Ex Parte Baker et alDownload PDFPatent Trial and Appeal BoardOct 23, 201712089876 (P.T.A.B. Oct. 23, 2017) Copy Citation United States Patent and Trademark Office UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O.Box 1450 Alexandria, Virginia 22313-1450 www.uspto.gov APPLICATION NO. FILING DATE FIRST NAMED INVENTOR ATTORNEY DOCKET NO. CONFIRMATION NO. 12/089,876 04/23/2010 Ian Baker 479964 7217 30955 7590 10/25/2017 T ATHROP ^ GAGV. T T P EXAMINER 4845 PEARL EAST CIRCLE LEE, REBECCA Y SUITE 201 BOULDER, CO 80301 ART UNIT PAPER NUMBER 1734 NOTIFICATION DATE DELIVERY MODE 10/25/2017 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address(es): patent @ lathropgage. com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte IAN BAKER and QI ZENG Appeal 2017-003426 Application 12/089,8761 Technology Center 1700 Before ROMULO H. DELMENDO, KAREN M. HASTINGS, and JAMES C. HOUSEL, Administrative Patent Judges. PER CURIAM. DECISION ON APPEAL STATEMENT OF THE CASE Appellants seek our review under 35 U.S.C. § 134(a) of the Examiner’s decision rejecting claims 1, 3, 5-7, 21, and 24-28, which constitute all the claims pending in this application.2 We have jurisdiction over the appeal under 35 U.S.C. § 6(b). We AFFIRM. 1 According to Appellants, the real party in interest is The Trustees of Dartmouth College. (Appeal Br. 2). 2 Claims 15-20 have been withdrawn from consideration due to a lack of unity of invention in this application filed under 35 U.S.C. § 371. Appeal 2017-003426 Application 12/089,876 Independent claim 1 is illustrative of the subject matter on appeal (emphasis added): 1. An intermetallic composition comprising a mechanically milled nano structured manganese aluminum alloy comprising at least 80% of a nanocrystalline magnetic x phase and having permanent magnetic properties, wherein the alloy has a macroscopic composition of MnxAly, X ranges from 53-56 atomic %, Y ranges from 44-47 atomic%, and the alloy further comprises non-magnetic phases. The Examiner maintains the following rejections: (a) claims 24-28 under 35U.S.C. § 112, first paragraph, as failing to comply with the written description requirement; (b) claims 1, 3, 5-7, 21, and 28 under 35 U.S.C. § 103(a) as unpatentable over Crew et al. (D.C. Crew et al., “MnAl and MnAlC Permanent Magnets Produced by Mechanical Alloying,” 32 Scripta Metallurgica et Materialla 315-318 (1995)) (“Crew”) in view of Ermakov (A.E. Ermakov, et al., “Magnetization Reversal Processing in MnAl-Based Permanent Magnets,” 2 IEEE Transactions on Magnetics 1924-1926 (1988)) (“Ermakov”) and Morisako (A. Morisako et al., “Synthesis of ferromagnetic x phase of MnAl films by sputtering,” 61 J. Appl. Phys.4281- 4283 (1987)) (“Morisako”); (c) claims 24-27 under 35 U.S.C. § 103(a) as unpatentable over Yanagiya (JP 2002-356703 A, published Dec. 13, 2002) (“Yanagiya”) in view of Crew, Ermakov, and Morisako; and 2 Appeal 2017-003426 Application 12/089,876 (d) claims 1, 3, 5-7, 21, and 24-28, provisionally, on the ground of nonstatutory obviousness-type double patenting as being unpatentable over claims 1-5 of Application 13/164,495. ANALYSIS The §112 rejection Claims 24-28 are rejected under 35 U.S.C. § 112, first paragraph, as failing to comply with the written description requirement. The Examiner finds a lack of written description support for the saturation magnetization recited in claim 24 and the coercivity recited in claim 27 (Ans. 2). Claims 24 and 27 The rejections of claims 24 and 27 regard a similar issue because the recitations rejected by the Examiner are directed to numerical ranges that are greater than a minimum value (i.e., saturation magnetization greater than 65 emu/g in claim 24 and coercivity greater than 3.5 kOe in claim 27). Therefore, we address these separately argued claims together. Appellants argue that paragraph 38 of Appellants’ Specification and Figures 13 and 14 of their disclosure support claims 24 and 27 (Appeal Br. 12). The Examiner finds Figure 13 discloses saturation magnetization of 60-80 emu/g and Figure 14 discloses coercivity of 3^1 kOe but not the claimed ranges of greater than 65 emu/g and greater than 3.5 kOe, which include an infinite value (Ans. 10). Appellants respond by contending the Examiner has acknowledged support for saturation magnetization greater than 65 emu/g (e.g., by finding Figure 13 discloses 65-80 emu/g) and acknowledges support for coercivity 3 Appeal 2017-003426 Application 12/089,876 greater than 3.5 kOe (e.g., by finding Figure 14 discloses coercivity of 3—4 kOe) but argue one of ordinary skill in the art would understand that saturation magnetization and