Arno Refke et al.Download PDFPatent Trials and Appeals BoardApr 1, 202012418014 - (D) (P.T.A.B. Apr. 1, 2020) Copy Citation UNITED STATES PATENT AND TRADEMARK OFFICE UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www.uspto.gov APPLICATION NO. FILING DATE FIRST NAMED INVENTOR ATTORNEY DOCKET NO. CONFIRMATION NO. 12/418,014 04/03/2009 Arno Refke P7765US 7589 78631 7590 04/01/2020 ROBERT S. GREEN OERLIKON METCO (US) INC. 1101 PROSPECT AVENUE WESTBURY, NY 11590 EXAMINER BAREFORD, KATHERINE A ART UNIT PAPER NUMBER 1718 NOTIFICATION DATE DELIVERY MODE 04/01/2020 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address(es): ROBERT.GREEN@OERLIKON.COM gbpatent@gbpatent.com greenblum.bernsteinplc@gmail.com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte ARNO REFKE and CHRISTOPH HOLLENSTEIN Appeal 2018-004498 Application 12/418,014 Technology Center 1700 Before BEVERLY A. FRANKLIN, GEORGE C. BEST, and JENNIFER R. GUPTA, Administrative Patent Judges. GUPTA, Administrative Patent Judge. DECISION ON APPEAL1 STATEMENT OF THE CASE Pursuant to 35 U.S.C. § 134(a), Appellant2 appeals from the Examiner’s decision to reject claims 18–25, 28, 29, 32, and 34–39. We have jurisdiction under 35 U.S.C. § 6(b). 1 In this Decision, we refer to the Specification filed April 3, 2009 (“Spec.”), the Final Office Action dated April 20, 2017 (“Final Act.”), the Appeal Brief filed October 23, 2017 (“Appeal Br.”), the Examiner’s Answer dated January 26, 2018 (“Ans.”), and the Reply Brief filed March 26, 2018 (“Reply Br.”). 2 We use the word Appellant to refer to “applicant” as defined in 37 C.F.R. § 1.42(a). Appellant identifies the real party in interest as Oerlikon Metco AG, Wohlen. Appeal Br. 3. Appeal 2018-004498 Application 12/418,014 2 We AFFIRM. CLAIMED SUBJECT MATTER The claims are directed to a method for coating and/or surface treating substrates using a plasma beam. Spec. 1, ll. 7–11. Independent claims 18, 29, and 32, reproduced below, are illustrative of the claimed subject matter: 18. A method for the coating and/or for the surface treatment of substrates in a working chamber, the method comprising: producing and directing via a plasma torch a plasma beam onto a substrate disposed in a working chamber, said plasma torch being spaced from the substrate by between 0.2 m and 2 m and said plasma beam being produced when a plasma gas is directed through the plasma torch and is heated via at least one of: electrical gas discharge; electromagnetic induction; and/or mircrowaves; and coating plural layers on the substrate having different compositions and thicknesses by applying said plural layers utilizing a same plasma torch and directly one after the other, wherein a first coating layer of the plural layers is arranged over the substrate and has greater thickness than a second coating layer arranged over the first coating layer, wherein the first coating layer is applied via thermal plasma spraying using greater power than the second coating layer and the second coating layer is applied via thermal plasma spraying using a power of between 8 and 16 kW and that utilizes a reactive component and wherein the reactive component is introduced into the plasma beam at a location that is: spaced from the plasma torch; where the plasma beam is a free plasma beam; and Appeal 2018-004498 Application 12/418,014 3 closer to the substrate than to the plasma torch. Appeal Br. 33 (Claims App.). 29. A method for the coating and/or for the surface treatment of substrates in a working chamber, the method comprising: producing and directing via a plasma torch a plasma beam onto a substrate disposed in a working chamber, said plasma beam being produced when a plasma gas, is directed through the plasma torch and is heated via at least one of: electrical gas discharge; electromagnetic induction; and/or microwaves; spacing said plasma torch from the substrate between 0.2 m and 2 m; and coating plural layers on the substrate having different compositions and thicknesses by applying said plural layers utilizing a same plasma torch and directly one after the other, wherein a first coating layer of the plural layers is arranged over the substrate and has less thickness than a second coating layer arranged over the first coating 1ayer, and wherein the second coating layer is applied via thermal plasma spraying using greater power than the first coating