Ex Parte Davis et alDownload PDFPatent Trial and Appeal BoardNov 26, 201814237878 (P.T.A.B. Nov. 26, 2018) Copy Citation UNITED STA TES p A TENT AND TRADEMARK OFFICE APPLICATION NO. FILING DATE 14/237,878 04/07/2014 96537 7590 11/28/2018 BEUS SE WOLTER SANKS & MAIRE Mail Stop AG 390 N. ORANGE A VE, SUITE 2500 ORLANDO, FL 32801 FIRST NAMED INVENTOR Anthony Davis UNITED STATES DEPARTMENT OF COMMERCE United States Patent and Trademark Office Address: COMMISSIONER FOR PATENTS P.O. Box 1450 Alexandria, Virginia 22313-1450 www .uspto.gov ATTORNEY DOCKET NO. CONFIRMATION NO. 2011P08691WOUS (053) 4839 EXAMINER BRATLAND JR, KENNETH A ART UNIT PAPER NUMBER 1714 NOTIFICATION DATE DELIVERY MODE 11/28/2018 ELECTRONIC Please find below and/or attached an Office communication concerning this application or proceeding. The time period for reply, if any, is set in the attached communication. Notice of the Office communication was sent electronically on above-indicated "Notification Date" to the following e-mail address(es): USPTO@patentorlando.com USPTO@dockettrak.com PTOL-90A (Rev. 04/07) UNITED STATES PATENT AND TRADEMARK OFFICE BEFORE THE PATENT TRIAL AND APPEAL BOARD Ex parte ANTHONY DA VIS and DETLEF HAJE Appeal2017-007564 Application 14/237,878 Technology Center 1700 Before MICHAEL P. COLAIANNI, JENNIFER R. GUPTA, and DEBRA L. DENNETT, Administrative Patent Judges. COLAIANNI, Administrative Patent Judge. DECISION ON APPEAL Appellants 1 appeal under 35 U.S.C. § 134 the final rejection of claims 16-33 and 35.2 We have jurisdiction over the appeal pursuant to 35 U.S.C. § 6(b). We AFFIRM. The claims on appeal are directed to a method of manufacturing a component, such as a gas turbine blade, from a single crystal or a directionally solidified material (Spec. 1:9-11 ). 1 "The real party in interest in this Appeal is the assignee, Siemens Aktiengesellschaft." App. Br. 1. 2 Appellants canceled claim 34 in their November 4, 2016, Response to the Final Office Action. See Advisory Action 2. Appeal2017-007564 Application 14/237,878 Claim 16 is illustrative: 16. A method for manufacturing a component of a single crystal or a directionally solidified material, said component being manufactured having a predefined shape, compnsmg: superimposing at least a powder layer of a powder of a first material onto at least a surface of a substrate out of a second, single crystal or directionally solidified, material; transforming the powder layer into a substrate layer with a new surface of the substrate by altering at least a physical condition of the first material of the powder by applying energy to the powder layer; wherein said substrate layer is becoming a part of the substrate; wherein the second, single crystal or directionally solidified, material of the substrate has a grain orientation and the material of the substrate layer has a grain orientation; wherein the material of the substrate layer adopts the same grain orientation as the grain orientation of the substrate during the transforming process; detecting the grain orientation of the material of the substrate layer in situ and when the grain orientation of the material of at least a section of the substrate layer is different from the grain orientation of the substrate, said section of the substrate layer is transformed by altering a physical condition of the material of the section by applying energy to correct the grain orientation of the section of the substrate layer in situ; and wherein the steps are repeated till the component has grown layer by layer into the predefined shape while a process temperature is maintained below a melting temperature of at least the first material. Appellants appeal the following rejections: 1. Claims 16-21, 23-31, and 33 are rejected under 35 U.S.C. § I03(a) as unpatentable over Morris et al. (US 2011/0135952 Al; publ. June 9, 2011) ("Morris") in view of Chen-Nan Sun et al. (Effect of Laser 2 Appeal2017-007564 Application 14/237,878 Sintering on Ti-ZrB2 Mixtures, 94 J. AM. CERAM Soc. 3282-85 (2011)) ("Sun"). 2. Claims 22, and 32 are rejected under 35 U.S.C. § I03(a) as unpatentable over Morris in view of Sun and Benda et al. (US 5,508,489; iss. Apr. 16, 1996) ("Benda"). 