coercivity cannot practically have values of infinity (Reply Br. 3—4). In other words, Appellants assert claims 24 and 27 would be limited to practical values of saturation magnetization and coercivity, not infinite values. These arguments are not persuasive because Appellants have not directed us to any evidence of what these practical values for saturation magnetization and coercivity would be. Moreover, claims 24 and 27 do not recite upper limits and therefore encompass values significantly beyond the ranges described and supported in the disclosure, as the Examiner finds. In re Wertheim, 541 F.2d 257, 263-264 (CCPA 1976) (solids contents ranging from 25-60% did not provide written description for “at least 35%”). Therefore, for these reasons and those set forth in the Examiner’s Answer, we sustain the Examiner § 112, first paragraph, rejections of claims 24 and 27. Claims 26 and 28 The rejections of claims 26 and 28 regard a similar issue. Therefore, we address these separately argued claims together. The Examiner finds a lack of written description support for the atomic % of carbon recited in claim 26 (i.e., greater than 0 to 1.0 atomic % carbon) and the annealing temperature recited in claim 28 (i.e., between 350°C to less than 400°C for 10 min) (Ans. 2). Specifically, the Examiner finds the cited passages disclose carbon compositions of 0-3 atomic % and 1-3 atomic % but not the recited range of 0-1 atomic % in claim 26 {id. at 10). The Examiner further finds the cited passages disclose annealing 4 Appeal 2017-003426 Application 12/089,876 temperatures of 350-600°C and 400°C but not the upper limit of less than 400°C recited in claim 28 {id.). A Specification need not disclose the exact range recited in a claim in order to satisfy the written description requirement. See Wertheim, 541 F.2d at 265 (“The PTO has done nothing more than to argue lack of literal support, which is not enough.”); Ralston Purina Co. v. Far-Mar-Co., Inc., 772 F.2d 1570, 1575 (Fed. Cir. 1985) (rejecting the notion that ranges found in the applicant’s claim language must correspond exactly to ranges disclosed in the specification). Rather, a disclosure is sufficient when, as a factual matter, persons skilled in the art would consider the claimed range as part of the appellant’s invention. See Wertheim, 541 F.2d at 265 (“we are of the opinion that, as a factual matter, persons skilled in the art would consider processes employing a 35-60% solids content range to be part of appellants’ invention and would be led by the Swiss disclosure so to conclude.” (specification disclosed range of 25-60% and specific embodiments of 36% and 50% solids content)). Here, the Examiner appears to find a lack of literal support for the ranges recited in claims 26 and 28. The Examiner does not find or explain that one of ordinary skill in the art would not consider the ranges recited in claims 26 and 28 to be part of Appellants’ invention. Appellants argue claim 26 is supported by paragraphs 8, 24, 38, and original claims 2, 4, and 11 because they disclose ranges of 0-3 atomic % carbon and a compositional boundary of 1 atomic % carbon (Appeal Br. 12; Reply Br. 4). Paragraph 8 of Appellants’ Specification and original claims 2, 4, and 11 disclose a carbon composition of 0 to 3 atomic % and paragraph 38 of Appellants’ Specification discusses an atomic % of 1-3 for carbon and 5 Appeal 2017-003426 Application 12/089,876 its effect upon magnetic properties. Therefore, there is a basis for one of ordinary skill in the art to understand that a carbon atomic % of greater than 0 to 1.0 % was part of Appellants’ invention. With regard to claim 28, Appellants contend paragraph 33 supports the claimed range of between 350°C to less than 400°C for 10 minutes (id. ). Paragraph 33 discloses a range of 350°C to 450°C for annealing and an anneal at 400°C.3 Similar to the disclosures relevant to claim 26, this disclosure provides a basis for one of ordinary skill in the art to understand that the range recited in claim 28 was part of Appellants’ invention. In view of the above, we do not sustain the Examiner’s § 112, first paragraph, rejections of claims 26 and 28. The §103 rejection over Crew in view of Ermakov and Morisako Claims 1, 3, 5-7, 21, and 28 are rejected under 35 U.S.C. § 103(a) as unpatentable over Crew in view of Ermakov and Morisako. Upon consideration of the evidence relied upon in this appeal and each of Appellants’ contentions, we find that the preponderance of evidence supports the Examiner’s conclusion that the subject matter of Appellants’ claims 1, 3, 5-7, 21, and 28 are unpatentable over the applied prior art. We sustain the Examiner’s rejections essentially for the reasons set out by the Examiner in the Answer. We add the following primarily for emphasis. 