layer and the first coating layer is applied via thermal plasma spraying using a power between 8 and 16 kW and that utilizes a reactive component, and wherein the reactive component is introduced into the plasma beam at a location that is: where the plasma beam is a free plasma beam; closer to the substrate than to the plasma torch; and a few centimeters from the substrate. Id. at 35. Appeal 2018-004498 Application 12/418,014 4 32. A method for the coating and/or for the surface treatment of substrates in a working chamber, the method comprising: producing and directing via a DC plasma torch a plasma beam unto a substrate disposed in a working chamber, said plasma beam being produced when a plasma gas is directed through the plasma torch and is heated via at least one of: electrical gas discharge; electromagnetic induction; and/or microwaves; spacing said DC plasma torch from the substrate between a range of 0.2 m and 2 m; coating plural layers on the substrate having different compositions and thicknesses by applying said plural layers utilizing a same plasma torch and directly one after the other; utilizing a first power of between 8 and 16 kW and a pressure in the working chamber during application of a one of the plural layers via thermal plasma spraying of one of: between 0.01 and 10 mbar; between 0.02 and 5 mbar; or between 0.05 and 2 mbar; and utilizing a second power greater than the first power and a pressure in the working chamber during application of an other of the plural layers via thermal plasma spraying of one of: between 0.3 and 1 mbar; between 0.5 and 500 mbar; or between 1 and 200 mbar, wherein the one of the plural layers is applied using the second power and by introducing a reactive component into the plasma beam at a location that is: where the plasma beam is a free plasma beam; and closer to the substrate than to the plasma torch, and Appeal 2018-004498 Application 12/418,014 5 wherein the reactive component is a mixture of gaseous hexamethyldisiloxane (HMDSO) and oxygen. Id. at 35–36. REJECTIONS The Examiner maintains, and Appellant requests review of, the following rejections: 1. Claims 18–25, 28, 29, 32, and 34–39 under 35 U.S.C. § 112, first paragraph; 2. Claims 18–20, 22–24, 29, and 37–39 under pre-AIA 35 U.S.C. § 103(a) over Grosse3, either Muehlberger4 or Ray5, and Kang6, alone or further in view of Yang;7 3. Claim 21 under pre-AIA 35 U.S.C. § 103(a) over Grosse, either Muehlberger or Ray, and Kang, alone or further in view of Yang, and either Gruner8 or Truszkowska;9 4. Claim 25 under pre-AIA 35 U.S.C. § 103(a) over Grosse and either Muehlberger or Ray, and Kang, alone or further in view of Yang and Bao;10 5. Claim 28 under pre-AIA 35 U.S.C. § 103(a) over Grosse and either Muehlberger or Ray, and Kang, alone or in further view of Yang, and Wang;11 and 6. Claims 25, 32, and 34–36 under pre-AIA 35 U.S.C. § 103(a) over Grosse and either Muehlberger or Ray, and Kang, alone or further in view of Yang and Martin.12 3 Grosse et al., WO 01/40542 A1, published June 7, 2001 (“Grosse”). 4 Muehlberger, WO 96/06517, published February 29, 1996 5 Ray et al., US 6,238,843 B1, issued May 29, 2001 (“Ray”). 6 Kang, US 4,788,077, issued November 29, 1988. 7 Yang, US 6,641,673 B2, issued November 4, 2003. 8 Gruner, US 4,898,785, issued February 6, 1990. 9 Truszkowska, US 5,875,228, issued February 23, 1999. 10 Bao et al., US 2005/0009373 A1, published January 13, 2005 (“Bao”). 11 Wang et al., US 2002/0108871, published August 15, 2002 (“Wang”). 12 Martin, US 5,702,770, issued December 30, 1997. Appeal 2018-004498 Application 12/418,014 6 OPINION After review of the cited evidence in light of the Appellant’s and the Examiner’s opposing positions, we determine that Appellant has not identified reversible error in the Examiner’s rejections. In re Jung, 637 F.3d 1356, 1365 (Fed. Cir. 2011). Accordingly, we affirm the rejections for the reasons set forth below, in the Final Office Action, and in the Examiner’s Answer. We add the following. Written Description Although presented under separate headings, Appellant’s arguments regarding independent claims 18, 29, and 32 are substantially the same. Appeal Br. 9–11. We limit our discussion below to those claims. Each of the dependent claims included in the rejection will stand or fall with the independent claim from which it depends. 