Ex Parte Antoine et alDownload PDFPatent Trial and Appeal BoardFeb 25, 201914288986 (P.T.A.B. Feb. 25, 2019) Copy Citation UNITED STA TES p A TENT AND TRADEMARK OFFICE APPLICATION NO. FILING DATE 14/288,986 05/28/2014 22928 7590 02/27/2019 CORNING INCORPORATED SP-TI-3-1 CORNING, NY 14831 FIRST NAMED INVENTOR Keisha Chantelle Ann Antoine UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www .uspto.gov ATTORNEY DOCKET NO. CONFIRMATION NO. SP13-184 9202 EXAMINER FRANKLIN, JODI COHEN ART UNIT PAPER NUMBER 1741 NOTIFICATION DATE DELIVERY MODE 02/27/2019 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address(es): usdocket@corning.com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte KEISHA CHANTELLE ANN ANTOINE, PO-HAO KAO, and CLAIRE JEANNETTE WARREN GINN AN Appeal2017-006284 Application 14/288,986 Technology Center 1700 Before LINDA M. GAUDETTE , JEFFREY W. ABRAHAM , and CHRISTOPHER L. OGDEN, Administrative Patent Judges. GAUDETTE, Administrative Patent Judge. DECISION ON APPEAL 1 1 This Decision includes citations to the following documents: Specification filed May 28, 2014 ("Spec."); Final Office Action dated May 5, 2016 ("Final"); Appeal Brief filed Sept. 30, 2016 ("Appeal Br."); Examiner's Answer dated Jan. 13, 2017 ("Ans."); and Reply Brief filed Mar. 10, 2017("Reply Br."). Appeal2017-006284 Application 14/288,986 The Appellant2 appeals under 35 U.S.C. § 134(a) from the Examiner's decision finally rejecting claims 11-20. We have jurisdiction under 35 U.S.C. § 6(b ). We AFFIRM. The invention relates to methods of mixing multi-component, molten, ion exchange baths used in ion exchange systems for glass, glass-ceramic, and ceramic articles. Spec. ,r 2. Claim 11, the sole independent claim on appeal, is reproduced below. 11. A method of maintaining an ion exchange bath, comprising the steps: providing a substrate having an outer region containing a plurality of substrate metal ions; preparing an ion exchange bath that includes a first metal salt having a plurality of first metal ions at a first metal ion concentration and a second metal salt having a plurality of second metal ions at a second metal ion concentration; providing a vessel for containing the ion exchange bath and the substrate; submersing the substrate in the ion exchange bath such that a portion of the plurality of substrate metal ions is exchanged with a portion of the plurality of first metal ions; and mixing the bath such that the first metal ion concentration in the bath is uniform throughout the vessel, and wherein the first and second metal salts are miscible and molten. Appeal Br. 20 (Claims Appendix). The Examiner relies on the following references as evidence of unpatentability: 2 The Appellant, Coming Incorporated, is the applicant under 3 7 C.F .R. § 1.46, and is also identified as the real party in interest. See Appeal Br. 3. 2 Appeal2017-006284 Application 14/288,986 Roemer Cornejo Murata Wang '715 Wang '338 US 2010/0199720 Al US 2011/0293942 Al US 2012/0196110 Al US 2013/0202715 Al W0/2011/069338 Al Aug. 12, 2010 Dec. 1, 2011 Aug. 2, 2012 Aug. 8, 2013 June 16, 2011 The Examiner maintains the following grounds of rejection on appeal (see Ans. 2---6): 1. claims 11-14, 16, and 17 under 35 U.S.C. § 103 as unpatentable over Cornejo; 2. claims 13-15 under 35 U.S.C. § 103 as unpatentable over Cornejo in view of Wang; 3. claims 18 and 19 under 35 U.S.C. § 103 as unpatentable over Cornejo in view of Murata; and 4. claim 20 under 35 U.S.C. § 103 as unpatentable over Cornejo in view of Roemer. Rejection of claims 11-14, 16, and 17 as unpatentable over Cornejo Claim 11 The Examiner finds Cornejo discloses the invention as recited in claim 11, with the exception that Cornejo does not disclose explicitly that the mixing step results in a uniform, first metal ion concentration throughout the vessel. Final 3--4. The Examiner finds, however, that Cornejo discloses mixing the bath with the same types of devices used in the present invention in order to "increase the rate of dissolution of the first metal salt into the ion exchange bath and drain[] areas enriched with a particular cation to restore a