3 Paragraphs 25 and 35 of Appellants’ Specification discloses an anneal at 400°C for 10 minutes. 6 Appeal 2017-003426 Application 12/089,876 Appellants argue claims 1, 5-7, and 21 as a group and claims 3 and 28 as a group (Appeal Br. 4-10). We select claims 1 and 3 as representative claims for these groups. Claims 1, 5-7, and 21 Appellants’ principal argument on appeal is there would not have been a reasonable expectation of success with some degree of predictability to combine Crew, Ermakow, and Morisako, as in the Examiner’s rejection (Appeal Br. 6-8; Reply Br. 6-9). Specifically, Appellants contend the applied references do not disclose a composition comprising 43-56 atomic % Mn and 45—47 atomic % aluminum and at least 80% nanocrystalline x phase, as recited in claim 1, because Crew and Ermakov do not disclose a nanocrystalline phase size, Morisako discloses nanocrystalline x phase for a composition of 60 atomic % Mn and 40 atomic % Al, and it would not have been predictable to apply the sputtering technique of Morisako to the teachings of Crew (Appeal Br. 6-7; Reply Br. 6-8). Appellants further assert the Examiner has not supported a conclusion of obviousness in view of these deficiencies (Appeal Br. 8; Reply Br. 8-9). Appellants’ arguments are unpersuasive. The Examiner finds Crew discloses a nanostructured manganese aluminum alloy having a magnetic x phase (Ans. 3). Crew is directed to MnAl alloys including the ferromagnetic x phase (Crew 315:§ 1 Introduction). For microstructure size, Crew discloses the annealed alloy includes x phase having a grain size similar to that of the e phase prior to annealing, which was 300-500 nm (Crew 3 lb- 317:3.1 Structure). 7 Appeal 2017-003426 Application 12/089,876 Appellants state in Table 1 at pages 6 and 11 of the Appeal Brief that the composition of Crew is “Non-nanocrystalline (400 nm)” and state in footnote 2 at page 11 of the Appeal Brief that “[t]he Office has acknowledged that Crew, et al. do not expressly teach claimed nanocrystalline grain size.” Appellants’ arguments are not persuasive. First, Appellants have not limited “nanocrystalline” in claim 1 to exclude the x phase grain sizes of 300-500 nm disclosed by Crew or otherwise defined nanocrystalline to exclude such grain sizes. Thus, Crew alone may be viewed as disclosing a MnAl alloy including nanocrystalline magnetic x phase as recited in claim 1. Second, the Examiner finds Crew discloses a nanocrystalline x phase for its MnAl alloy (e.g., 400 nm) but not “the claimed nanocrystalline grain size” (Ans. 3). As discussed above, claim 1 does not recite a grain size. It appears the Examiner finds Crew does not disclose the grain size of approximately 30 nm recited in dependent claim 21. To address this, the Examiner finds Ermakov discloses that coercivity depends upon grain size, with smaller grain sizes being preferred (Ans. 3). Ermakov studies the ferromagnetic x phase in MnAl alloys and states coercivity for such alloys strongly depends on its grain size (Ermakov 1924-26). Therefore, the disclosure of Ermakov supports the Examiner’s findings. Moreover, one of ordinary skill in the art would have understood that Ermakov demonstrates the grain size of a MnAl alloy to be a result-effective variable for coercivity of the alloy (see In re Applied Materials, Inc., 692 F.3d 1289, 1297 (Fed. Cir. 2012) (“A recognition in the prior art that a property is affected by the variable is sufficient to find the variable result- effective.”)). As a result, discovery of the optimum or workable ranges for 8 Appeal 2017-003426 Application 12/089,876 grain sizes that produce desirable coercivity values would have been obvious via routine experimentation. Where the general conditions of a claim are disclosed in the prior art, it is not inventive to discover the optimum or workable ranges by routine experimentation {In re Aller, 220 F.2d 454, 456 (CCPA 1955)). In view of the above, the grain size recited in claim 21 would have been obvious over Crew and Ermakov alone. Nonetheless, Morisako further demonstrates the obviousness of the grain size recited in claim 21 by disclosing a MnAl alloy including the x phase can possess a grain size of about 300 angstroms (30 nm) (Morisako 4281 introduction, 4283:Results and Discussion). As noted above, Appellants argue it would not have been predictable to apply the sputtering technique of Morisako to the teachings of Crew (Appeal Br. 6-7). This argument is unpersuasive