37 C.F.R. § 41.37(c)(1)(iv) (2017). The Examiner finds that the Specification, as filed, describes the layer applied using a power of between 8 kW and 16 kW as a thin SiOx (silicon oxide) layer. Final Act. 3. In addition, the Examiner finds that the Specification discloses that, typically, the power supply for thermal plasma spraying is 60 kW to 100 kW, “not every possible pressure greater than 8–16 kW.” Id.; Spec. 16, ll. 3–5. Therefore, the Examiner determines that the scope of claims 18, 29, and 32 is “broader than what is supported by the disclosure as filed” (Ans. 4, 5, 7) because the Specification does not provide written description support for: (1) claim 18 reciting “the first coating layer is applied via thermal plasma spraying using greater power than the second coating layer and the second coating layer is applied via thermal plasma spraying using a power of between 8 and 16 kW;” (2) claim 29 reciting “the Appeal 2018-004498 Application 12/418,014 7 second coating layer is applied via thermal plasma spraying using greater power than the first coating layer and the first coating layer is applied via thermal plasma spraying using a power of between 8 and 16 kW;” and (3) claim 32 reciting “utilizing a first power of between 8 and 16 kW and a pressure in the working chamber during application of a one of the plural layers via thermal plasma spraying.” Final Act. 3–4. Appellant argues that: (1) the paragraph bridging pages 14–15 of the Specification describes applying a SiOx layer using 8 kW to 16 kW power supplied to a plasma torch, (2) the paragraph bridging pages 15–16 of the Specification describes applying a first layer using 60 kW to 100 kW power supplied to the plasma torch, and (3) page 17, lines 4–11 of the Specification describes applying a second SiOx layer (11) over a first layer (12) (Fig. 3A). Appeal Br. 9–11. Appellant contends that this disclosure “provides full and clear written description support” for the disputed limitations of claims 18, 29, and 32. Id. “[T]he test for [compliance with the written description requirement] is whether the disclosure of the application relied upon reasonably conveys to those skilled in the art that the inventor had possession of the claimed subject matter as of the filing date.” Ariad Pharm., Inc. v. Eli Lilly & Co., 598 F.3d 1336, 1351 (Fed. Cir. 2010) (en banc). We have reviewed the portions of the Specification relied upon by Appellant, but find that the written description is not commensurate in scope with claims 18, 29, and 32, i.e., Appellant has not pointed to sufficient written description support for applying a coating layer other than SiOx via thermal plasma spraying using a power of between 8 kW and 16 kW. Likewise, we do not find that Appellant’s have pointed to sufficient written description support for applying two coating layers where one layer is Appeal 2018-004498 Application 12/418,014 8 applied using a power of between 8 kW and 16 kW and another layer is applied using any power greater than between 8 kW and 16 kW. Although we acknowledge that page 16 of Appellant’s Specification discloses using a greater power (e.g., 60 kW to 100 kW) in applying a first layer (Spec. 16), the claims on appeal are not so limited. Accordingly, we sustain the Examiner’s written description rejection of claims 18–25, 28, 29, 32, and 34–39. Obviousness over Grosse, either Muehlberger or Ray, and Kang, alone or further in view of Yang The Examiner rejected claims 18–20, 22–24, 29, and 37–39 under pre-AIA 35 U.S.C. § 103(a) over Grosse13, either Muehlberger or Ray, and Kang, alone or further in view of Yang. Final Act. 5. Although presented under separate headings, Appellant’s arguments regarding independent claims 18 and 29 are substantially the same. Appeal Br. 14, 19–20. We limit our discussion to those claims, and in particular to the elements of those claims in dispute between the Appellant and the Examiner. Each of the dependent claims included in the rejection will stand or fall with the independent claim from which it depends. 