus, there is a need for additional processes for forming, processing, handling, transporting, dispersing and using nanoparticles" (Spec. ,-J 6). The Claims Claims 55-61, 92-98, and 128-132 are on appeal. Independent claim 55 is representative and reads as follows: 55. A process for making multi-component particles comprising inorganic nanoparticles distributed in an organic matrix, the process comprising the steps of: (a) generating an aerosol comprising droplets, wherein the droplets comprise a liquid vehicle, an inorganic nanoparticle precursor and an organic matrix precursor; and (b) removing at least a portion of the liquid vehicle from the droplets under conditions effective to convert at least a portion of the organic matrix precursor to the organic matrix and to convert at least a portion of the inorganic nanoparticle precursor to the inorganic nanoparticles distributed in the organic matrix. 2 Appeal 2018-008156 Application 14/285,804 (App. Br. 18). The Issues A. The Examiner has rejected claims 55-60, 92-96, and 128-132 under 35 U.S.C. § 103(a) as obvious over Hampden-Smith,3 Kunze,4 and Tong5 (Final Act. 2-12). B. The Examiner has rejected claims 61, 97, and 98 under 35 U.S.C. § 103(a) as obvious over Hampden-Smith, Kunze, Tong, and Flagan6 (Final Act. 12-15). C. The Examiner has rejected claims 55-61, 92-98, and 128-132 on the ground of nonstatutory double patenting as being unpatentable over claims 1-108 of U.S. Patent No. 6,338,809 with Kunze, Tong, and Flagan (Final Act. 23-26). A.-C. Obviousness and Obviousness-type double patenting Because the same issue is dispositive for the all of the rejections, we consider the rejections together. The Examiner finds Hampden-Smith teaches a process for making a particulate product by generating an aerosol including droplets containing a liquid and at least one precursor material, removing at least a portion of the liquid from the droplet, and forming particles of the material (see Final Act. 4-5, citing Hampden-Smith claim 1). The Examiner finds Hampden-Smith teaches making multi-phase particles that include a metallic phase and a 3 Hampden-Smith et al., US 6,338,809 Bl, issued Jan. 15, 2002. 4 Hampden-Smith et al., US 6,193,908 Bl, issued Feb. 27, 2001 5 Tong et al., US 5,536,994, issued July 16, 1996. 6 Flagan et al., US 2002/0098653 Al, published July 25, 2002. 3 Appeal 2018-008156 Application 14/285,804 non-metallic phase (Final Act. 5-6, citing Hampden-Smith 2:25-30). The Examiner finds Hampden-Smith teaches the "particles can include organic coatings such as polymethylmethacrylate (PMMA), polystyrene, or the like" (Final Act. 8, citing Hampden-Smith 45: 1-10). The Examiner acknowledges that Hampden-Smith "does not expressly teach the process results in inorganic nanoparticles distributed in an organic matrix material" (Final Act. 9). The Examiner finds Kunze teaches phosphor nanoparticles dispersed in a polymer matrix (Final Act. 10, citing Kunze 40:54-65). The Examiner determines it would have been obvious to incorporate an organic polymer as a second precursor material in the process in order to produce phosphor nanoparticles in a polymer organic matrix (see Final Act. 11 ). The issue with respect to this rejection is: Does a preponderance of the evidence of record support the Examiner's conclusion that the prior art renders the claims obvious? Findings of Fact ("FF'') 1. Hampden-Smith recites: An aerosol method for making a particulate product ... comprising the steps of: generating an aerosol stream including droplets suspended in a carrier gas ... said droplets are released from a reservoir of an ultrasonically energized flowable medium, said flowable medium comprising a liquid and at least one precursor for a material to be included in the particulate product; removing at least a portion of said liquid from at least a portion of said droplets of said aerosol stream and forming particles including said material (Hampden-Smith 50:19-30 (claim 1)). 4 Appeal 2018-008156 Application 14/285,804 2. Hampden-Smith teaches "[t]he liquid feed 102 may include multiple precursor materials, which may be present together in a single phase or separately in multiple phases" (Hampden-Smith 6:20-22). 3. Hampden-Smith teaches "the multi-phase particles may include an intimate mixture of the first material phase and the second material phase, as in the multi-phase particle 500. Typically, with such an intimate mixture, the first material phase is a continuous phase throughout which the second material phase is dispersed" (Hampden-Smith 40:40-45). 4. Hampden-Smith teaches "[t]he multi-phase particles include a metallic phase and a non-metallic phase ... the non-metallic phase comprises at least one of silica, alumina, titania and zirconia [or] a titanate, such as barium titanate, neodymium titanate or other titanates" (Hampden- Smith 2:25-35). 5. Hampden-Smith teaches "[fJor most phosphor applications, the average particle size is [] preferably from about 0.1 micron to about 4 microns" (Hampden-Smith 44:5-8). 