3. Claim 35 is rejected under 35 U.S.C. § I03(a) as unpatentable over Morris in view of Sun and Tanabe et al. (US 2004/0009632 Al; publ. Jan. 15, 2004) ("Tanabe"). FINDINGS OF FACT & ANALYSIS Rejection (1): Claims 16-21, 23-31, and 33 Appellants argue the subject matter of claims 16, 29, and 30 separately (App. Br. 7-17). Any claim not argued separately will stand or fall with the sole independent claim 16. Claim 16 Appellants argue that neither Morris nor Sun teach all the limitations of claim 16 (App. Br. 7-8). Appellants contend that Morris and Sun do not teach detecting grain orientation of the substrate layer in situ when the grain orientation of the material of at least a section of the substrate layer is different from the grain orientation of the substrate and applying energy to correct the grain orientation of the section of the substrate layer in situ (App. Br. 7). Appellants contend that the Examiner's determination that the one of ordinary skill in the art, based upon the teachings of Morris and Sun, would have applied additional laser sintering until the desired microstructure is 3 Appeal2017-007564 Application 14/237,878 obtained is unsupported by evidence because the references do not teach the disputed steps (App. Br. 8). The claim limitation in dispute recites: detecting the grain orientation of the material of the substrate layer in situ and when the grain orientation of the material of at least a section of the substrate layer is different from the grain orientation of the substrate, said section of the substrate layer is transformed by altering a physical condition of the material of the section by applying energy to correct the grain orientation of the section of the substrate layer in situ. (Emphasis added). The Examiner finds that the step of applying additional energy to correct the grain orientation is conditioned on the material having a different grain orientation than the grain orientation of the substrate (Ans. 2). We construe the disputed claim limitation in accord with the Examiner that the step of applying additional energy to correct grain orientation is only used when a different grain orientation is detected. In other words, the grain correction step is optional and is not be necessary when no defect in grain orientation is detected. With this claim construction in mind, we find that the Examiner's rejection is premised on combining Sun's teaching to use high temperature X-ray diffraction (HTXRD) to monitor the crystal structure of a high temperature material with Morris' process for forming a gas turbine by laser sintering layers of metal alloy powder atop one another. Final Act. 5. In other words, taking into account the conditional nature of the grain reorienting step, the process recited in the claim is satisfied by applying layers which have the desired grain orientation as determined by the HTXRD of Sun. The combined teachings of Morris and Sun do not need to teach the subsequent reheating with additional energy to reorient the grain in 4 Appeal2017-007564 Application 14/237,878 order to satisfy the claim. Ex parte Schulhauser, 2013-007847, 2016 WL 6277792, at *5 (PTAB Apr. 28, 2016) (precedential). Accordingly, we are unpersuaded by Appellants' argument that the art does not teach detecting and reorienting the grain of the alloy. Appellants make the following additional arguments regarding claim 16: (1) a person of ordinary skill would not have found it obvious to modify Morris's process that laser sinters two substantially identical materials with Sun's HTXRD technique, which assesses the elemental distribution between phases of two different materials (App. Br. 9), (2) prolonging the laser sintering process to achieve the desired microstructural orientation runs counter to Morris' teaching to reduce lead time in making a rotor (App. Br. 9), (3) Sun teaches away from prolonging the laser sintering by using an induction heater to mitigate thermal stress caused by the scanning laser beam (App. Br. 10), (4) the combination would have required replacing one or both laser scans in Morris with Sun's induction heater, which would have frustrated Morris' purpose (App. Br. 11 ), ( 5) the Examiner engaged in impermissible hindsight in concluding that the ordinarily skilled artisan interested in utilizing the laser-based process of Morris would instantly recognize that additional corrective measures necessary in response to the XRD measurements may be performed using the laser itself (App. Br. 12), (6) Sun teaches heating the sintered sample to a temperature between 298 Kand 1023 K which would likely damage Morris' equipment (App. Br. 12), and (7) Morris teaches that the metal powder layer has the same orientation as the seed crystal, so there is no defect to correct (App. Br. 13). 