37 C.F.R. § 41.37(c)(1)(iv). A complete statement of the rejection is set forth in the Final Office Action at pages 5–19. We focus our discussion below, however, on the 13 The Examiner refers to Grosse et al., US 7,771,798 B1, issued August 10, 2010, as an English language equivalent of WO 01/40542 A1. Ans. 9. Because Appellant does not contest the Examiner’s reliance on US 7,771,798 B1, we do the same. Thus, the cited column and line number for Grosse herein refer to US 7,771,798. Appeal 2018-004498 Application 12/418,014 9 elements of claims 18 and 29 in dispute between the Appellant and the Examiner. The Examiner finds that Grosse teaches a method for coating and/or for the surface treatment of substrates in a working chamber (Final Act. 5 (citing Grosse 1:5–7)) where the method includes, inter alia: (1) a plasma torch being spaced from the substrate between 0.2 m and 2 m (id. at 7 (citing Grosse 5:1–6; Fig. 2)); and (2) a reactive component introduced into the plasma beam at a location that is: a. spaced from the plasma torch (id. at 6 (citing Grosse Fig. 2)), b. where the plasma beam is a free plasma beam (id. at 6–7 (citing Grosse Fig. 2)), and c. closer to the substrate than to the plasma torch (id. at 6 (citing Grosse 5:15–46, 50–52, 6:10–35, 8:50–65; Fig. 2)). Regarding thermal plasma spraying using a power between 8 kW and 16 kW, the Examiner finds that Grosse discloses that its method can include composite layer systems using different precursor materials in a plasma jet source (torch), such as a DC torch, having adjustable conditions so that different precursor materials may be processed differently. Final Act. 13 (citing Grosse 2:64–3:10, 45–55). Like Grosse, the Examiner finds that Kang discloses a method for coating the surface of a substrate using a direct current (DC) torch and adjusting the process conditions or parameters to optimize the properties of the coating, and further teaches that power input for its plasma spraying include powers ranging from 8 kW to 16 kW. Id. at 13–14 (citing Kang 2:25–45, 9:35–40). The Examiner finds that it would have been obvious, based on Kang’s teachings, to use a plasma spraying torch with a power of between 8 kW and 16 kW in Grosse’s coating method to provide a desirable coating. Id. at 14. Appeal 2018-004498 Application 12/418,014 10 Appellant identifies four main reasons for reversing the Examiner’s rejection. Appeal Br. 14, 19–20. The reactive component is introduced into the plasma beam at a location that is “closer to the substrate than to the plasma torch.” First, Appellant’s argue that Grosse teaches that the reactive gas (15) is introduced into the plasma beam (10) at a location from the substrate that is farther from, not closer to, the substrate (12) than to the plasma torch (11). Id. at 14, 19. Appellant’s argument is not persuasive of reversible error. As the Examiner finds, Grosse teaches that its precursor material (16), a reactive component, can be introduced into the free plasma beam downstream of the plasma torch and closer to the plasma. Ans. 9 (citing Grosse 5:50–52, 6:10– 35, 8:50–65; Fig. 2). Spacing the plasma torch from the substrate “between 0.2 m and 2 m.” Second, Appellant’s argue that the Examiner “has not alleged” that Grosse “teaches the recited spacing between the plasma torch and the substrate of between 0.2 m and 2 m.” Appeal Br. 14, 20. Appellant’s argument is not persuasive of reversible error because merely reciting the claim language, and asserting that the Examiner’s findings do not describe such limitations is not a persuasive argument. See In re Lovin, 652 F.3d 1349, 1357 (Fed. Cir. 2011) (“[W]e hold that the Board reasonably interpreted Rule 41.37 to require more substantive arguments in an appeal brief than a mere recitation of the claim elements and a naked assertion that the corresponding elements were not found in the prior art.”). Appeal 2018-004498 Application 12/418,014 11 Additionally, as the Examiner finds, Grosse teaches that its plasma jet typically impinges on a substrate at a distance of about 10 cm to 100 cm (0.1 m to 1.0 m). Ans. 10–11 (citing Grosse 5:1–6). It is well-established that a prima facie case of obviousness exists when the claimed and prior art ranges overlap. In re Peterson, 315 F.3d 1325, 1329 (Fed. Cir. 2003). The reactive component is introduced into the plasma beam at a location that is “where the plasma beam is a free plasma beam.” Third, Appellant argues that the Examiner has not shown that Grosse “teaches or suggests that the reactive component is introduced into the plasma beam at a location that is where the plasma beam is a free plasma beam.” Appeal Br. 14, 20. As with the previous argument, Appellant’s third argument is not persuasive of