Ex Parte 7279018 et alDownload PDFBoard of Patent Appeals and InterferencesMar 22, 201290010549 (B.P.A.I. Mar. 22, 2012) Copy Citation UNITED STATES PATENT AND TRADEMARK OFFICE UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www.uspto.gov APPLICATION NO. FILING DATE FIRST NAMED INVENTOR ATTORNEY DOCKET NO. CONFIRMATION NO. 90/010,549 05/22/2009 7279018 11202.0002-00 5242 22852 7590 03/22/2012 FINNEGAN, HENDERSON, FARABOW, GARRETT & DUNNER LLP 901 NEW YORK AVENUE, NW WASHINGTON, DC 20001-4413 EXAMINER LOPEZ, CARLOS N ART UNIT PAPER NUMBER 3991 MAIL DATE DELIVERY MODE 03/22/2012 PAPER Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE ____________ BEFORE THE BOARD OF PATENT APPEALS AND INTERFERENCES ____________ Ex parte Neste Oil Oyj, Patent Owner and Appellant ____________ Appeal 2012-002608 Reexamination Control 90/010,549 Patent 7,279,018 B2 Technology Center 3900 ____________ Before ROMULO H. DELMENDO, JEFFREY B. ROBERTSON, and RAE LYNN P. GUEST, Administrative Patent Judges. ROBERTSON, Administrative Patent Judge. DECISION ON APPEAL Appeal 2012-002608 Reexamination Control 90/010,549 Patent 7,279,018 B2 2 Neste Oil Oyj, the owner of Patent 7,279,018 B2 under reexamination (hereinafter the “‘018 Patent”), appeals under 35 U.S.C. §§ 134(b) and 306 from a final rejection of claims 1-6 (Appeal Brief filed July 6, 2011, hereinafter “App. Br.,” at 10; Final Office Action mailed January 7, 2011). We have jurisdiction under 35 U.S.C. §§ 134(b) and 306. We AFFIRM. STATEMENT OF THE CASE This reexamination proceeding arose from a third-party request for ex parte reexamination filed by Todd D. Mattingly, of Bracewell & Giuliani LLP (Request for Ex Parte Reexamination filed May 22, 2009). The ‘018 Patent relates to fuel compositions for diesel engines. (Col. 1, ll. 5-10.) Claim 1 on appeal reads as follows (underlining and bracketing show additions and subtractions, respectively, relative to the original claims of the ‘018 patent): 1. A fuel composition for diesel engines [comprising] consisting of: a) 0.1-99% by volume of a component or a mixture of components, which are free of aromates and suitable for a diesel fuel, produced from biological raw material originating from animals or originating from both plants and animals by hydrogenating and decomposing fatty acids and/or fatty acid esters to give hydrocarbons and isomerizing the hydrocarbons to give isoparaffins; b) 0-20% by volume of components containing oxygen selected from the group consisting of aliphatic alcohols, ethers, fatty acid esters, water and mixtures containing the same; Appeal 2012-002608 Reexamination Control 90/010,549 Patent 7,279,018 B2 3 both components a) and b) being mixed as an emulsion with or dissolved in diesel components based on crude oil and/or fractions from Fischer-Tropsch process. (Claims App’x, App. Br. 21.) The Examiner relied upon the following as evidence of unpatentability (Examiner’s Answer mailed August 12, 2011, hereinafter “Ans.,” 3): Monnier US 5,705,722 Jan. 6, 1998 Nylund WO 95/25152 Sep. 21, 1995 Neste Oy SE 9700149 Aug. 6, 1997 (English Translation of Record, hereinafter “SE ‘149”) Appellant relied on certain parts of the following (App. Br. 23): Decl. of Pekka Aalto dated March 23, 2010 (hereinafter “the Aalto Declaration”). REJECTION The Examiner rejected claims 1-6 under 35 U.S.C. § 103(a) as obvious over Monnier in view of Nylund and SE ‘149. (Ans. 3-5.) ISSUE The Examiner found that Monnier discloses the components recited in claim 1, with the exception that Monnier does not disclose that the hydrocarbons derived from animal materials corresponding to component a) are isomerized as recited in claim 1. (Ans. 3-4.) The Examiner found that because Nylund discloses that all bio-oils are structurally similar, and that Appeal 2012-002608 Reexamination Control 90/010,549 Patent 7,279,018 B2 4 SE ‘149 discloses isomerizing vegetable oils in order to improve low temperature properties in diesel fuels, it would have been obvious to isomerize the hydrocarbons derived from the animal materials disclosed in Monnier. (Ans. 4-5.) Appellant contends that Monnier does not disclose that the hydrocarbons corresponding to component a) are free of aromates and suitable for a diesel fuel as required by the claims. (App. Br. 15-18.) For support, Appellant points to the Aalto Declaration, which purports to reproduce Monnier’s examples to show that the hydrocarbons produced therein include aromates and are unsuitable for diesel fuel additives. (App. Br. 16-18.) Appellant also contends that Monnier is non-enabling because the reproduced examples in the Aalto Declaration do not yield the values disclosed in Monnier. (App. Br. 19.) Appellant further argues that there is no reason to modify Monnier because Monnier