5 Appeal2017-007564 Application 14/237,878 Appellants' arguments are not persuasive. Regarding arguments ( 1) and (7), the Examiner's rejection is based upon using Sun's X-ray diffraction to monitor the change in phases/microstructure with temperature, if any (Final Act. 5; Ans. 2). Under the broadest reasonable claim construction, the conditional limitation need not be performed for the claim to be satisfied. Therefore, using Sun's high temperature X-ray diffraction (HTXRD) to monitor the phases in Morris' formed layers would have been obvious. If, as argued by Appellants, Morris' process yields layers having the desired crystal structure as determined by using Sun's HTXRD, then the claims are satisfied even though no grain reorienting step is used. Regarding arguments (2) to (4), Sun teaches to use an induction heater in addition to the laser heating (Sun 3282). Sun teaches that the induction heater mitigates thermal stress, but Sun does not teach using an induction heater in lieu of laser sintering. In other words, even assuming that Appellants' argument is correct that an induction heater would have been required by the combination, the claim does not exclude using an induction heater in addition to the laser sintering; the claim uses the open ended transition language "comprising." Moreover, including Sun's induction heater would appear to reduce the laser sintering time because the layer would be heated by means other than the laser itself. Appellants' argument that extending the time of laser sintering runs counter to Morris' teachings to reduce lead time is not persuasive. Morris teaches that reducing lead time is desirable (i14). However, ensuring that a layer has the desired phase would appear to shorten lead time because the discard and remake cycling would be reduced. We are not persuaded that Morris' teaching to reduce lead time 6 Appeal2017-007564 Application 14/237,878 would teach way from using a longer laser sintering time to achieve the desired microstructure. Regarding argument ( 5), the Examiner did not engage in impermissible hindsight in concluding that the claimed invention given the broadest reasonable interpretation would have been obvious over the combined teachings of Morris and Sun. Sun teaches monitoring a material by using HTXRD to determine how the microstructure of the layer changes with temperature (Sun Figs. 6 & 7). We conclude that the combined teachings of Morris and Sun would have suggested that monitoring the crystal phases using HTXRD and controlling the laser sintering/heating to achieve a desired phase. Accordingly, the applied prior art would have suggested monitoring the crystal phases and controlling the heating to achieve the desired phase. Regarding argument ( 6), Appellants' argument amounts to arguing that a person of ordinary skill in the art would have bodily incorporated Sun's teaching regarding temperatures into Morris' process. Morris and Sun use different materials, so that one of ordinary skill in the art would have tailored the temperature to suit the particular material being treated. Appellants' argument fails to appreciate that one of ordinary skill in the art is a person of ordinary creativity, not an automaton. KSR Int 'l Co. v. Teleflex Inc., 550 U.S. 398,421 (2007). On this record, we affirm the Examiner's§ 103(a) rejection of claim 16. 7 Appeal2017-007564 Application 14/237,878 Claim 29 Claim 29 depends from claim 16 and recites that the "thickness of the powder layer of the powder of the first material is 2 mm." Appellants argue that Morris' teaching to use a powder layer thickness between 15 to 50 microns does not overlap with the powdered thickness recited in claim 29 (App. Br. 14--15). Appellants contend that there is no prima facie case of obviousness because there is no overlap between the thicknesses (App. Br. 15). Appellants' argument is not persuasive because the Examiner does not rely on overlapping ranges as a basis for concluding obviousness. Rather, the Examiner finds that Morris teaches that the powder layer thickness may be greater than the 15 to 50 micron example (Final Act. 8). The Examiner finds that since the layer thickness determines the ultimate thickness of the sintered layer, the ordinarily skilled artisan would have tailored the thickness to suit a particular application (Final Act. 8). Appellants' arguments fail to identify reversible error in the specific findings and conclusion of the Examiner. Claim 30 Claim 30 depends from claim 16 and recites wherein the energy applied during the