6. Hampden-Smith teaches the phosphor particles can include organic coatings such as PMMA (polymethylmethacrylate ), polystyrene or the like. The organic coating should be on the order of 1 to 100 nanometers thick and be substantially dense and continuous about the particle. Such coatings can be formed after the powders are prepared by a liquid phase process. The organic coatings can advantageously prevent corrosion of the phosphor particles especially in electroluminescent lamps and also can improve the dispersion characteristics of the particles (Hampden-Smith 45: 1-10). 7. Kunze teaches phosphor nanoparticles (Kunze 31 :51-62). 5 Appeal 2018-008156 Application 14/285,804 8. Kunze teaches the phosphor particles can be coated with an organic compound such as PMMA (polymethylmethacrylate ), polystyrene or similar organic compounds, including surfactants that aid in the dispersion and/or suspension of the particles in a flowable medium. The organic coating is preferably not greater than about 100 nanometers thick and is substantially dense and continuous about particle. The organic coatings can advantageously prevent corrosion of the phosphor particles and also can improve the dispersion characteristics of the particles in a paste or other flowable medium (Kunze 35:19-29). 9. Kunze teaches "a phosphor powder/polymer composite 1142 [] sandwiched between two electrodes 1144 and 1146, the front electrode 1144 being transparent. The composite layer 1142 includes phosphor particles 1148 dispersed in a polymer matrix 1150" (Kunze 40:39-65). Principles of Law A prima facie case for obviousness "requires a suggestion of all limitations in a claim," CFMT, Inc. v. Yieldup Int 'l Corp., 349 F.3d 1333, 1342 (Fed. Cir. 2003), and "a reason that would have prompted a person of ordinary skill in the relevant field to combine the elements in the way the claimed new invention does." KSR Int 'l Co. v. Teleflex Inc., 550 U.S. 398, 418 (2007). Analysis Appellants contend "Kunze merely discloses that the inorganic phosphor particles can be coated with an organic coating. According to Kunze, the coating should be performed in a separate step" (App. Br. 12, citing Kunze, 19:43-57; 35:30-46; Figure 33). Appellants contend "[t]his organic coating does not teach or disclose the process of the claimed 6 Appeal 2018-008156 Application 14/285,804 invention," namely generating an aerosol comprising droplets wherein the "droplets comprise a liquid vehicle, an inorganic nanoparticle precursor and an organic matrix precursor" (see id.). As such, Appellants argue "the Examiner fails to specify that the organic precursor is known from Kunze and/or Tong in order to support modifying Hampden-Smith" (App. Br. 14). We find this argument persuasive because the Examiner does not identify any teaching in Hampden-Smith, Kunze, or Tong that suggests "generating an aerosol comprising droplets, wherein the droplets comprise a liquid vehicle, an inorganic nanoparticle precursor and an organic matrix precursor" in order to form inorganic nanoparticles distributed in an organic matrix. That is, claim 55 requires all of the components are present in the same aerosol at the same time, and then both the inorganic nanoparticle precursor and the organic matrix precursor are converted into the final multi- component particle with inorganic particles distributed in the organic matrix. For this reason, we are not persuaded by the Examiner's finding that: The disclosure cited regarding a second coating step is directed to particle exiting the furnace (KUNZE: col. 19, 4th paragraph), and is not excluded by the rejected claims. The disclosure in column 35, 3rd paragraph is not specific to a coating using a separate step. One of ordinary skill in the art would have recognized that the general teaching that "The organic coatings can advantageously prevent corrosion of the phosphor particles [ ... ]" (KUNZE: col. 35, lines 26-27) would have been equally applicable to phosphor nanoparticles dispersed in an organic matrix as the nanoparticles would be dispersed in and thus coated by the organic matrix. (Ans. 9). The citations by the Examiner to Hampden-Smith and Kunze all describe applying an organic material to inorganic nanoparticles as a coating 7 Appeal 2018-008156 Application 14/285,804 after the phosphor nanoparticles are formed. So the aerosol with both precursor components in claim 55 is never formed in these prior art references. Kunze's disclosure of a composite layer including inorganic (phosphor) nanoparticles distributed in an organic (polymer) matrix does not provide the missing teaching of the claimed process (see App. Br. 12). Because the Examiner has not met the initial burden of establishing prima facie obviousness, we reverse the Examiner's rejection. Conclusion of Law The evidence of record does not support the Examiner's conclusion that the prior art renders claim 55 obvious under 35 U.S.C. § 103(a) or obviousness-type double patenting. SUMMARY In summary, we reverse the rejection of claims 55-60, 92-96, and 128-132 under 35 U.S.C. § 103(a) as obvious over Hampden-Smith, Kunze, and Tong. We reverse the rejection of claims 61, 97, and 98 under 35 U.S.C. § 103(a) as obvious over Hampden-Smith, Kunze, Tong, and Flagan. We reverse the rejection of claims 55-61, 92-98, and 128-132 on the ground of nonstatutory double patenting as being unpatentable over claims 1-108 of U.S. Patent No. 6,338,809 with Kunze, Tong, and Flagan. REVERSED 8 Copy with citationCopy as parenthetical citation