is directed to high cetane number additives, and it is well known that isomerization reduces cetane number. (App. Br. 18.) Thus, the principal issue in this appeal is: Does the evidence of record as a whole support the Examiner’s conclusion that the fuel composition as claimed would have been obvious to one of ordinary skill in the art in view of Monnier, Nylund, and SE ‘149? FINDINGS OF FACT (“FF”) 1. The ‘018 Patent discloses: “The properties of the diesel fuel composition of biological origin according to the invention correspond to those of a high quality diesel fuel based on crude Appeal 2012-002608 Reexamination Control 90/010,549 Patent 7,279,018 B2 5 oil, it is free of aromates and, in contrast to FAME [fatty acid methyl ester], it leaves no impurity residues.” (Col. 5, ll. 1-5.) 2. The ‘018 Patent does not expressly describe the conditions used to hydrogenate and isomerize the biological raw materials in producing isoparaffins. 3. Monnier discloses additives for diesel fuels having high cetane number derived from biomass feedstocks including animal fats. (Col. 1, ll. 10-13, 58-67.) 4. Monnier discloses that the biomass feedstock is subjected to hydroprocessing at temperatures of at least 350 ºC, where the hydrogen pressure can vary widely between about 4 MPa and 15 MPa and the liquid hourly space velocity (LHSV) can vary widely between 0.5-5.0 hr-1. (Col. 2, ll. 44-63.) 5. SE ‘149 discloses a process where fatty acids or triglycerides of a vegetable oil are hydrogenated to give n-paraffins, which are then converted to paraffins with branched chains and used as components for diesel fuels. (P. 2, ll. 15-24.) 6. SE ‘149 discloses that the n-paraffins are isomerized so as to retain favorable properties such as high cetane number. (P. 3, ll. 13-19, p. 5, ll. 15-16.) 7. SE ‘149 discloses that the products may be free of aromatics. (P. 5, l. 6.) 8. SE ‘149 discloses that the isomerization takes place at a temperature from 200 to 500 ºC. (P. 4, l. 21.) Appeal 2012-002608 Reexamination Control 90/010,549 Patent 7,279,018 B2 6 9. In reproducing Monnier Example 5, the Aalto Declaration notes the following differences between reproduced example and the Example 5: the animal tallow employed is from Tyson Foods, Inc. rather than animal tallow from West Coast Reduction Ltd.; the hydrogen pressure was varied; and dimethyl sulfide was used for spiking instead of CS2. The Aalto Declaration characterizes such differences as insignificant. (Para. 1.2.) 10. The Aalto Declaration produces two examples that allegedly reproduced Example 5 of Monnier at temperatures of 370 and 369 ºC, hydrogen pressures of 80 and 82 bar, and 1.0 and 1.1 h- 1 liquid space velocity, designated as “Monnier Example 5 HDO A” and “Monnier Example 5 HDO B,” respectively. (Para. 1.2.) 11. The Aalto Declaration states that in producing a hydrogenated product of animal tallow from Tyson Foods, Inc. according to the ‘018 Patent, the temperature was decreased by 60 degrees C (370 ºC v. 310 ºC), and the pressure was decreased by 31 bar (80 bar v. 49 bar), where the conditions take into account the starting material used in the process. (Para. 1.3, FN 1.) ANALYSIS The Examiner’s position is that because claim 1 is directed to a composition and includes “diesel components based on crude oil and/or fractions from Fischer-Tropsch process,” whether component a) is initially Appeal 2012-002608 Reexamination Control 90/010,549 Patent 7,279,018 B2 7 free of aromates is irrelevant as the diesel components recited in the claims may contain aromates, such that the composition as a whole may contain aromates. (Ans. 7-9.) Appellant contends that in order for the prior art to teach or suggest the claimed compositions, at some point, each of the claimed components must be present, including component a), which is free of aromates. (App. Br. 13-14, Reply Brief filed October 11, 2011, hereinafter (Rep. Br.” at 1-3, citing Exxon v. Lubrizol, 64 F.3d 1553, 1558 (Fed. Cir. 1995).) We essentially agree with the Examiner that the claims are directed to the composition, which may include aromates as a result of containing diesel components based on crude oil and/or fractions from Fischer-Tropsch process. Accordingly, we do not agree that the recitation that component a) is free of aromates distinguishes the prior art. However, even if we assume that Appellant’s claim construction is correct, we are not persuaded by Appellant’s evidence that the hydrogenated animal tallows disclosed in Monnier would necessarily contain aromates or that preparing hydrocarbons free of aromates would not have been obvious to one of ordinary skill in the art. Specifically, Monnier discloses that the hydroprocessing temperature may be as low as 350 ºC and that the hydrogen pressure