because the Examiner does not rely upon the incorporation of Morisako’s sputtering technique to achieve the grain size recited in claim 21. Moreover, Morisako is not necessary to demonstrate the obviousness of claim 21 because the combination of Crew and Ermakov is sufficient, as discussed above. With regard to the atomic % ranges recited in claim 1, the Examiner finds Crew discloses a composition of 70 wt% Mn and 30 wt% A1 (Ans. 3). Alloy A in Table 1 at page 316 of Crew discloses this composition. The Examiner finds this composition would convert to an atomic % of approximately 54 atomic % Mn and 46 atomic % A1 (id.). Appellants do not dispute the Examiner’s finding (Appeal Br. 6). For the recitation of the composition “comprising at least 80% of a nanocrystalline magnetic x phase,” as recited in claim 1, the Examiner finds the composition of Crew comprises substantially the x phase (Ans. 3). The 9 Appeal 2017-003426 Application 12/089,876 disclosure of Crew supports this finding because Crew discloses that when its Mn-Al alloy was milled, annealed, heat treated at 1050°C, quenched, and then aged at 600°C for 10 minutes, which “caused the remaining c phase to transform to the x phase” and x-ray diffraction showed “a small amount of (3 phase was also formed during ageing” (Crew 316-317:3.1 Structure). As shown in Figure 1, curve (d), which corresponds to the aged sample, the alloy is almost entirely the x phase. In view of the above, Appellants’ arguments that the applied references do not disclose or suggest a nanostructured Mn-Al alloy comprising at least 80% of a nanocrystalline magnetic x phase, as recited in claim 1, are unpersuasive. As a result, Appellants have not identified a reversible error in the Examiner’s § 103(a) rejection of claim 1. Claims 3 and 28 For claims 3 and 28, Appellants refer to the arguments set forth for claim 1 above (Appeal Br. 9-10). As discussed above with regard to claim 1, these arguments do not identify a reversible error in the Examiner’s rejection. Appellants further contend claims 3 and 28 recite a combination of features not disclosed or suggested by the applied references, specifically “forming at least 80% of a nanocrystalline magnetic x phase in the specified composition range by annealing a solid which has been milled to form a nanocrystalline e phase” (Appeal Br. 10; Reply Br. 9). For the reasons discussed above and in the Examiner’s Answer, the applied references disclose a Mn-Al alloy that is milled and annealed so it has at least 80% nanocrystalline magnetic x phase in the claimed compositional range, as recited in claim 1 (which claim 3 depends from). We further note claim 3 10 Appeal 2017-003426 Application 12/089,876 recites “milling the crushed solid to form a nanocrystalline c phase” and “annealing the milled solid to form the nanocrystalline magnetic x phase.” Therefore, claim 3 does not require the composition to include the c phase with the x phase after annealing. As discussed above, Crew discloses annealing a MnAl alloy to provide a nanocrystalline x phase. In addition, the Examiner finds the process limitations set forth in claims 3 and 28 are product-by-process limitations and Appellants have not demonstrated that applied references would result in a different product (Ans. 4). The prior art and claimed products appear to be the same, and we agree that Appellants’ arguments do not demonstrate that the applied references would produce a different product than that recited in claims 3 and 28. For the reasons discussed above and those set forth in the Examiner’s Answer, we sustain the Examiner’s § 103(a) rejection of claims 1,3, 5-7, 21, and 28 over Crew in view of Ermakov and Morisako. The §103 rejection over Yanagiya in view of Crew, Ermakov, and Morisako Claims 24-27 are rejected under 35 U.S.C. § 103(a) as unpatentable over Yanagiya in view of Crew, Ermakov, and Morisako. For the rejection of claims 24-27, Appellants contend the combination of the applied references fails to provide a reasonable expectation that would successfully and predictably arrive at the claimed composition (Appeal Br. 11-12; Reply Br. 10-11). In particular, Appellants argue the references do not disclose nanocrystalline x phase for the Mn-Al-C composition recited in claim 24 {id.). 