transforming of the powder layer into the substrate layer has a first power per unit area and the energy applied to correct the grain orientation of the section of the substrate layer has a second power per unit area that is less than the first power per unit area. Appellants argue that none of the disclosed laser power ranges are used to correct the grain orientation of a section of the substrate layer (App. Br. 16). This argument is not persuasive because the broadest reasonable 8 Appeal2017-007564 Application 14/237,878 interpretation of the claim includes a process where the grain reorienting step depends upon the detection of an improper grain microstructure. As argued by Appellants, Morris teaches that the powder layers have the same grain orientation as the substrate, so the condition necessary for implementing the grain reorienting step is not satisfied. In other words, the other limitations in the claims are met and the grain reorienting step is not necessary in the process as taught by the combined teachings of Morris and Sun. Rejection (2): Claims 22and 32 Appellants argue the subject matter of claim 22 only (App. Br. 18- 20). Appellants argue that Morris requires a particular laser beam power per unit area and the Examiner's proposed modification to use a lower energy per unit area would frustrate Morris' purpose of melting the specific metal powder (App. Br. 18-19). Appellants contend that the Examiner has not established a prima facie case of obviousness (App. Br. 19). Appellants argue that Morris' laser power per unit area is 6250 W/cm2 which does not overlap or lie inside the claimed laser power per unit area range of 50 W/cm2 to 150 W/cm2 (App. Br. 20). Contrary to Appellants' arguments, the Examiner relies on the teachings of Benda to teach that the laser power is a result effective variable (Final Act. 11 ). The Examiner finds that Benda would have suggested adjusting "the laser beam intensity to within the range of 50 to 150 Watts/ cm2 ... [ in order to achieve the] desired amount of heating to the powdered layer during the laser-based sintering process of Morris and Sun" 9 Appeal2017-007564 Application 14/237,878 (Final Act. 11 ). We understand the Examiner's combination of the teachings of Benda with Morris as modified by Sun to include using the less focused and more focused laser beam arrangement in Benda. In other words, the claims do not exclude using two laser beams, wherein one of them operates at a power per unit area within the claimed range to heat the material broadly while the more focused beam laser sinters the material. Benda teaches that the using a split laser beam arrangement that includes a focused and unfocused beam reduces thermal gradients and prevents curling of the material being sintered (Benda col. 1, 11. 55-59; col. 2, 11. 49-52). Appellants do not dispute the Examiner's finding that Benda teaches that laser power per surface area is a result effective variable that would have been readily optimizable (App. Br. 18-20). The combination would not have frustrated Morris' purpose because the lower power, less focused laser beam, would have been used with the higher power, more focused laser beam, to sinter the material on the substrate as taught by Benda. Rejection (3): Claim 35 Appellants argue that Morris and Tanabe do not teach forming a melt pool of the melted metal powder and melted substrate as required by claim 35 (App. Br. 21 ). Appellants argue that Tanabe does not teach cooling a melt pool by applying energy with a second power per unit area applied to correct the grain orientation of the section of the substrate layer (App. Br. 21 ). Appellants contend that Tanabe does not teach cooling a melt pool prior to detecting the grain orientation, which is different than the grain orientation of the substrate (App. Br. 21). 10 Appeal2017-007564 Application 14/237,878 Under the broadest reasonable interpretation noted above, the step of correcting the grain orientation does not need to be performed as it is a conditional step. Therefore, Appellants' argument that Tanabe does not teach applying a second power per unit area to correct grain orientation is not persuasive. The Examiner finds that Morris must teach some melting of the substrate along with the powdered layer to form a melt pool in order for the melted powder to assume the crystal structure of the substrate (Final Act. 13-14). The Examiner's position is reasonable in light of Morris' teachings that the laser scan re-melts the powder layer