reversible error because it merely recites the claim language, and asserts that the Examiner’s findings do not describe such limitations. See Lovin, 652 F.3d at 1357. Further, the Examiner finds that Grosse teaches introducing its reactive component into a free plasma beam. Ans. 11–12 (citing Grosse 5:20–25, Fig. 2). Appellant does not address or identify a reversible error in the Examiner’s finding. Appeal Br. 14, 20; Reply Br. 2–5. Applying a coating layer “using a power of between 8 and 16 kW.” Finally, Appellant argues that Grosse fails to teach or suggest the coating layer with a reactive component is applied using lower power than used for another applied layer, where the lower power is in the range of 8 to 16 kW. Appeal Br. 14. Again, as with Appellant’s previous arguments, Appellant’s fourth argument is not persuasive of reversible error because it merely recites the Appeal 2018-004498 Application 12/418,014 12 claim language, and asserts that the Examiner’s findings do not describe such limitations. See Lovin, 652 F.3d at 1357. Moreover, Appellant’s argument is not persuasive because it fails to address the facts and reasoning set forth by the Examiner in the rejection. The Examiner does not rely on Grosse alone for teaching a power of between 8 kW and 16 kW. Rather, the Examiner determines that it would have been obvious to modify Grosse’s plasma torch, based on Kang, to use a power of between 8 kW and 16 kW to produce a desirable coating. Final Act. 13–15; Ans. 12–14. Appellant does not dispute or otherwise identify error in the Examiner’s findings and reasoning. See In re Keller, 642 F.2d 413, 426 (CCPA 1981) (“one cannot show non-obviousness by attacking references individually where, as here, the rejections are based on combinations of references.”). Remaining Rejections Although presented under separate headings, Appellant does not make additional arguments for the patentability of separately rejected claims 21, 25, 28, 32, and 34–36. Appeal Br. 23–31. Appellant argues claim 32 is patentable for the same reasons as claims 18 and 29 discussed above. Id. at 28. Appellant argues that claims 21, 25, and 28, which depend from claim 18, and claims 34–36, which depend from claim 32, are allowable based on their dependency. See id. Because we find no insufficiency in the Examiner’s rejection of claims 18 and 29 over Grosse and either Muehlberger or Ray, and Kang, alone or further in view of Yang, we sustain the rejections of claims 21, 25, 28, 32, and 34–36. Appeal 2018-004498 Application 12/418,014 13 DECISION SUMMARY In summary: Claims Rejected 35 U.S.C. § Reference(s)/Basis Affirmed Reversed 18–25, 28, 29, 32, 34– 39 112 Written Description 18–25, 28, 29, 32, 34– 39 18–20, 22– 24, 29, 37– 39 103(a) Grosse, Muehlberger, Kang 18–20, 22– 24, 29, 37– 39 18–20, 22– 24, 29, 37– 39 103(a) Grosse, Muehlberger, Kang, Yang 18–20, 22– 24, 29, 37– 39 18–20, 22– 24, 29, 37– 39 103(a) Grosse, Ray, Kang 18–20, 22– 24, 29, 37– 39 18–20, 22– 24, 29, 37– 39 103(a) Grosse, Ray, Kang, Yang 18–20, 22– 24, 29, 37– 39 21 103(a) Grosse, Muehlberger, Kang, Gruner 21 21 103(a) Grosse, Muehlberger, Kang, Yang, Gruner 21 21 103(a) Grosse, Muehlberger, Kang, Truszkowska 21 21 103(a) Grosse, Muehlberger, Kang, Yang, Truszkowska 21 21 103(a) Grosse, Ray, Kang, Gruner 21 21 103(a) Grosse, Ray, Kang, Yang, Gruner 21 Appeal 2018-004498 Application 12/418,014 14 21 103(a) Grosse, Ray, Kang, Truszkowska 21 21 103(a) Grosse, Ray, Kang, Yang, Truszkowska 21 25 103(a) Grosse, Muehlberger, Kang, Bao 25 25 103(a) Grosse, Muehlberger, Kang, Yang, Bao 25 25 103(a) Grosse, Ray, Kang, Bao 25 25 103(a) Grosse, Ray, Kang, Yang, Bao 25 28 103(a) Grosse, Muehlberger, Kang, Wang 28 28 103(a) Grosse, Muehlberger, Kang, Yang, Wang 28 28 103(a) Grosse, Ray, Kang, Wang 28 28 103(a) Grosse, Ray, Kang, Yang, Wang 28 25, 32, 34– 36 103(a) Grosse, Muehlberger, Kang, Martin 25, 32, 34– 36 25, 32, 34– 36 103(a) Grosse, Muehlberger, Kang, Yang, Martin 25, 32, 34– 36 25, 32, 34– 36 103(a) Grosse, Ray, Kang, Martin 25, 32, 34– 36 25, 32, 34– 36 103(a) Grosse, Ray, Kang, Yang, Martin 25, 32, 34– 36 Overall Outcome 18–25, 28, 29, 32, 34– 39 Appeal 2018-004498 Application 12/418,014 15 TIME PERIOD FOR RESPONSE No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. § 1.136(a). See 37 C.F.R. § 1.136(a)(1)(iv). AFFIRMED Copy with citationCopy as parenthetical citation