chemical balance." Id. at 3 (citing Cornejo ,r,r 35, 38). The Examiner determines Cornejo's mixing step necessarily would result in a uniform first metal ion concentration as claimed. Id. at 3--4. The Appellant argues Cornejo discloses mixing the bath to increase turbulent flow or flow perturbation. Appeal Br. 11. The Appellant argues this type 3 Appeal2017-006284 Application 14/288,986 of mixing would increase "convective movement, transport and flow of the molten salt, but do nothing to limit the differences in density and concentrations of the molten salt due to the temperature differences." Id. The Appellant's argument is not persuasive for the reasons discussed below. The Specification discloses embodiments wherein an impeller, or a sparging assembly configured to bubble inert gas, is used "to agitate, mix and/or otherwise move" a bath within a vessel to ensure concentrations of the salts are substantially uniform throughout the vessel. Spec. ,r,r 43, 49. According to the Specification, the duration of impeller operation "can be based on predetermined time periods that have been calculated based on prior-obtained empirical test data," id. ,r 44, and various inputs, such as gas feed rate and pressure, that can be empirically determined to optimize reduction in stratification in the bath, id. ,r 50. However, there are no examples or other disclosures of the specific time periods or inputs that result in uniformity of salt concentration throughout the vessel. The Specification discloses an embodiment wherein vertical movement of a mixing frame assembly causes cavitation within the bath, thereby generating turbulence to reduce stratification and concentration non-uniformity. Id. ,r 56. The Specification also discloses an embodiment wherein an agitator assembly is used to minimize stratification and concentration non-uniformity within an ion exchange bath. Id. ,r 62. Cornejo discloses that temperature gradients in an ion exchange bath give rise to differences in density and concentrations of molten salt in the bath. Cornejo ,r 35. To address this issue, Cornejo teaches increasing turbulent flow or flow perturbation in the ion exchange bath by internal or external means, including bubbles, stirrers, screws or other known devices for agitating fluid. Id.; cf Final 4 (citing Cornejo ,r 35 as evidence ofunpatentability of claims 16 and 17). Thus, 4 Appeal2017-006284 Application 14/288,986 although Cornejo does not state expressly that the bath should be mixed so as to achieve a uniform first metal ion concentration throughout the vessel, the Examiner had a reasonable basis for finding that Cornejo's method necessarily would result in a bath having a first metal ion concentration that is uniform throughout the vessel. This is because Cornejo utilizes the same techniques to increase flow in the bath as described in the Specification, and is concerned with eliminating differences in concentrations of molten salt throughout the bath. Therefore, the burden was shifted to the Appellant to prove that the bath in Cornejo's method would not necessarily contain a first metal ion concentration that was uniform throughout the vessel. See In re Best, 562 F.2d 1252, 1255 (CCPA 1977) ("Where, as here, the claimed and prior art products are identical or substantially identical, or are produced by identical or substantially identical processes, the PTO can require an applicant to prove that the prior art products do not necessarily or inherently possess the characteristics of his claimed product."). We agree with the Examiner that the Appellant has not met this burden. See Ans. 7-8. Claim 12 The Appellant argues Cornejo fails to disclose that "the step of mixing the bath is also conducted to increase the rate of dissolution of the first metal salt into the ion exchange bath" (claim 12). Appeal Br. 12. As discussed in connection with claim 11, the Appellant has not provided persuasive evidence to refute the Examiner's finding that the claimed and prior art methods are substantially the same and, therefore, necessarily would produce ion exchange baths having the same properties. See Ex parte