and liquid hourly space velocity may vary quite widely. (FF 4.) Thus, the examples allegedly reproduced from Monnier test one similar set of conditions, and are not reflective of Monnier’s entire disclosure. (FF 9, 10.) In addition, the only identified differences between Appellant’s reproduced examples of Monnier and the inventive hydrogenated product Appeal 2012-002608 Reexamination Control 90/010,549 Patent 7,279,018 B2 8 appear to be the conditions used to hydrogenate the starting animal tallow. (FF 11.) Thus, it appears that the process conditions (temperature, pressure, liquid hourly space velocity) control whether aromates are produced in the hydrogenation reaction. As discussed above, Monnier discloses hydroprocessing temperatures as low as 350 ºC, which lies between the temperatures of Appellant’s reproduced examples of Monnier and the temperatures used to produce the hydrogenated product according to the ’018 Patent. (FF 9-11.) We have not been directed to sufficient evidence that at a temperature of 350 ºC, or at other pressures and liquid hourly space velocities, the hydrogenated products would contain aromates. Moreover, although Appellant contends that SE ‘149 recommends isomerization temperatures of about 330 ºC, SE ‘149 discloses a broad range of between 200-500 ºC, which does not require a “higher operating temperature” as argued by Appellant. (App. Br. 16; FF 8.) Further, SE ‘149 discloses that hydrogenated products may be free of aromatics. (FF 5, 7.) Thus, since Appellant does not identify any particular process conditions in the ‘018 Patent (FF 2), we presume that one of ordinary skill in the art would have been capable of adjusting the process conditions in order to obtain a hydrogenated product free of aromates as suggested by SE ‘149. We are also not persuaded by Appellant’s argument that Monnier’s products are unacceptable for diesel fuel compositions in view of the experimental results obtained in the Aalto Declaration. Monnier expressly discloses the use of fuel additives for diesel fuel. (FF 3.) SE ‘149 also discloses that the isomerized products are useful for diesel fuel additives. (FF 5.) Appellant acknowledges that the reproduced examples from Appeal 2012-002608 Reexamination Control 90/010,549 Patent 7,279,018 B2 9 Monnier differ from the actual examples disclosed therein, but asserts that such differences are insignificant. (Aalto Declaration, para. 1.2.) However, in reviewing the results of the reproduced examples, we observe that by varying the temperature by one degree, the hydrogen pressure by 2 bar, and the liquid space velocity by 0.1 h-1, the resulting products produce different results between “Monnier Example 5 HDO A” and “Monnier Example 5 HDO B” with respect to boiling point distribution, cloud point, and cloud point of isomerized products. (FF 10; Aalto Declaration, Examples 2, 4, and 6.) The Aalto Declaration does not explain why the noted differences in starting materials and conditions would have been insignificant, given that very slight changes in conditions produce varying results. Accordingly, we do not find Appellant’s experimental results persuasive in determining whether Monnier’s additives are suitable for diesel fuels. For similar reasons, we do not subscribe to Appellant’s view that Monnier is non-enabling because the results of the allegedly reproduced examples of Monnier are not consistent with the results reported in Monnier. We are also not persuaded that one of ordinary skill in the art would not have been motivated to isomerize the hydrocarbons produced in Monnier, because Monnier discloses additives with high cetane number. SE ‘149 expressly discloses that isomerization may take place while retaining favorable properties such as high cetane number. (FF 6.) Accordingly, we find that the evidence of obviousness of record outweighs the evidence presented by Appellant. Appeal 2012-002608 Reexamination Control 90/010,549 Patent 7,279,018 B2 10 CONCLUSION On this record, the evidence of record as a whole supports the Examiner’s conclusion that the fuel composition as claimed would have been obvious to one of ordinary skill in the art in view of Monnier, Nylund, and SE ‘149. DECISION The Examiner’s decision to reject claims 1-6 under 35 U.S.C. § 103(a) is affirmed. Requests for extensions of time in this ex parte reexamination proceeding are governed by 37 C.F.R. § 1.550(c). See 37 C.F.R. § 41.50(f). AFFIRMED Appeal 2012-002608 Reexamination Control 90/010,549 Patent 7,279,018 B2 11 FOR PATENT OWNER: FINNEGAN, HENDERSON, FARABOW, GARRETT & DUNNER LLP 901 NEW YORK AVENUE, NW WASHINGTON, DC 20001-4413 FOR THIRD-PARTY REQUESTER: BRACEWELL & GIULIANI LLP P.O. BOX 61389 HOUSTON, TX 77208-1389 Copy with citationCopy as parenthetical citation