11 Appeal 2017-003426 Application 12/089,876 These arguments are unpersuasive. As discussed above, Crew discloses a magnetic composition that includes nanocrystalline x phase. Crew further discloses “[t]he addition of carbon to the alloy stabilizes the x phase against decomposition [3] and improves both the magnetic properties and ductility” (Crew 315:§ 1 Introduction). Thus, Crew discloses carbon addition to be a result-effective variable for the stabilization of the x phase, magnetic properties, and ductility. As a result, it would have been obvious to modify the 70 wt% Mn, 30 wt% A1 alloy of Crew (which the Examiner converts to approximately 54 atomic % Mn and 46 atomic % A1 (Ans. 3)) to include carbon in some amount greater than 0, as recited in claim 24, to determine the optimal or workable ranges for a composition that includes stabilized x phase as well as excellent magnetic properties and ductility. Nonetheless, the Examiner finds Yanagiya discloses a magnetic alloy composition including 68-73 wt% Mn, 0.2-2.1 wt% C, and balance aluminum, which overlaps the claimed composition for atomic % (Ans. 5). Yanagiya discloses this composition in its abstract and thus supports the Examiner’s finding. The Examiner finds Yanagiya does not disclose that the composition is nanostructured, includes the x phase, and a non-magnetic phase (e.g., P phase) {id.). However, Crew discloses these recitations, as discussed above with regard to the rejection of claim 1, and the Examiner provides a rationale to modify Yanagiya in view of Crew {id.). Like claim 1, claim 24 also does not specify a grain size value. As a result, the combination of Yanagiya and Crew also demonstrates the obviousness of the composition of claim 24 and Appellants’ arguments do not identify a reversible error in the Examiner’s rejection. 12 Appeal 2017-003426 Application 12/089,876 In the Reply Brief, Appellants argue the proposed modification of Yanagiya in view of Crew, Ermakov, and Morisako would have changed the principle of operation of Yanagiya’s anisotropic magnet or rendered it unsuitable for its intended purpose (Reply Br. 12-13). Appellants have not shown good cause why these arguments could not have been presented in the Appeal Brief.4 Therefore, we will not consider these arguments that were newly raised in the Reply Brief. 37 C.F.R. § 41.41(b)(2). Nonetheless, even if these arguments had been timely submitted, our analysis would have remained the same because Appellants merely submit attorney arguments that the material of Yanagiya would lose anisotropy after the modification. Appellants do not direct us to any evidence demonstrating that the material of Yanagiya would no longer be anisotropic after such a modification. For the reasons discussed above and those set forth in the Examiner’s Answer, we sustain the Examiner’s § 103(a) rejection of claims 24-27 over Yanagiya in view of Crew, Ermakov, and Morisako. Provisional Obviousness-Type Double Patenting Rejection Claims 1,3, 5-7, 21, and 24-28 are provisionally rejected on the ground of nonstatutory obviousness-type double patenting as being unpatentable over claims 1-5 of Application 13/164,495. Appellants do not submit arguments regarding the propriety of the rejection, other than to state the rejection “will be addressed upon resolution of the rejections under appeal” and that the claims cited in Application 4 To the extent Appellants would assert this argument is in response to the Examiner’s finding that Appellants have not shown that the modification “would have upset the composition of Crew” (Ans. 9), the Examiner previously made this finding at page 12 of the Final Office Action. 13 Appeal 2017-003426 Application 12/089,876 13/164,495 are withdrawn from consideration (Appeal Br. 13). We therefore summarily affirm the Examiner’s non-statutory obviousness-type double patenting rejection of claims 1,3, 5-7, 21, and 24-28. DECISION On the record before us, we: A. sustain the Examiner’s decision to reject claims 24 and 27 under 35 U.S.C. § 112, first paragraph, as failing to comply with the written description requirement; B. do not sustain the Examiner’s decision to reject claims 26 and 28 under 35 U.S.C. § 112, first paragraph, as failing to comply with the written description requirement; C. sustain the Examiner’s decision to reject claims 1, 3, 5-7, 21, and 28 under 35 U.S.C. § 103(a) as unpatentable over Crew in view of Ermakov and Morisako; D. sustain the Examiner’s decision to reject claims 24-27 under 35 U.S.C. § 103(a) as unpatentable over Yanagiya in view of Crew, Ermakov, and Morisako; and E. sustain the Examiner’s decision to provisionally reject claims 1, 3, 5-7, 21, and 24-28 on the ground of nonstatutory obviousness-type double patenting over claims 1-5 of Application 13/164,495. The decision of the Examiner is affirmed. No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. § 1.136(a)(l)(iv). AFFIRMED 14 Copy with citationCopy as parenthetical citation