Obiaya, 227 USPQ 58, 60 (BP AI 1985) ("The fact that appellant has recognized another advantage which would flow naturally from following the suggestion of the prior art cannot be the 5 Appeal2017-006284 Application 14/288,986 basis for patentability when the difference would otherwise have been obvious."). In addition, claim 12, as drafted, merely recites an intended result of the mixing step, but does not require that mixing effect an actual increase in rate of dissolution. Claims 13 and 14 The Appellant argues the Examiner fails to identify a teaching or suggestion to select first and second metal salts that differ in density by at least 25% as required by claim 13, or to select silver nitrate and potassium nitrate as required by claim 14. Appeal Br. 12-13. Cornejo discloses that "the ion exchange bath comprises ... at least one alkali metal salt such as ... nitrates, sulfates, and halides of sodium and potassium" and "may also include salts of other monovalent metals ( e.g., Ag+, Tl+, Cu+, or the like)." Cornejo ,r 25. Thus, although Cornejo's disclosure of suitable salts may be broad, see Appeal Br. 13, we agree with the Examiner that Cornejo explicitly identifies, and therefore provides direction, to select silver nitrate and potassium nitrate, see Ans. 8. The Appellant has not shown error in the Examiner's finding that the difference in density between these two salts is greater than 25%. See Final 8. Rejection of claims 13-15 as unpatentable over Cornejo in view of Wang The Appellant contends Wang fails to cure the deficiencies in the Examiner's rejection of claims 13 and 14 based on Cornejo alone. Appeal Br. 15. This argument is not persuasive for the reasons discussed above. The Appellant also argues the Examiner has not provided the requisite articulated reasoning with rational underpinning to explain why the ordinary artisan would have combined Cornejo and Wang. Id. This argument is not persuasive because it fails to identify error in the Examiner's finding that the 6 Appeal2017-006284 Application 14/288,986 ordinary artisan would have modified the amount of silver nitrate in Cornejo's bath based on Wang's teaching that that presence of silver nitrate in amounts that overlap the claimed range provides antimicrobial properties. See Final 6. Rejection of claims 18 and 19 as unpatentable over Cornejo in view of Murata and Rejection of claim 20 as unpatentable over Cornejo in view of Roemer The Examiner has fully addressed the arguments advanced by the Appellant in support of patentability of claims 18-20, and we agree that these arguments are unpersuasive for the reasons stated in the Answer. See Appeal Br. 15-18; Reply Br. 3--4; Ans. 9-11. We add that the Appellant's arguments fail to address the facts and reasons relied on by the Examiner in determining claims 18-20 are unpatentable under 35 U.S.C. § 103. As found by the Examiner, "Cornejo discloses mixing the molten salt bath by any stirring means known in the art of stirring fluids." Final 6-7; see Cornejo ,r 35 ("[T]urbulent flow or flow perturbation in ion exchange bath 100 may be increased by either internal or external means ... for agitating fluid that are known in the art."). Cornejo is concerned with eliminating differences in concentrations of molten salt throughout the bath. Cornejo ,r 35. The Appellant has not explained persuasively why the Examiner erred in finding that the ordinary artisan would have utilized a basket as taught in Murata or a separate stirring section as taught by Roemer, i.e., known means for agitating fluid, as the means for providing turbulent flow or flow perturbation in Cornejo in order to eliminate differences in concentrations of molten salt throughout the bath. See Final 6-8. In sum, for the reasons stated in the Final Office Action, the Answer, and above, we are not persuaded of reversible error in the Examiner's conclusion of obviousness as to claims 11-20. We sustain all four grounds of rejection. 7 Appeal2017-006284 Application 14/288,986 No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. § 1.136(a)(l )(iv). AFFIRMED 8 Copy with citationCopy as parenthetical citation