Ariz. Admin. Code § tit. 9, ch. 14, art. 6, tbl. 6.4
QUALITY CONTROL PARAMETERS WITHOUT ACCEPTANCE CRITERIA SPECIFIED IN THE METHOD | DEFAULT LIMITS |
Matrix Spike/LFM (processed or non-processed) | LCS/LFB |
Matrix Spike/LCS for 8000 methods | ±30%. |
LCS/LFB (processed or non-processedVSecond source reference standard | CCV/continuing IPC |
LOO/MRL (non-processed) | CCV/continuing IPC or ± 50% |
LOO/MRL (processed) | LCS/LFB or ±50% |
Methods that do not specify the LOO/MRL | ± 50% |
OCS (non-processed) | ICV/continuing IPC/manufacturer's limits |
OCS (processed) | LCS/LFB/manufacturer's limits |
IDOC limits | LFB/LCS |
LFB/LCS/LFM/duplicate RPD | IDOC limits/?20% |
Non-CCC compounds | CCC limits |
ICV/CCV | ± 10% |
500, 600, 1600, and 8000 series methods that do not specify surrogates or acceptance limits for surrogates | 70-130%. |
500, 600, 1600, and 8000 series methods that do not specify internal standards or acceptance limits for internal standards | 70-130%. |
Methods that do not list a precision measurement | 20% RPD |
Ariz. Admin. Code tit. 9, ch. 14, art. 6, tbl. 6.4