and few micron thickness of the substrate (i135). Appellants do not specifically identify reversible error with that finding. Appellants argue that Tanabe is non-analogous art because it is not in the same field of endeavor and not reasonably pertinent to Appellants' problem (App. Br. 22). Appellants argue that Tanabe is not in the same field of endeavor because it does not share the same U.S. Patent Office classification class and subclass (App. Br. 22). Appellants contend that Tanabe is not reasonably pertinent to Appellants' problem, namely, a method of manufacturing a component of a single crystal or a directionally solidified material (App. Br. 22). Appellants argue that Tanabe is directed to forming thin films on semiconductors, whereas Morris is directed to the field of engines and turbine components for engines (App. Br. 23). Appellants contend that the mere fact that Tanabe and Morris use laser melting does not mean that their teachings are reasonably pertinent to a method of manufacturing a gas turbine component (App. Br. 23). 11 Appeal2017-007564 Application 14/237,878 The Examiner finds that Tanabe's method includes laser-based melting and recrystallization of a deposited layer, which is the exact same process as used by Morris (Ans. 7). The Examiner finds that Tanabe is both in the same field of endeavor as Morris and is reasonably pertinent to the problem to be solved (Ans. 7). The field of endeavor is determined by reference to explanations of the invention's subject matter in the patent application, including the embodiments, function, and structure of the claimed invention. In re Bigio, 381 F.3d 1320, 1325 (Fed. Cir. 2004). The proper inquiry is determined by consulting the structure and function of the claimed invention as perceived by one of ordinary skill in the art. Id. at 1326. In the present case, the claimed invention is forming a "component" by laser sintering. The claims are not limited to a gas turbine component. Indeed, the field of invention section of the Specification states, "[ t ]he present invention relates to a method for manufacturing a component from a single crystal or a directionally solidified material." (Spec. 1:9-11). The disclosure and claims include a field of endeavor broader than argued by Appellants. Therefore, we find that Tanabe's laser-melting and recrystallization process would have been in the same field of endeavor as Appellants' claimed invention. Like the Examiner, we also find that Tanabe' s disclosure regarding laser sintering and recrystallization of the melt would have been reasonably pertinent to Appellants' problem of ensuring the desired crystal structure in the layer. Appellants argue that combining Tanabe' s teaching to use a lower power after melting powder would render Morris unsatisfactory for its intended purpose (App. Br. 24). Appellants contend that proposed 12 Appeal2017-007564 Application 14/237,878 modification would entail using a second lower power scan in which the metal powder does not melt and Morris' structure would not be formed (App. Br 24). Appellants argue that Tanabe's teachings are specific to silicon films and would not have been applicable to Morris' metal powders (App. Br. 24). Appellants argue that Tanabe uses pulse laser parameters, which would not have been applicable to Morris' continuous-wave parameters (App. Br. 24). Appellants' arguments are not persuasive because these arguments would require us to find that one of ordinary skill in the art would have bodily incorporated Tanabe's parameters into Morris' method without regard for the material being processed. A person of ordinary skill in the art is a person of ordinary creativity, not an automaton. KSR, 550 U.S. at 421. The Examiner finds that Tanabe teaches the benefits of using lower laser power during cooling of the melt to encourage recrystallization (Final Act. 14). A person of ordinary skill in the art would have tailored the laser parameters to the particular material in order to achieve the desired benefits taught by Tanabe (i.e., forming a crystalline material rather than a mi crocrystalline material). On this record, we affirm the Examiner's§ 103(a) rejections (1) to (3) listed above. DECISION The Examiner's decision is affirmed. No time period for taking any subsequent action in connection with this appeal may be extended under 37 C.F.R. § 1.136(a). See 37 C.F.R. § 1.136(a)(l )(iv). 13 Appeal2017-007564 Application 14/237,878 AFFIRMED 14 Copy with citationCopy as parenthetical citation